EUROPEAN COMMISSION Brussels, 07.04.2011

Transcripción

EUROPEAN COMMISSION
Brussels, 07.04.2011
SEC(2011) 475 final
PART III
COMMISSION STAFF WORKING DOCUMENT
ON THE IMPLEMENTATION OF NATIONAL RESIDUE MONITORING PLANS IN
THE MEMBER STATES IN 2009
(Council Directive 96/23/EC)
1
PART III
Actions taken as a consequence of non compliant results
including modifications of the national residue plan for
2009
2
AT
AUSTRIA
Group A substances
Modification of national residue
plan
Information with regard to the
recommendations of the CRL
Bilthoven
Berlin (plan 2008)
Accreditation and validation of
Group A substances or
forbidden substances
according to Council Decision
2002/657/EC
New in the plan 2009
Due to compliant results over a
two or more years period, the
number of samples will be
decreased
Due to non-compliant results in
2008, the number of samples
will be increased
General information
Non-compliant results
1 17alpha-boldenone-21.9 µg/l and
17 beta-boldenone-< 0.38 µg/l and
1 17alpha-boldenone-3.4 µg/l-young
bovine
(1. follow-up investigation; suspect
sample, farm)
2 17alpha-boldenone- 2.87 and 6.46
µg/l-young bovines
(2. follow-up investigation; suspect
samples, farm)
Aggregate for all animal products and substances
See Plan Data Information of Plan 2010
Follow-up actions
Bovines
• Three follow-up samples (1. Follow-up
investigation, urine samples) were taken as a
consequence of a non compliant result in 2008.
The farm was investigated by an official
veterinarian. About
70 bovine animals were held on the farm.
• Verification of the records.
• 2. Follow-up investigation: 2 Official samples
were taken (urine samples).
• Intensified supervision/checks for the following
12 months.
• Sampling in 2010 showed a negative result.
There was no indication of an illegal use of 17betaboldenone; therefore no administrative proceedings
3
1 17alpha-boldenone-4.55 µg/l young bovine
(suspect sample, farm)
were started against the farmer.
• Three follow-up samples were taken as a
consequence of a non compliant result in 2008.
The farm with about 12 bovine animals was
investigated by an official veterinarian.
• Verification of the records.
• Intensified supervision/checks for the following
12 months.
• Sampling in 2010.
There was no indication of an illegal use of 17betaboldenone; therefore no administrative proceedings
were started against the farmer.
Sheep and goats
1 17alpha-nortestosterone-1.02 µg/l
• The farm was investigated and placed under
and 17 beta-nortestosterone-< 0.37
official control (18/06/2009-24/08/2009) by the
µg/l-lamb
Provincial Governor (official veterinarian) in
(targeted sample, slaughterhouse)
accordance with article 58 of the Food Safety
and Consumer Protection Act.
• Verification of the records and the
administration of veterinary medicinal products.
• Three official samples were taken (on-farm
sampling; urine); the analyses showed a negative
result.
There was no indication of an illegal treatment of
the
animals;
therefore
no
administrative
proceedings were started against the farmer.
1 17alpha-boldenone- 2.55 µg/l and
17beta-boldenone- < 0.33 µg/l-lamb
(suspect sample, farm)
•
•
This was a follow-up sample as a consequence
of a positive test result in 2008.
Investigations on the farm of origin by official
veterinarian including verification of records.
There was no indication of an illegal use of 17betaboldenone.
4
Group B substances
Modification of national residue plan
Berlin (plan 2008)
New in the plan 2009
General information
Due to compliant results over a
two or more year period, the
number of samples will be
decreased
Due to non-compliant results in
2008, the number of samples will
be increased
1 Sulfadiazin-312.8 ppb and
Sulfadimidin-5,369.9-muscle-veal calf
1 Penicillin G-96.2 ppbmuscle-young
bovine
Aggregate for all animal products and
substances
-
Follow-up actions
Bovines
• Investigations on the farm of origin by official
• The withdrawal period had not been observed.
• Administrative proceedings were started
against the farmer.
•
The withdrawal period had been observed
correctly.
Animals of the farm will be checked in 2010
(sampling at slaughterhouse).
•
•
1 Ivermectin-543.4 ppb-liver-young
bovine
•
The administration of Ivermectin was not
entered in the register.
One official follow-up sample (liver) was
taken; the analysis showed a negative result.
Oral instruction of the farmer.
•
•
•
1 Dihydrostreptomycin-9,055.8 ppbkidney-veal calf
(suspect sample, slaughterhouse)
•
The carcase was impounded at the
slaughterhouse and the offals were declared
unfit for human consumption.
The treatment had been recorded correctly; the
withdrawal period had been observed.
•
•
5
1 Oxytetracycline-2,654.97 ppbmuscle-cow
•
Emergency slaughter because of a liver
damage.
slaughterhouse and declared unfit for human
consumption.
The veterinary practitioner’s dispensary of the
veterinarian in charge of the farm was checked
too.
correctly but the withdrawal period was too
short (due to a mistake of the veterinarian in
charge).
Administrative proceedings were started
against the farmer and the veterinarian in
charge of the farm.
•
•
•
•
•
1 Oxytetracycline-2,389.0 ppbmuscle-cow
•
consumption.
The storage of the VMPs on the farm was not
correct.
(later on, the manufacturers extended the
withdrawal period from 14 to 21 days).
The veterinary practitioner`s dispensary of the
veterinarian in charge of the farm was checked
too.
•
•
•
•
•
1 Penicillin G-315.0 ppb- kidney-cow
•
consumption.
veterinarian.
Incomplete
documentation
of
the
administration of VMPs.
The farmer is a member of the Animal Health
Service of Lower Austria.
The veterinary practitioner`s dispensary of the
veterinarian in charge of the farm (member of
the Animal Health Service) was checked too.
Intensified supervision/checks of the farm and
the veterinarian have been planned for the
•
•
•
•
•
6
following
6 months.
Oral instruction of the farmer and the
veterinarian in charge.
•
1 Penicillin G-179.4 ppb- kidney-cow
•
veterinarian.
• The carcase was impounded at the
slaughterhouse and the offals were declared
• The withdrawal period has been observed
Intensified supervision/checks for the following
6 months.
It was not possible to identify the reason of this test
result.
1 Ampicillin-302.4 ppb- kidney-cow
•
Emergency
slaughter
outside
the
slaughterhouse.
consumption.
veterinarian.
Verification of the records.
Intensified
supervision/checks
for
the
following
6 months.
•
•
•
•
•
•
result.
1 Methylaminoantipyrin (Metamizole)515.00 ppb-muscle;
Methylaminoantipyrin-3,453.3 ppb and
Penicillin G-712.3 ppb–kidney-cow
•
consumption.
Intensified
supervision/checks
for
the
following
6 months.
•
•
•
result.
1 Methylaminoantipyrin (Metamizole)
-30,202.03 ppb-kidney-cow
•
•
Emergency slaughter.
The carcase was
7
impounded
at
the
consumption.
No documentation of the treatment by the
veterinarian in charge.
Intensified
supervision/checks
for
the
following
6 months.
Oral instructions.
•
•
•
•
1 Methylaminoantipyrin (Metamizole)
-186.5 ppb-kidney-cow
•
Emergency
slaughter
outside
the
slaughterhouse.
consumption.
Service of Lower Austria.
Incomplete
documentation
of
the
administration of VMPs.
The withdrawal period had not been observed.
against the farmer, the official veterinarian of
the slaughterhouse and the veterinarian in
charge of the farm.
•
•
•
•
•
•
5 WHO-PCDD/F-PCB-TEQ-4,50,
5.20, 8.79, 8.84 and 11.2 pg/g-muscleveal calves (4) and young bovine (1)
(suspect samples, slaughterhouse)
•
In 2008, an official veterinarian of Bavaria
informed that as a result of a routine control in
meat of a bovine animal originating from
Austria 17.7 pg/g fat dioxin-like PCBs had
been found.
Two farms were involved and investigated and
placed under official control by the Provincial
Governor (official veterinarian).
Both farms are small farms with a special form
of cattle breeding; the cows and their calves are
kept together in their natural environment
(organic animal husbandry). Most of the time
cows of both farms were pastured together. On
one of these pastures there is a feeding place
for wild game with six hay racks; They used
contaminated railway sleepers to build the hay
racks.
39 official samples were taken: 9 meat
samples, 13 milk samples, 5 samples of
feeding stuff, 4 soil samples, 2 samples of
wood (hay racks), one egg sample, 4 samples
•
•
•
8
of wild game meat and one sample of the paint
of the stable;
The contamination of the wood samples varied
between 11.19 and 29.68 ng WHO-PCDD/FPCB-TEQ/kg; one explanation for the higher
levels of dioxins and dioxin-like PCBs were
the contaminated wood of the hay racks;
particularly with regard to the fact that calves
like to nibble and suckle.
The carcases of 4 veal calves and one young
bovine were impounded at the slaughterhouse
and declared unfit for human consumption.
In both farms a lot of reconstruction (clean-up)
measures, especially the improvement of the
hay racks had been done.
Further investigations are still ongoing.
In three milk samples the maximum limits had
been exceeded and therefore the cows were
killed and sent to a processing plant according
to the requirements of Reg. (EC) No.
1774/2002. All batches of contaminated milk
were disposed as well.
•
•
3 WHO-PCDD/F-PCB-TEQ-6.51, 6.82
and 7.87 pg/g- cow milk (see also table
“Group B substances – Bovines”)
(suspect samples, farm)
1 Sulphamethoxazole-135.9 ppbmuscle- fattening pig
•
•
Pigs
On-farm mixer.
One follow-up sample of feed was taken and
showed a negative result.
Oral instructions.
•
•
•
•
1 Ochratoxin A-2.41 ppb-kidneyfattening pig
•
One official feed sample was taken which
showed a negative result.
•
It was not possible to identify the reason of this
test result.
1 Oxytetracycline-2,186.0 ppb and
Sulfadimidin-136.7 ppb musclefattening pig
•
Incomplete
documentation
of
the
administration of VMPs and withdrawal
periods.
consumption.
•
•
9
•
•
1 Nicarbazin-1.09 ppb-liver-broiler
1 Nicarbazin-1.94 ppb-liver-broiler
1 Semicarbacid-1.93 ppb – casings
(import, Pakistan)
1 Sulfadiazin-153.4 ppb-and
Methylaminoantipyrin (Metamizole) 261.9 muscle-other horse
1 cadmium-0.26 ppm-muscle- other
horse
Intensified
supervision/checks
for
the
following
6 months.
Oral
instructions
and
administrative
proceedings were started against the farmer.
Poultry
• One official sample was taken (on farm); the
analysis showed a negative result.
• Oral instructions
No indication of misuse of Nicarbazin.
• One official sample was taken (on farm); the
analysis showed a negative result.
• Oral instructions
No indication of misuse of Nicarbazin.
Sheep and goats
• Border rejection of 200 kg salted sheep
casings.
• Date of notification: 18/11/2009.
Horses
• The administration of Metamizole was not
documented!
• The equine identification document was
available and was rendered invalid at least by
stamping it ‘invalid’ on the first page.
• The owner stopped horse keeping.
•
10
The horse was 39 years old.
1 Penicillin G-57.3 µg/l – targeted
sample
•
•
•
•
Milk
The farm was investigated by the official
Service of Upper Austria.
One official milk sample (on-farm sampling)
showed a compliant result (suspect sample).
against the farmer.
It was not possible to identify the reason of this
test result.
3 WHO-PCDD/F-PCB-TEQ-6.51, 6.82
and 7.87 pg/g- cow milk
(suspect samples, farm)
1 Salinomycin-6.51 ppb
(targeted sample)
Please refer to “Group B substances – Bovines”
•
•
•
•
•
Eggs
Official detention of 300 eggs.
The eggs had been cracked and destroyed
according to the requirements of Regulation
(EC) No. 1774/2002.
The analytical result of one follow-up sample
was compliant.
A written warning was given to the farmer and
administrative proceedings were started.
result.
1 Malachite Green-Leuco-1.8 ppbmuscle-trout
(targeted sample)
Aquaculture
• The farm was investigated and has been placed
under official control (15/06/09–18/08/09) by
the Provincial Governor (official veterinarian)
in accordance with article 58 of the Food
Safety and Consumer Protection Act; about
1,000 trout were held on the farm as a
consequence of the positive finding.
• Verification of the records; most of
accompanying records, documentations and
other information were insufficient.
11
•
•
•
(suspect sample)
2 Malachite Green-1,235 and 356 ppb
and Malachite Green-Leuco-2,934 and
930 ppb-muscle-char
(targeted samples)
No verification of the illegal use of malachite green
• One follow-up sample of above mentioned
trout (LMG 1.8 ppb).
•
•
•
•
•
•
4 Malachite Green-76.0, 107.0, 134.0
and 182.0 Malachite Green-Leuco1.092, 943.0, 1,483.0 and 2.131.0 ppbmuscle-trout
(suspect samples)
1 Malachite Green-< 0.4 ppb
Malachite Green-Leuco11.1 ppb-muscle-char
(targeted sample)
Official samples were taken (6 samples); the
analyses of one sample showed a non
compliant result.
All fish ready for slaughter (310 kg) of the
“positive” ponds were killed and sent to a
processing plant of category 1 material as
required by Regulation (EC) No. 1774/2002.
Intensified checks for the following 12 months.
The farm was investigated and placed under
and Consumer Protection Act; In four ponds
trout and chars of different weight were held
on the farm as a consequence of the positive
finding.
Official samples were taken (11 samples); the
analyses of four samples showed again noncompliant results. (Please refer to information
below).
All fish (2,800 kg) were killed and sent to a
processing plant of category 1 material as
required by Regulation (EC) No. 1774/2002.
against the farmer.
The farmer lodged a complaint against persons
unknown. The farmer strongly denied the use of
malachite green.
• Four of eleven follow-up samples of above
mentioned chars (MG 1,235 ppb) showed noncompliant results (three of these samples were
taken from a pond which was located in
another area; these samples were negative).
•
12
The farm was placed under official control
(02./12/2009-05/01/2010) by the Provincial
Governor (official veterinarian) in accordance
with article 58 of the Food Safety and
Consumer Protection Act; about 100 chars
•
•
•
were held on the farm as a consequence of the
positive finding.
One official sample was taken and showed a
negative result.
Verification of the records;
No verification of the illegal use of malachite
green
1 Malachite Green-Leuco-1.3 ppbmuscle-carp
(targeted sample)
•
•
•
•
(suspect sample)
(targeted sample)
The farm (a small farm) was placed under
official control (16/10/2009-18/03/2010) in
and Consumer Protection Act.
One follow-up sample was taken; the amount
of Malachite Green-Leuco found was below
the reference point for action of 2.0 ppb (see
below).
Intensified checks for the next 12 months.
No verification of the illegal use of malachite green.
• One follow-up sample of above mentioned
carp (LMG 1.3 ppb).
•
•
•
The follow-up sample showed a negative
result.
The farm will be kept under official control.
No verification of the illegal use of malachite green.
(suspect sample)
•
•
7 Malachite Green-Leuco<2.2/2.2/2.5/2.6/4.3 and 6.7 ppbmuscle-carps
(suspect samples)
•
•
13
One follow-up sample was taken from the farm
which has been placed under official control by
the Provincial Governor since 2008 which has
been already reported last year.
against the farmer.
The farm was investigated in 2008 for the first
time.
Due to the positive test results parts of the farm
(4 ponds) had been placed under official
control on 21/08/2009 in accordance with
article 58 of the Food Safety and Consumer
Protection Act.
•
•
1 Malachite Green-1.2 and
Malachite Green-Leuco-18.8 ppbmuscle-carp
(suspect sample)
•
•
•
•
3 Malachite Green-<0.4/0.6 and 0.0
Malachite Green-Leuco-17.7/35.5 and
1.7 ppb-muscle-carps
•
•
•
The farmer purchased most of the
contaminated fish from the farm described
below (please refer to non compliant result MG
1.2 ppb and LMG 18.8 ppb).
Further investigations are still ongoing.
The farm was investigated and placed under
and Consumer Protection Act; in 28 ponds
about 5 tons of carp, chars and pike perches of
different weight were held in the farm as a
consequence of the positive finding.
Eight official samples were taken and four of
these samples showed a non-compliant result
(see information below).
All fish of three ponds were killed (650 kg)
and sent to a processing plant of category 1
material as required by Regulation (EC) No.
1774/2002.
Parts of the farm are still blocked.
Four follow-up samples of above mentioned
carp (MG 1.2 ppb and LMG 18.8 ppb) showed
a non-compliant result.
1 Malachite Green-<0.4 ppb and
Malachite Green-Leuco-35.3 ppbmuscle-pike perch
(suspect samples)
2 lead-0.74 and 1.08 ppm-muscle-deer
(targeted samples)
Wild game
• In wild game the detection of lead can be
traced back more or less to environmental
pollution and sometimes to bullets (to some
extent depending on the modern construction
of bullets and the type of bullets). The
contamination of the meat also depends on the
way the bullets penetrate the body of the
animals.
• During the next hunting season deer of the
hunting grounds will be sampled again.
14
BE
BELGIUM
Group A substances
-
substances
Increase of the number of analysis for A1/A3 and A4 made in fat and urine
instead of feces and muscle;
No more A2 analysis in poultry;
A5 analysis in milk;
Increase of the number of analysis for CAP, nitrofuranes and nitroimidazoles
in poultry.
1/ CAP-muscle-target sampleslaughterhouse-broiler
2/ CAP-muscle-target sampleslaughterhouse-broiler
3/ Prednisolone (>4 ppb)-feces-target
sample-slaughterhouse-pig
Follow-up actions
Investigation still ongoing.
4/ Dexamethasone ()-feces-target samplefarm-bovine
5/ Prednisolone ()-feces-target sample-farmcalf
Investigation on farm. Samples of
animal matrices, feed and material
were taken. Fattening animals were
put under temporary seizure. All
samples were compliant.
put under temporary seizure. Samples
of feces and material not compliant
(see 18 and 19).
6/ AMOZ-muscle-target sample-pigeonsslaughterhouse
Animals from the Netherland.
Products were recall.
7/ AOZ-muscle-target sampleslaughterhouse-broiler
Products still present at
slaughterhouse (16 460 kg) were put
under seizure.
Investigation on farm. Check of the
VMP register. Interview of the holder.
Carcass destroyed.
Carcass destroyed. See also Group B
results.
8/ Prednisolone-suspect sample-urineslaughterhouse-bovine
9/ Prednisolone-injection site-suspect
sample-slaughterhouse-bovine
15
11/ Dexamethasone (> 1.5 ppb)-injection
site-suspect sample-slaughterhouse-bovine
13/ Dexamethasone-injection site-suspect
sample-slaughterhouse-pig
14/ Dexamethasone-muscle-suspect sampleslaughterhouse-pig
17/ Dexamethasone-muscle-suspect sampleslaughterhouse-bovine
Carcass destroyed.
See also Group B results. Carcass
destroyed. Investigation on farm.
Samples of animal matrices, feed and
material were taken. Fattening animals
were put under temporary seizure.
One material sample non compliant
(see 20).
put under temporary seizure. All
Carcass destroyed. See also Group B
results.
Carcass destroyed.
Carcass destroyed.
The bovine farm was investigated due
to dexamethasone residues in feces
found on farm (see 4).
18/ Dexamethasone-suspect sample-feces bovine-farm
19/ Dexamethasone isonicotinoate-suspect
sample-material
20/ Dexamethasone-suspect sample-material
21/ Dexamethasone isonicotinoate,
progesterone-beta testosterone-suspect
samples-material
16
to dexamethasone residues in injection
site at slaughterhouse (see 11).
The bovine farm was investigated
following presence of low
concentration of propylthiouracil
found at slaughterhouse (see below
“results not considered as non
compliant”). Samples of animal
matrices, feed and material were
taken. Fattening animals were put
under temporary seizure.
22/ Prednisolone, prednisolone actetatesuspect sample-material
to prednisolone residues in suspect
sample at slaughterhouse. See below
“results not considered as non
compliant”.
Results from official samples taken during
monitoring/suspicion in farm or at
slaughterhouse level showing presence of
some A substances but which could not
been considered as non compliant.
Results from non-official samples.
In these cases, an investigation on
farm was performed, samples of
animals, feed and material are
taken and fattening animals are put
under temporary seizure until the
results.
Progesterone (3.5 ppb), testosterone (3.48
ppb)-muscle-slaughterhouse-target samplecalf
The farm of calves was investigated.
were put under temporary seizure. All
these samples were compliant.
Alpha boldenone and beta boldenone-fecesThe farm of calves was investigated.
slaughterhouse-target sample-calf
were put under temporary seizure. All
these samples were compliant.
Prednisolone (< 1 ppb)-urine-non official
sample-slaughterhouse-calf
Samples of animal matrices, material
and milk were taken. Fattening
animals were put under temporary
seizure. All these samples were
compliant.
Prednisolone (6 ppb)-urine-non official
sample -slaughterhouse-calf
and feed were taken. Fattening
compliant.
Cortisol-feces-suspect sampleThe bovine farm was investigated.
slaughterhouse-bovine
compliant.
Thiouracyl-suspect sample-slaughterhouseThe bovine farm was investigated.
bovine
compliant.
Prednisolone-suspect sample-slaughterhouse- The bovine farm was investigated.
17
bovine
Alpha boldenone (1.2 ppb), alpha
testosterone (8,6 ppb)-feces-target sampleslaughterhouse-bovine
Prednisolone-target sample-slaughterhousebovine
Dexamethasone-target sampleslaughterhouse-bovine
Alpha boldenone (182 ppb), alpha
testosterone (186 ppb)-feces-target sampleslaughterhouse-bovine
Delmadinone (2 ppb)-muscle-target sampleslaughterhouse-bovine
Propylthiouracyl-non official sample-bovine
Prednisolone (>4 ppb)-feces-target sampleslaughterhouse-bovine
Prednisolone-target sample-slaughterhousebovine
18
Samples of material and feed were
under temporary seizure. Samples
were also taken at slaughterhouse.
Samples of materials were found non
compliant. See 21 in Group A results
The bovine farm was investigated.
Samples of animal matrices and feed
put under temporary seizure. All these
Samples of feces and feed were taken.
Fattening animals were put under
temporary seizure. All these samples
were compliant.
compliant.
compliant.
compliant.
seizure. Samples of material were non
compliant (see 21 in Group A results).
compliant.
Samples of animal matrices were
under temporary seizure. All these
Delmadinone (2 ppb)-muscle-target sampleslaughterhouse-pig
Prednisolone-target sample-slaughterhousepig
The pig farm was investigated.
The pig farm was investigated.
Administrative measures
H status : for 52 weeks, animals from
the farm may only be sent to
slaughterhouse in Belgium where 10
% of them are analysed at the expense
of the farmer. In case of new
infringement during this period,
another period of 104 weeks is added
to the first one.
No H status were allocated in 2009.
Criminal penalties
In all cases of infringements relating
to group A substances (except A6), a
Pro Justitia is sent to prosecutor who
decides whether prosecution or not
(Law 15 July 1985 Hormones1 e.a.).
1
Loi du 15 Juillet 1985 relative à l’utilisation de substances à effet hormonal, à effet antihormonal, à effet beta-adrénergique ou à effet stimulateur de production chez les animaux.
Group B substances
-
Anticoccidials analyses added in milk;
Analysis for anthelmintics are planned depending of the grazing season;
Analysis for antibiotics, benzimodazoles and coccidiostatics planned in piglets;
Increase of the number of analysis for B2c and pesticides in pigs.
Oxytetracycline (235 ppb)-muscletarget sample-slaughterhouse-calve
Follow-up actions
Bovines
Investigation on farm. Check of the VMP register.
Interview of the holder. Interview of the veterinarian.
Dioxin (22 pg TEQ/g fat) and sum
dioxin and dioxin-like PCB (43 pg
TEQ/g fat)-fat-target sample-bovine-
Products still at slaughterhouse (10 kg) destroyed.
The farm was blocked. Investigation on the source of
contamination. Samples of feed and of 2 bovines
19
slaughterhouse
Sulfadiazine (>200 ppb)-kidneytarget sample-slaughterhouse-bovine
Sulfadiazine (>200 ppb)-muscletarget sample-slaughterhouse-bovine
Sulfadimidine (>200 ppb)-muscletarget sample-slaughterhouse-bovine
Sulfadimethoxine- kidney (>200
ppb))-target sample-slaughterhousecalve
Sulfadimethoxine- muscle (>200
ppb)-target sample-slaughterhousecalve
Sulfadimethoxine- kidney (>200
Sulfadimethoxine- muscle (>200
Sulfadimethoxine (170 ppb)-kidneytarget samplecalf-slaughterhouse
Dihydrostreptomycine (2880 ppb)injection site-suspect sampleslaughterhouse-bovine
Flunixine (873 ppb)-injection sitebovine- suspect sampleslaughterhouse
Flunixine (2094 ppb) + tolfenamic
acid (773 ppb)-injection sitesuspect
sample-bovine-slaughterhouse
negative, release of the farm.
Interview of the holder. Allocation R-status. Carcass
destroyed.
Sulfadoxine (229 ppb)-injection sitesuspect sample-bovineslaughterhouse
Sulfadoxine (199 ppb)- musclesuspect sample-bovineslaughterhouse
Tilmicosine (1390 ppb)-injection sitebovine- suspect sampleslaughterhouse
Interview of the holder. Carcass destroyed.
Flunixine (2300 ppb)-muscle-suspect
Interview of the holder. Allocation R-Status. Carcass
destroyed.
Phenylbutazone (2350 ppb)-injection
site-bovine- suspect sampleslaughterhouse
Phenylbutazone (1850 ppb)-musclebovine-slaughterhouse
Carcass destroyed.
Official report against the veterinarian. Carcass
destroyed.
Allocation R-Status. Carcass destroyed.
20
Tylosine (5185 ppb)-injection sitesuspect sample-bovineslaughterhouse
Tolfenamic acid (275 ppb)- injection
sitesuspect sample-bovineslaughterhouse
Sulfadimethoxine (15500 ppb)injection sitesuspect sample-bovineslaughterhouse
Sulfadimethoxine (300 ppb)-musclesuspect sample-bovineslaughterhouse
Tolfenamic acid (1311 ppb)-injection
Benzylpenicilline (3500 ppb) +
sulfadimethoxine (3400 ppb)injection sitesuspect sample-bovineslaughterhouse
Benzylpenicilline (1500000 ppb)injection sitesuspect sample-bovineslaughterhouse
Benzylpenicilline (500 ppb)-musclesuspect sample-bovineslaughterhouse
Caprofen (2345 ppb)-injection sitesuspect sample-bovineslaughterhouse
Tylosine (1400 ppb)-injection sitesuspect sample- bovineslaughterhouse
Flunixine (950 ppb) + spiramycine
(16000 ppb)-injection sitesuspect
Interview of the holder. Interview of the dealer.
Carcass destroyed. Allocation R-status. Official
report against the dealer.
Tetracycline sum (3000 ppb) +
oxytetracycline sum (57000 ppb)injection sitesuspect sample-bovineslaughterhouse
See (11) in Group A Results.
Tilmicosine (107 ppb)-injection site-
Animal from the Luxembourg.
Interview of the holder. Official report against the
holder. Carcass destroyed.
Carcass destroyed. Allocation R-status.
21
suspect sample-bovineslaughterhouse
Allocation R-status.
Flunixine (> 750 ppb)-injection sitesuspect sample-bovineslaughterhouse
Flunixine (200 ppb)-musclesuspect
Flunixine (49 ppb) +
Sulfadimethoxine (250 ppb)-musclebovine- suspect sampleslaughterhouse
Tolfenamic acid (168.08 ppb)injection site-bovine- suspect sampleslaughterhouse
Allocation R-status. Official report.
Flunixine (437 ppb)-injection sitesuspect sample-bovineslaughterhouse
Sulfadimethoxine (329 ppb)-musclesuspect sample-bovineslaughterhouse
Benzylpenicilline ( 63000 ppb) +
dihydrostreptomycine (4447 ppb) +
streptomycine (572 ppb)-injection
site-bovine-slaughterhouse
Ampicilline (3000 ppb)-injection sitesuspect sample-bovineslaughterhouse
dihydrostreptomycine (1739 ppb)injection sitesuspect sample-bovineslaughterhouse
sites- suspect sample-bovine-suspect
samples-slaughterhouse
sites- suspect sample-bovine-suspect
samples-slaughterhouse
Interview of the holder. Interview of the
veterinarian. Official report against the veterinarian.
Carcass destroyed.
Interview of the holder. Allocation R-status. Carcass
destroyed.
22
Oxytetracycline sum (5000 ppb) +
oxytetracycline sum (100000 ppb) +
marbofloxacine (725 ppb)-injection
Benzylpenicilline (675 ppb) +
Meloxicam (830 ppb) + sulfadoxine
Sulfadoxine (180 ppb)-muscle suspect sample-bovineslaughterhouse
Enrofloxacine + ciprofloxacine
oxytetracycline sum (800 ppb)injection sitesuspect sample-bovineslaughterhouse
Tetracycline sum (183 ppb)-injection
Oxytetracycline sum (176 ppb) +
tilmicosine (3600 ppb)-injection sitesuspect sample-bovineslaughterhouse
Tilmicosine (76 ppb)-muscle suspect sample-bovineslaughterhouse
Ceftiofur (> 5000 ppb)-injection sitesuspect sample-bovineslaughterhouse
Tylosine (588 ppb) + Tilmicosine
Allocation R-Status. Carcass destroyed.
Interview of the veterinarian. Carcass destroyed.
Official report against the veterinarian. Carcass
destroyed.
Allocation R-status. Carcass destroyed. Official
23
Benzylpenicilline (737 ppb)-injection
Tilmicosine (5013 ppb)-injection sitesuspect sample-bovineslaughterhouse
Tilmicosine (786 ppb)-musclesuspect sample-bovineslaughterhouse
Enrofloxacine + ciprofloxacine
Dihydrostreptomycine (4442 ppb) +
benzylpenicilline (30561 ppb)injection sitesuspect sample-bovineslaughterhouse
Benzylpenicilline (352 ppb)-musclesuspect sample-bovineslaughterhouse
Sulfadimethoxine (2400 ppb)injection sitesuspect sample-bovineslaughterhouse
Oxytetracycline sum (1091 ppb)injection sitesuspect sample-bovineslaughterhouse
Enrofoxacine + ciprofloxacine (204
ppb)-injection sitesuspect samplebovine-slaughterhouse
Tilmicosine (250 ppb)-muscle-
report against the veterinarian.
Carcass destroyed.
24
suspect sample-bovineslaughterhouse
Flufenamic acid ()-muscle-target
sample-slaughterhouse
Marbofloxacine (> 200 ppb)-kidneytarget sample-slaughterhouse
Pigs
Interview of the holder.
Interview of the holder. Allocation R-Status.
Sulfadiazine (120 ppb)-kidney-target
Sulfadiazine (203 ppb)-kidney-target
Sulfadimethoxine (>200 ppb)-kidneytarget sample-slaughterhouse
Sulfadimethoxine (>200 ppb)muscle-target sample-slaughterhouse
Sulfadimethoxine (>200 ppb)-kidneytarget sample-slaughterhouse
Sulfadimethoxine (>200 ppb)muscle-target sample-slaughterhouse
Ampicilline (5519 ppb)-injection sitesuspect sample-slaughterhouse
4-Methylaminoantipyrin (884 ppb) +
tetracycline sum (7372 ppb) +
oxytetracycline sum (220000 ppb)injection site-suspect sampleslaughterhouse
4-Methylaminoantipyrin (174 ppb) +
oxytetracycline sum (1049 ppb)muscle-suspect sampleslaughterhouse
Doxycycline (345 ppb) + sulfadiazine
sample-pig-slaughterhouse
Doxycycline (545 ppb) + sulfadiazine
sample-pig-slaughterhouse
Ampicilline (95000ppb)-injection
sitesuspect sample-pigslaughterhouse
Nicarbazine (387 ppb)-musclebroiler-target sample-slaughterhouse
Doxycycline (229 ppb)-muscle-
Animal from the Netherland.
Poultry
25
broiler-target sample-slaughterhouse
Doxycycline (179 ppb)-musclebroiler-target sample-slaughterhouse
Monensin (17,3 ppb) -muscle-broilertarget sample-slaughterhouse
Ketoprofen (44 ppb)-muscle-broilertarget sample-slaughterhouse
Ketoprofen (13 ppb)-muscle-broilertarget sample-slaughterhouse
Nicarbazine (48.7 ppb)-musclebroiler-target sample- slaughterhouse
Nicarbazine (77.8 ppb)-musclebroiler-target sample- slaughterhouse
Enrofloxacine + ciprofloxacine (460
ppb)-injection sitesuspect samplepig-slaughterhouse
Enrofloxacine + ciprofloxacine (353
ppb)-musclesuspect sample-pigslaughterhouse
sitesuspect sample-pigslaughterhouse
Animals from the Netherlands.
Products still at slaughterhouse (200 kg) were
destroyed. Investigation on farm. Check of the VMP
register. Interview of the holder. Interview of the
veterinarian.
Products still at slaughterhouse (50 kg) were
destroyed.
Animals from the Netherlands.
Interview of the holder. Allocation R-Status. Carcass
destroyed.
Sheep and goat
No non-compliant results
Horses
Moxidectine (5 ppb) – equine milk –
target sample
Flunixine – ewe milk – target sample
Milk
Investigation on farm.
Investigation on farm.
Eggs
Rabbit
26
Ketoprofen-muscle-target sampleslaughterhouse
Aquaculture
Farmed game
No non-compliant results.
Wild game
No non-compliant result
Honey
Administrative measures
R status : R-status: for a 8 weeks period the
identification document of the animals of the same
species (bovine, pigs) from the herd are marked with
a R symbol. In the slaughterhouse, 10 % of these
animals are sampled. In case of new infringements
during this period, the period will be extended by 26
weeks. The analysis are at the expense of the
responsible of the herd.
R-status were allocated to bovine farms : 16
R-status were allocated to pig farms : 5
Official reports sent to the legal service for the
attribution of administrative penalty : 19. Fines paid :
5. In 6 cases, the report was sent to the prosecutor
for follow-up. In 3 cases prosecution was given up.
27
BG
BULGARIA
ANALYSIS OF THE RESULTS FROM THE NATIONAL MONITORING
PROGRAMME FOR CONTROL ON RESIDUES (NMPCR) FOR THE YEAR 2009
IN BULGARIA
No presence of any residues from veterinary medicinal products and environmental
contaminants above MRL or from illegal use of forbidden substances has been ever
detected for the year 2009.
28
CY
•
•
•
•
•
•
CYPRUS
Sampling should take place over the entire year (January to December);
The tender of Veterinary Services of Cyprus for the interest of accredited
laboratories to carry out the laboratory examinations of substances of animal
tissues and food of animal origin that are included in the National Residues Plan
concerning the year 2011 must be published in the European gazette early in July
2010;
Horsemeat. There is not slaughterhouse for horses. Horsemeat is not used for
human consumption in Cyprus. Horses exported from Cyprus accompanied by a
Passport (Commission Decision 2000/68/EC) is implemented on the basis of
“Genetic improvement of Animals” Law 86 (I) 2001, Κ.∆.Π. 522/2005, Αρ. 4051,
18.11.2005 in which mentioned all the drugs used for this horse and the withdrawal
period;
The number of Horses (Animals) 5700 which included in the plate of
PRODUCTION by SPECIES of the DATABASE are the total live horses population
of Cyprus NOT SLAUGTERED ANIMALS
Efforts are in progress to arrange NRP tests to be carried out in foreign accredited
laboratories in order to cover all the numbers on all substances provided in the
programme for the year 2010;
WE CONFIRM that all methods used by the foreign laboratories to carry out
analysis were validated and accredited. This is a basic term included in the Tender.
During the evaluation of laboratories responded to the Tender, the evaluation
committee checked first if the method used by the laboratory is validated and
accredited and for which matrix and if this method is included in the list of the
accreditation body;
DETAILS OF NON-COMPLIANT RESULTS – TARGETED SAMPLING
MEMBER STATE: CYPRUS
GROUP SUBSTANCE
RESIDUE
YEAR: 2009
ANIMAL
CATEGORY/
SPECIES
A1
A2
A3
A4
A5
FARM/
SLAUGHTERHOUSE/
OTHERS
NONCOMPLIANT
0
0
0
0
0
0
A6
29
B1
Antibiotics,
Cows
chemotherapeu milk
tics / Inhibitors
Antibiotics,
Sheep and
chemotherapeu
Goats milk
tics/ Inhibitors
Antibiotics,
chemotherapeu
tics
Oxytetracyclin
e
Amoxycillin
Sulfadimidine
Oxytetracyclin
e/Tetracycline
Farm
Farm
Bovines
Bovines
26
Slaughterhouse
Slaughterhouse
Porcine
Porcine
8
1
1
Slaughterhouse
Slaughterhouse
1
1
Slaughterhouse
2
Rabbits
Slaughterhouse
7
Sheep and
goats
Slaugterhouse
1
Sheep and
goats
Oxytetracyclin
e/Tetracycline
B2a
B2b
B2c
B2d
B2e
Diclazuril
Diclofenac
B3a
B3b
B3c
B3d
B3e
48
SUM
Bovine
Muscles
Porcine
Muscles
2
2
30
Sheep and goats
Muscle
3
Milk
Cows milk
8
Sheep and goats milk 26
Rabbits
Liver
7
Total number of non compliant samples 48
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
NONE
Follow-up actions
•
Information to be included for each non-compliant result. In case of several noncompliant results for the same substance in the same holding or related holdings, data
could be aggregated. Data on concentration and matrix is very useful to be used as
background information for the monitoring of the prevalence of use of group A
substances.
Group B substances
Modification of national residue Aggregate for all animal products and substances
plan
NON-COMPLIANT RESULTS
B 1. Antibiotics /
Chemotherapeutics
Follow-up actions
Bovines
B1. Antibiotics / Chemotherapeutics
Bovine/ Bovine farms (Two
farms)
31
1.Discarded cow
Amoxycillin
Bovine/ Discarded cow (CYB
4202009) – (One bovine farm)
LCMSMS- Amoxycillin 1199 µg/kg
muscle
1. Pastou Bros, (CYB 101058714) AthienouNicosia
•
Investigation in the farm of origin √
•
Verification of records √
•
Additional sampling √
•
Animals held in the farm (Bovines 528)
•
Intensified checks on the animals and
products from the farm / establishment in
the event of repeated infringements √
•
Carcasses and products declare unfit for
human consumption (1carcass / 258 kg)
•
Administrative measures (NONE)
•
Others
(Mrl in muscle 50 µg/kg)
2. Discarded cow
Oxytetracycline
Bovine/ Discarded cow (CYB
1108009) – (One bovine farm)
LCMSMS / HPLC-DPA
Oxytetracycline 963 µg/kg
muscle
1. Dimitris and Andreas Petrou, (CYB
101287442) Lympia- Nicosia
•
•
•
•
Animals held in the farm (Bovines 281)
•
•
human consumption (1 carcass / 252 kg)
•
•
Others
32
B1.Antibiotics /
Chemotherapeutics
Pigs
B1. Antibiotics / Chemotherapeutics
Porcine/ Fattening pigs (Two
porcine farm)
1. Oxytetracycline
Porcine/ Fattening pigs – (One 1. Pantelis Vassou Ltd, (CY 117) Marki-Nicosia
porcine farm)
• Investigation in the farm of origin √
LCMSMS / HPLC-DPA • Verification of records √
muscle
• Additional sampling √
• Animals held in the farm (1717 Fattening
pigs / 417 sows)
•
•
human consumption (NONE)
•
•
Others
2. Sulphonamides
Porcine/ Fattening pigs – (One
porcine farm)
1. Chr. Nicodemou and others Ltd
2.1. Sulphadimidine
(CY 145) –Kato Moni-Nicosia
LCMSMS, Sulphadimidine
1426 µg/kg –porcine muscle
•
•
•
•
Animals held in the farm (16000 fattening
pigs/ 1052 sows)
33
•
•
•
•
Others
Poultry
Sheep and goat
B1.Antibiotics /
Chemotherapeutics
Sheep and Goats (One farm- 2
cases)
Chlortetracycline
1. Demetris Varnavas- (CYS 4012103)
Dromolaxia-Larnaca
LCMSMS / HPLC-DPA
Mrls: Muscle- 100 µg/kg
Animals held in the farm (2508)
Intensified checks on the animals and products
from the farm / establishment in the event
of repeated infringements √
Carcasses and products declare unfit for human
consumption (2 carcasses/ 52 kg)
Others
34
B2e NSAIDs
Sheep and Goats (One farm)
1. Loucas Philippou and sons Farm Ltd(CYS 5021014) – Kato Polemidia-Lemesos
LCMSMS Diclofenac 12 µg/kg
(Sheep muscle)
No Mrls 2010.
Additional sampling
of repeated infringements
consumption (NONE)
Others
Horses
None
None
Milk
B1.
Antibiotics/Chemotherapeutics
Antibiotics (Delvo SP test)
Dairy cows farms (8 cases)
1. Farmes Sanx Ltd-(CYB 4110003) –Kiti Larnaka
consumption (6793lt)
35
Administrative measures √
Others
2. Kypros Hadjistasou (CYB 112006) –Potamia,
Nicosia
•
•
•
•
•
•
human consumption (11161.3 litre milk)
•
•
Others
3. Lambros Hadjigiorgallis- (CYB 1107016) –
Dali - Nicosia
•
•
•
•
•
•
human consumption (2000lt)
•
•
Others
36
4. G & D Farm Ltd – (CYB 4202018) –
Athienou - Larnaka
•
•
•
•
•
•
human consumption (7623.1 litre milk)
•
•
Others
5. Victoria & Giannakis Charalambous -(CYB
1225006) –Tseri-Nicosia
•
•
•
•
•
•
human consumption (11859 litre milk)
•
•
Others
6. Νeka Farm (CYB 5210001) –Kolossi –
37
Limassol
consumption (None)
Others
7. Christodoulos Theodorou
1107018) –Dali - Nicosia
–
(CYB
consumption (None)
Others
8. Makromallis Farm- (CYB 3111004)Dasaki Achnas - Ammochostos
38
Animals held in the farm (170 )
Sheep and Goats farm 26 (26
cases)
consumption (3000 litre milk)
Others
1. Dimitris Afxentiou-(CYS 3110023) –Dasaki
Achnas, Ammochostos
consumption (None)
Others
2. Stelios Giorgallou-(CYS 3111039) –Dasaki
Achnas - Ammochostos
•
39
•
•
•
Animals held in the farm (457 sheep-117
goats)
•
•
human consumption (None)
•
•
Others
3. Georgios M. Savva-(CYS 4106010) –Ormideia
- Ammochostos
•
•
•
•
•
•
•
•
Others
4. Loukas & Petros Adamou-(CYS 4106042) –
Ormideia - Ammochostos
•
40
•
•
•
Animals held in the farm (30 goats- 483
sheep)
•
•
•
Administrative measures (√)
•
Others
5. Pavlos Adamou -(CYS 4106086) –OrmideiaAmmochostos
•
•
•
•
Animals held in the farm (93 goats and 636
sheep)
•
•
•
•
Others
6. Isidoros Savva Posios-(CYS 4106026)
•
41
•
•
•
Animals held in the farm (142 sheep)
•
•
•
•
Others
7. Petros Koulendrou - (CYS 4106057) –
Ormideia- Ammochostos
•
•
•
•
•
•
•
•
Others
8. Panagiotis Christodoulou-(CYS 4106051)Ormideia - Ammochostos
•
•
42
•
•
sheep)
•
•
•
•
Others
9. Ioannis Prodromou-(CYS 4106027)-Ormideia Ammochostos
sheep)
consumption (None)
Administrative measures (None)
Others
10. Andreas Evgeniou - (CYS 4106098) –
•
•
43
•
•
Animals held in the farm (136 goats)
•
•
•
•
Others
11. Paraskevas Fesas-(CYS 3110068) –Avgorou Ammochostos
sheep)
consumption (None)
Others
12. Kostas Hadjiilia-(CYS 1241022) –
Paliometocho - Nicosia
44
sheep)
consumption (160litre milk)
Others
13. Kostas Petrou-(CYS 4217004) – Lympia Nicosia
Others
14. Kostis Hadjistavri -(CYS 1108018) – Lympia
- Nicosia
45
sheep)
Others
15. Georgios Georgiou-(CYS 1207004) –Kalo
Chorio Oreinis - Nicosia
Animals held in the farm (329 goats)
Others
16. Savvas Pieri-(CYS 3111041)-Dasaki Achnas –
Ammochostos
46
sheep)
consumption (None)
Others
17. Christofis Symeou-(CYS 3111045) –
Vrysoulles – Ammochostos
consumption (None)
Others
18. Christos Iona-(CYS 4124022) –Kivisili Larnaka
47
sheep)
Others
19. Neofytos Makri - (CYS 4210071) –Kalo
Chorio - Larnaka
sheep)
Others
20. Ttooulou Bros - (CYS 4202033) – Athienou Larnaka
48
sheep)
Others
21. Meliton Farm - (CYS 5222006) –Avdimou Limassol
sheep)
Others
22. Anthemis Kosti - (CYS 3110016) –Avgorou Ammochostos
49
sheep)
Others
23. Stelios Giorgallou - (CYS 3111039) – Dasaki
Achnas - Ammochostos
sheep)
Others
24. Neofytos Groutidis - (CYS 1226007) –Politiko
- Lefkosia
•
•
50
•
•
sheep)
•
•
•
•
Others
25. Anastasis Karoullas - (CYS 3114033) –
Vrysoulles - Ammochostos
•
•
•
•
sheep)
•
•
•
•
Others
26. Andreas Savvidis - (CYS 4309111) – Kofinou
- Larnaka
•
•
51
•
•
sheep)
•
•
•
•
Others
Eggs
None
None
Rabbit
B2b Coccidiostats (Five rabbit
farms-Seven cases)
1. Diclazuril (Five rabbit farms)
1.1. LCMSMS- Diclazuril 612
µg/kg (Rabbit liver)
1. Sotiris Ioannou –Polemidia -Lemesos
•
•
•
•
Animals held in the farm (Females and
males parents 800/fattening 1000)
•
•
52
Diclazuril 223 µg/kg
(Rabbit liver) Diclazuril
242 µg/kg (Rabbit liver)
•
•
Others
2. Miltos Xadjimiltis –Mathicoloni -Lemesos
•
•
•
•
•
•
•
•
Others
3. Georgios Hadjizacharias – Augorou Ammochostos
•
•
•
•
•
•
53
•
•
Others
4. L.G.L. Rabbit Farm Ltd –Ergates -Nicosia
•
•
•
•
•
•
•
•
Others
1. Maria Kostantinou –-Marathounta-Paphos
•
•
•
•
•
•
•
•
Others
54
Eggs
None
None
Aquaculture
None
None
Farmed game
None
None
Wild game
None
None
Honey
None
None
IMPORTS
NON-COMPLIANT RESULTS
None
Follow-up actions
None
55
CZ
CZECH REPUBLIC
Group A substances
Follow-up actions
Not found
* Information to be included for each non-compliant result. In case of several non-compliant
results for the same substance in the same holding or related holdings, data could be
aggregated. Data on concentration and matrix is very useful to be used as background
information for the monitoring of the prevalence of use of group A substances.
Group B substances
plan
State Veterinary Administration (SVA) will carry out in cooperation with ISCVBM the
study focused on residues of antibiotics (beta-lactams) in sows (muscle, liver, kidney).
SVA will carry out in cooperation with CISTA the study focused on reason of high content
of cadmium in kidney of bovine animals in some localities (soil – plant – cow).
Follow-up actions
Bovines
B1: Neomycin cow/liver: 1740 ppb Action: investigation was conducted on the farm; the
treatment was not mentioned in FCI. Last treatment
was 9.12.2009 (Mastijet forte intra uberis, Alamycin
i.m.), cow was slaughtered 21.1.2010. Extraordinary
veterinary measures were imposed; additional
samples from other cows were taken: 5x livers (3x
NC neomycin, 1x NCDHSTM, 1x compliant), 2x
B1: Neomycin cow/muscle: 866
kidneys (1x NC DHSTM, 1x compliant).
ppb, liver: 723 ppb
Withdrawal period was not kept. There were
confiscated livers and kidneys from all cows which
B1: Tulathromycin calf/muscle:
were treated by neomycin and DHSTM during last
1122 ppb, liver: 11431 ppb
100 days before slaughter. Frequency of official
controls was increased on the farm.
B3c: Cadmium (Cd) 8x kidney
(cows) on 8 different farms: 2,22
ppm, 2,22 ppm, 2,2 ppm, 2,13 ppm,
1,97 ppm, 1,73 ppm, 1,48 ppm, 1,2
ppm.
Action: all tissues was confiscated (whole body: byproduct category 2 according to regulation (EC)
1774/2002). Investigation on the farm and at the
private veterinarian was conducted. Withdrawal
period was not kept.
Action: investigation on the farm and at the private
veterinarian was conducted. Withdrawal period was
kept for last application of PNC (which has been
written on list of treatment - 21 days) but it was used
56
Draxxin (tulathromycin - 49 days of WP).
Treatment was not mentioned in FCI.
B1: Sulfadiazin fattening
pig/muscle: 146 ppb, kidney: 246
ppb
B2b: Nicarbazin chicken/liver:
620,5 ppb, 350,0 ppb
Actions: investigations on the farms were conducted;
follow-up testing of feed and additional testing of
kidneys (in total 37 samples) were carried out on the
farms concerned. Non-compliant findings occurred
mostly in the older cows. Total condemnation of
cows´ kidneys above defined age was ordered on 5
farms.
Pigs
Action: investigation on the farm was conducted.
Withdrawal period was not kept. Treatment was not
mentioned in FCI. Additional samples from 2 pigs
(muscle, liver, kidney) was examined – compliant.
Poultry
Action: two farms - residues of nicarbazin were
detected in amount above the action limit which was
recommended for chicken liver by the Codex
Alimentarius - 200 ppb in liver. Investigation on the
farms was conducted; extraordinary veterinary
measures were imposed. Additional samples of livers
and feed were taken (other batches) - all samples on
two farms were compliant.
Sheep and goat
B3c: Cadmium (Cd) horse/liver:
2,78 ppm, kidney - 57,2 ppm
Horses
The horse was 20 years old.
Milk
B2b: Nicarbazin hen eggs: 916
ppb + narazin 6,5 ppb
B2b: Robenidin quail eggs: 63,2
ppb
Eggs
Action: investigation on the farm was conducted;
extraordinary veterinary measures were imposed;
additional samples of eggs (14x) and feed (3x) and
egg products (10x) were taken for further testing –
eggs with NC samples (two hens hall) and all noncompliant egg products (melange) were confiscated.
Probably it was cross contamination of feed; the
producers of feeding mixtures have been warned.
probably cause was cross-contamination of feed
mixture; extraordinary veterinary measures were
imposed, expedition of eggs was block; additional
samples (eggs and feed) were analysed – all
compliant.
57
B2b: Salinomycin rabbit/liver:
15,56 ppb
B3e: Sum of Malachite and Leucomalachite green (MG/LMG): 2x
(trout) from 2 sites were above the
MRPL (LMG: 5,33 ppb and 3,71
ppb) and 1 sample (carp) was
above MRPL (2,2 ppb); samples
from 5 fish farms were bellow the
MRPL.
Rabbit
extraordinary veterinary measures were imposed,
expedition of liver was block, additional samples
(other batch) of liver and feed were taken – all
compliant.
Aquaculture
Actions: investigations on the fish farms were
conducted; extraordinary veterinary measures were
imposed, prohibiting of sale (the non-compliant
batches) until the results are compliant.
Farmed game
B3c: Lead (Pb) roe-deer/muscle:
48,0 ppm and Mercury (Hg) 0,0623
ppm
Lead (Pb) above action level
0,3 ppm: phasant (2x), wild duck
(4x), roe-deer (2x), wild boar (1x)
Wild game
Actions: additional samples (muscle, liver, kidney)
were taken from two other roe-deer: compliant
(action levels: Pb - 0,3 ppm, Hg - 0,5 ppm)
Most likely contamination by bullet.
Honey
58
DE
GERMANY
plan
Group A substances
Group A substances
A5 = Beta antagonists
Aquacultures
On the occasion of an FVO inspection mission in 2009, the Commission recommended to
analyse aquacultures for ß antagonists, citing the minutes of a meeting in 2000 of the
Commission’s working group on residue control plans. Yet, the minutes do not contain such a
recommendation. As use of ß antagonists in aquacultures is questionable anyhow, we did not
follow the Commission recommendation. According to the National Reference Laboratory,
there is no new knowledge as regards the question whether it would make sense to include ß
antagonists in NRCP testing. The NRL therefore did not recommend including this aspect in the
NRCP, which is herewith brought to the Commission’s attention.
A6 = Dapsone
Bovines
Germany has so far declined to include dapsone in the NRCP because there is no need to use
the product as there have been no cases of granular dermatitis in cattle in Germany. The BVL
database shows negative findings in 415 samples from 2007 to 2009, four of them stemming
from other Member Sates. Dapsone was therefore considered only with a small sample number
in the 2010 NRCP.
A6 = Nitrofurans
Bovines, ovines/caprines, farmed game, horses, and rabbits
Oral administration of nitrofurans and nitroimidazoles seems little likely, but cannot be
excluded in general, at least not for nitroimidazoles. The 2010 plan therefore provides for a few
samples in cattle, sheep/goat, horses, farmed game, and rabbits to be analysed for nitrofurans
and nitroimidazoles.
A6 = Nitroimidazoles
Milk
The 2010 NRCP provides for testing milk for nitroimidazoles.
A6 = Chloramphenicol
Poultry
Positive findings here have been attributed to hygienic problems in sample taking. Therefore, it
does not seem necessary to enhance the sample number. The recommendation is to train sample
taking personnel in this respect.
59
1 Taleranol (beta-zearalanol);
fattening cattle; urine; 2.01 µg/kg
Follow-up actions
Contents of alpha and beta zearalenol and of zearalenone
indicate that mycotoxins are a likely cause of findings.
On-site investigation at the farm of origin; examination
of the records.
1 Taleranol (beta-zearalanol); cows; Contents of alpha and beta zearalenol and of zearalenone
urine; 2.58 µg/kg
indicate that mycotoxins are a likely cause of findings.
On-site investigation at the farm of origin; examination
of the records. Control report pursuant to Art. 9 letter e
of Regulation (EC) No. 796/2004 (Withdrawal of the
possibility of receiving or requesting EU subsidies).
1 alpha-boldenone; cows; urine; 0.6 The sample did not give rise to official complaint
µg/kg
because the level of alpha-boldenone found is
physiologically attributable to the animal’s pregnancy.
Illegal treatment is only indicated by beta-boldenone
conjugates.
1 alpha-boldenone; heifers; u.rine;
The sample did not give rise to official complaint
0.34 µg/kg
conjugates.
1 alpha-boldenone; heifers; urine;
0.34 µg/kg
conjugates.
0.36 µg/kg
conjugates.
1 alpha-boldenone; fattening calves; The sample did not give rise to official complaint
Urine; 0.36 µg/kg
because only alpha-boldenone conjugates were found,
while illegal treatment is only indicated by betaboldenone conjugates.
1 alpha-boldenone; fattening cattle; The sample did not give rise to official complaint
urine; 0.41 µg/kg
1 alpha-boldenone; cows; urine;
0.41 µg/kg
conjugates.
urine; 0.42 µg/kg
60
1 alpha-boldenone; fattening cattle;
urine; 0.43 µg/kg
1 17-alpha-19-nortestosterone;
heifers; urine; 0.44 µg/kg
0.46 µg/kg
urine; 0.49 µg/kg
0.54 µg/kg
urine; 0.55 µg/kg
0.59 µg/kg
1 17-alpha-19-Nortestosterone;
1 17-alpha-19-Nortestosterone;
cows; urine; 0.61 µg/kg
0.63 µg/kg
0.68 µg/kg
1 beta-boldenone, 1dehydrotestosteron; fattening pigs;
urine; 0.73 µg/kg
Probably endogenous. Therefore no further measures.
conjugates.
conjugates.
because the level of alpha-nortestosterone found is
physiologically attributable to the animal’s pregnancy
(calved 02 Nov 2009).
conjugates.
The sample did not give rise to official complaint,
because beta-boldenone naturally occurs in adult male
pigs.
61
physiologically attributable to the animal’s pregnancy..
0.86 µg/kg
urine; 0.98 µg/kg
1.02 µg/kg
1 17-alpha-19-nrtestosterone; cows; Probably endogenous. Therefore no further measures.
urine; 1.2 µg/kg
urine; 1.22 µg/kg
urine; 1.25 µg/kg
while illegal treatment is only indicated by betaboldenone conjugates, according to current state of
knowledge.
1 17-alpha-19-nortestosteron;
cows; urine; 1,5 µg/kg
1.51 µg/kg
conjugates.
urine; 1.66 µg/kg
1 17-beta-19-nortestosterone;
fattening pigs; urine; 1.8 µg/kg
62
fattening calves; Urine; 2.15 µg/kg
1 alpha-boldenone; fattening calves;
urine; 6.43 µg/kg
fattening pigs; urine; 8 µg/kg
cows; urine; 18,1 µg/kg
fattening pigs; urine; 592 µg/kg
1 chloramphenicol; turkey hens;
drinking water; 0.18 µg/kg
1 chloramphenicol; fattening pigs;
muscle; 0.3 µg/kg
Exceeding CC alpha, but below MRPL; therefore not
subject to complaint.
On-site investigation at the farm of origin, examination
of the records, 16 additional sampling, ban on transport
and delivery of livestock (634 animals), increased
controls in the establishment of origin (16)
1 semicarbazide (SEM); fattening
pigs, muscle; 1.53 µg/kg
of the records, ban on transport and delivery of livestock,
Control report pursuant to Art. 9 letter e of Regulation
(EC) No. 796/2004 (Withdrawal of the possibility of
receiving or requesting EU subsidies).
1 metronidazole; fattening pigs,
muscle; 18.44 µg/kg
of the records, 5 additional samplings.
aggregated. Data on concentration and matrix is very useful to be used as backgroand
63
plan
Group B substances
B1 = Amino glycosides
Bovine
Amino glycosides were included new in the 2009 plan, with a relatively low number of
samples. Because of positive findings in 2009, sample numbers in cattle and fattening calves
have been increased by 1/3 (one third) in the 2010 plan.
B1 = Sulfonamides
Pigs
After one finding exceeding the legal residue level of sulfonamide in swine in 2007 and six
findings in 2008, the number of samples of swine has been raised to roughly 2000 animals in
the 2010 NRCP.
B2a = Benzimidazoles
Milk, poultry and farmed game
Sample numbers have been enhanced for 2010 to the end of obtaining more analytic data for
an evaluation of relevance of the problem.
B2b = Coccidiostatics
The spectrum of coccidiostatic substances tested in eggs has been transferred to all other
animal species and matrices (with the exception of milk and honey), but is confined to the
substances subject to Regulation (EC) No. 124/2009.
B2c = Carbamates and pyrethroids
Horses
BVL pointed out that horses have so far not been tested for carbamates and pyrethroids,
though insecticides are playing an important role in horse keeping, in particular in summer.
It is, for instance, usual to braid horse manes with insecticide clips. Therefore, it was decided
that five horses should also be tested for pyrethroids under the 2010 NRCP.
B2c = Lambda-cyhalothrin
Honey
Sample number enhanced by 20 per cent.
B2d = Sedatives
Testing for xylazine (Rompun®) was discussed. According to Annex II to Regulation (EEC)
No. 2377/90, xylazine is authorised for use in bovines and Equidae, but not in pigs.
Xylazine is a widely used sedative. It is increasingly being used in cattle kept in extensive
pasture farming before slaughter, to facilitate handling of the animals. It was therefore decided
to include xylazine in testing in bovines and horses for one year.
B2e = NSAID
Samples of horses are tested for all kinds of NSAID tested also in other animal species under
the NRCP. In addition, ibuprofen and mefenamic acid have been included in analyses
conducted in red meat, poultry, milk, and farmed game, and tolfenamic acid has been included
in analyses in milk. Analyses of diclofenac in red meat are to be enhanced to improve the data
basis.
B2f = Carbadox and olaquindox
The Commission holds that the substances carbadox and olaquindox, though no longer
authorised for use, are relevant to health, and therefore recommends considering them in the
NRCP. This question was also discussed in Germany before. Both substances are feed
additives which are no longer permitted. They are subject to analyses in the framework of the
feed control plan. In 2007 and 2008, a total of nearly 800 samples of single feed, feed premixtures, and feed mixtures were analysed for carbadox and olaquindox, and all were
64
negative. According to our risk-based approach, carbadox and/or olaquindox will only be
considered in the NRCP after there have been relevant findings in the feed control plan, or
when there are other signs showing that the substances have actually been used. Hence, this
problem has to be discussed anew when the 2011 plan is prepared.
B2f = Cymiazole
Honey
Sample number enhanced by 20 percent for the whole group.
B3a = Nicotine
It was decided to raise the number of samples from 6 (to date) to 18 boiling chicken in the
2010 NRCP.
B3b = Phosmet
Phosmet has been included in the 2010 NRCP because there was one phosmet product about to
be authorised for use in laying hens. We have now learnt that the application for this product
has meanwhile been withdrawn.
B3e = malachite green
Aquacultures
Sample number enhanced by ten per cent in the 2010 plan.
Follow-up actions
Bovine
1 Enrofloxacin and
marbofloxacin; cows; muscle
and kidney
2 tetracycline; fattening calves;
muscle and 1 kidney
1 4-methylamino-aAntipyrin 4methylaminophenazone;
fattening cattle; liver
1 flunixin meglumin; fattening
cattle; kidney
1 phenylbutazone; fattening
cattle; plasma
Information to competent authority.
On-site investigation at the farm of origin, examination of the
records, 3 additional sampling, 2 increased controls in the
establishment of origin (blood and milk), injunction to notify
slaughter; criminal proceedings, control report pursuant to
Art. 9 letter e of Regulation (EC) No. 796/2004 (Withdrawal
of the possibility of receiving or requesting EU subsidies).
1 dexamethasone; cows; liver
On-site investigation at the farm of origin, 4 additional
sampling, notification of slaughter required, criminal
proceedings.
1 WHO-PCDD/F-PCB-TEQ
(WHO-TEF 1997) upper bound; sampling, following slaughter cattle will be sampled.
fattening cattle, fat
Likely source of contamination is a colour coating of
(WHO-TEF 1997) upper bound; protective barriers separating animals’ resting boxes. On-site
fattening cattle, fat
investigation at the farm of origin, 4 additional sampling, 18
65
1 lead Pb; fattening cattle;
kidney
1 cadmium Cd; cows; liver and
kidney
1 cadmium Cd; cows; kidney
2 mercury Hg; cows; kidney
1 mercury Hg; fattening cattle;
liver
liver
kidney
kidney
kidney
kidney
ban on transport and delivery of livestock (whole stock), 3
increased controls in the establishment of origin. The
suspected source of contamination has been eliminated.
Blood samples will be taken for a longer period ahead in
order to test effectiveness of the measure.
No information.
No information.
records, additional sampling. Control report pursuant to Art.
9 letter e of Regulation (EC) No. 796/2004 (Withdrawal of
the possibility of receiving or requesting EU-subsidies).
According to the relevant national regulations, positive
samples give only reason to complaint when the residues do
not stem from soil, water, or air pollution. In the present
cases, low contamination levels indicate that the source of
residues is environmental pollution. The maximum
permissible level in feed is 0.1 mg/kg, so that low-level
findings may also be attributable to legal feeding.
records.
sampling
records. Follow-up sampling. Control report pursuant to Art.
the possibility of receiving or requesting EU subsidies).
The animal was an 11-year old mother cow.
The farm of origin is in another Member State.
Pigs
1 dihydrostreptomycin; other
pigs; kidney
1 benzylpenicillin penicillin G;
fattening pigs; kidney
No information.
No information.
66
1 enrofloxacin; kidney and
muscle and sulfadimidin
muscle; other pigs
1 trimethoprim; fattening pigs;
kidney
1 sulfadiazine; other pigs;
kidney and muscle
1 sulfadiazine; fattening pigs;
muscle
1 sulfadiazine; kidney, and
trimethoprim; muscle and
kidney; fattening pig
1 chlortetracycline; fattening
pigs; kidney
1 tetracycline und
oxytetracycline fattening pigs;
muscle
1 tetracycline; fattening pigs;
muscle and kidney
5 cadmium Cd; other pigs;
kidney
kidney
kidney
1 cadmium Cd; fattening pigs;
kidney
Non-compliance with waiting period. On-site investigation at
the farm of origin, examination of the records, criminal
proceedings, More veterinary drug checks announced.
No information.
records, additional sampling, criminal proceedings. Control
report pursuant to Art. 9 letter e of Regulation (EC) No.
796/2004 (Withdrawal of the possibility of receiving or
requesting EU subsidies).
records, criminal proceedings, control report pursuant to Art.
the possibility of receiving or requesting EU subsidies).
Cross-contamination by liquid feeding. Information to
competent authority, examination of the record, criminal
proceedings, control report pursuant to Art. 9 letter e of
Regulation (EC) No. 796/2004 (Withdrawal of the possibility
of receiving or requesting EU-subsidies).
No information.
Breeding animal, aged over 24 months.
No information.
Animal aged over 18 months.
records, additional sampling, control report pursuant to Art. 9
letter e of Regulation (EC) No. 796/2004 (Withdrawal of the
possibility of receiving or requesting EU-subsidies).
10 mercury Hg; other pigs; liver Breeding animals aged over 24 months.
and 2 kidneys
26 mercury Hg; other pigs;
kidney
kidney
records.
Kidney and liver of the animal have not been sold as a food.
kidney
Early in 2010, all slaughter establishments will be addressed
with a recommendation not to place kidneys and livers of
67
breeding pigs on the market as food.
13 mercury Hg; fattening pigs;
liver and 37 kidneys
liver
liver and 6 kidneys
liver and 1 kidney
liver
liver
kidney
records, increased controls in the establishment of origin.
Slaughter and sampling/analysis of another sow. Sales ban on
livestock.
records, additional sampling.
The contaminated liver stems from a more than two-year-old
sow, in which natural environmental contamination with
heavy metals, including mercury, must be expected. The
slaughter establishment therefore condemns all livers and
kidneys from pigs aged over two years.
records, 7 additional sampling. Control report pursuant to
Art. 9 letter e of Regulation (EC) No. 796/2004 (Withdrawal
of the possibility of receiving or requesting EU-subsidies).
It is suspected that the mercury was released from pigs’ toys
(biting balls). On-site investigation at the farm of origin,
examination of the records, additional sampling, animals and
products classified as not suitable for human consumption.
Technical advice to the animal keeper.
Poultry
1 doxycycline; fattening
chicken; muscle
1 lindane; gammahexachlorocyclohexane;
gamma-HCH; fattening chicken;
fat; 0.057 mg/kg
records, 4 additional samplings, ban on transport and
delivery of livestock (33000)
Sheep / Goat
1 tulathromycin; sheep,
fattening lambs; muscle
No information.
1 mercury Hg; sheep, fattening
lambs; liver and 7 kidneys
68
1 mercury Hg; sheep, fattening
lambs; liver and 1 kidney
Horses
1 cadmium Cd; other horses;
muscle, liver and kidney
Milk
1 doramectin
Doramectin probably applied during the dry period. On-site
investigation at the farm of origin, examination of the
records, fine imposed. Control report pursuant to Art. 9 letter
e of Regulation (EC) No. 796/2004 (Withdrawal of the
possibility of receiving or requesting EU-subsidies).
Eggs
9 lasalocid
No information.
1 lasalocid
records, 3 additional samplings.
1 DDT, sum of DDT, DDE,
DDD, calculated as DDT and 1
DDE
1 endrin
No information.
(WHO-TEF 1997) upper bound
and 1 WHO-PCDD/F-TEQ
and 1 WHO-PCDD/F-TEQ
On-site investigation at the farm of origin, criminal
proceedings. Owner killed affected livestock on his own
responsibility.
records, additional sampling, animals and products classified
as not suitable for human consumption. Official
investigations with participation of the environmental
engineer; livestock/product barred; farmer advised. The
outdoor range of the fowl farm is subjected to various
sanitation measures. Flocks (total of 30 laying hens) are
killed.
69
Aquacultures
1 leucomalachite green; trout;
muscle of fish
No information.
muscle of fish
On-site investigation at the farm of origin, examination of
records, 1 additional sampling
muscle of fish
muscle of fish
On-site investigation at the farm of origin, examination of
records, 1 additional sampling. Ban on transport and delivery
of fish from that pond until results of investigations were
available. Increased controls in the establishment of origin.
Offence proceedings instituted.
muscle of fish; 0.026 mg/kg
records, 3 additional samplings, ban on transport and
delivery of livestock, farm barred. Fish may only be
delivered when proved to be free of any residues.
1 malachite green CI 42000 and It is suspected that waste water from the ornamental fish
pond was drained into rainbow trout and carp pond. On-site
muscle of fish
investigation at the farm of origin, examination of records, 4
additional samplings. Ban on transport and delivery of fish.
13 enhanced controls in the establishment of origin, criminal
proceedings.
1 malachite green CI 42000 and It is suspected that waste water from the ornamental fish
1 leucomalachite green; carp;
pond was drained into rainbow trout and carp pond. On-site
muscle of fish
investigation at the farm of origin, examination of records, 4
additional samplings. Ban on transport and delivery of fish.
13 enhanced controls in the establishment of origin, criminal
proceedings.
1 leucomalachite green; other
It is suspected that malachite green contaminated the ponds
fish; muscle of fish
during the previous owner’s era. On-site investigation at the
farm of origin, examination of the records. Ban on transport
and delivery of fish from all 4 ponds. Affected animals (210)
killed. 50 increased controls in the establishment of origin.
Animals and products classified as not suitable for human
consumption. Criminal proceedings. Control report pursuant
to Art. 9 letter e of Regulation (EC) No. 796/2004
(Withdrawal of the possibility of receiving or requesting EU
subsidies).
Farmed Game
1 mercury Hg; red deer; kidney
70
1 mercury Hg; fallow deer;
kidney
Game
1 mercury Hg; wild boar;
muscle; 0.017 mg/kg
16 mercury Hg; wild boar; liver
and 16 kidneys
5 mercury Hg; wild boar; liver
and 1 kidney
1 alpha-HCH and 1 beta-HCH;
wild boar; fat
1 beta-HCH; wild boar; fat
1 DDT, sum; 1 pp-DDE, wild
boar; fat
2 DDT, sum; wild boar; fat
1 DDT, sum; wild boar; fat
1 hexachlorebenzene HCB; wild
boar; fat
1 lindane; gammahexachlorocyclohexane;
gamma-HCH; wild boar
No information.
No information.
No definite exceeding of legal maximum level, as the value
measured is within the analytic method’s variance.
No information.
No information.
Honey
2 N,N-diethyl-m-toluamide
DEET
Attributable to use of insect deterrent spray "FABI". The
spray was an old-dated product which still contained the
substance DEET. The new spray products do no longer
contain this substance, according to the authority which
reported the finding.
71
DK
DENMARK
Group A substances
(aggregate for all animal products and substances)
Please explain changes introduced as a consequence of NC results in previous years
Follow-up actions
Thiouracil – Urine – Bull on farm, 9 5 subsequent suspicion samples were taken for
each Presumably Non-Compliant sample. The
months – 25,8 ppb
sample on farm was followed up in 2009 while the
Thiouracil – Urine – Bull in
sample from the slaughterhouse was followed up
Slaughterhouse, 13 months – 27
in 2010. Both cases proofed eventually to be
ppb
compliant because the 5 follow up samples
contained less than 25 ppb Thiouracil in both
Substance--Matrix-animal or animal cases.
Actions: (investigations in the farm of origin,
product-Concentration
animals held in farms, slaughtered animals,
intensified sampling in related farms, products
declared unfit for human consumption,
administrative measures, denial EC aid, others).
Group B substances
Follow-up actions
Bovines
1 WHO-PCDD / F-PCB-TEQ - Fat Investigations in order to find the source have led
to the hypothesis that it is a local pollution of the
feed due to spillage of PCB-containing liquid.
& Number of non-compliant
@ List actions: (e.g investigations in the farm of
results-substance (if possible
origin: verification of records, additional
matrix)
sampling; animals held in the farm, iintensified
checks on the animals and products from the
farm/establishment in the event of repeated
infringements, carcasses and products declare
unfit for human consumption, administrative
measures, others).
Pigs
6 Benzylpenicillin (Penicillin G)1 herd could not be identified, carcass declared
Sow Kidney
unfit for human consumption, no action.
1 verification of records concluded that withdrawal
period was compliant, therefore no action but
carcass declared unfit for human consumption.
Remaining 4 cases: Investigations in the farms of
2 Oxytetracycline – Sow kidney
origin, verifications of records, carcasses declared
72
unfit for human consumption, administrative fines.
2 Investigations in the farms of origin,
verifications of records, carcasses declared unfit
for human consumption, administrative fines.
Poultry
Sheep and goat
Horses
Milk
1 Salinomycin – 9,1 ppb in eggs
Eggs
Information of the Plant Directorate who takes
care of enforcement of rules on feed.
Rabbit
1 Leuco Malachite Green –
Uncertain concentration – Muscle
and skin of trout
Aquaculture
The Presumably Non-Compliant Sample was
eventually declared Compliant, because 5
subsequent suspicion samples were negative.
Farmed game
3 Lead-Muscle of Wild Game
Wild game
No action since game is a rare menu.
Honey
73
EE
ESTONIA
Group A substances
Follow-up actions
Chloramphenicol – 0.12 µg/kg- raw
milk- cow
The sample was taken from dairy industry before the
bulk tanker has discharged (milk from 2 farms cows
together). The farms of origin were investigated
immediately after receiving positive results. 2 milk
samples were taken and analysed with negative
results.
The follow-up inspection didn’t give any evidence of
an illegal use of chloramphenicol.
Thiouracil – 4.10 µg/kg – urine - pig
The farm of origin was investigated immediately.
There was no indication of an illegal use of
thiouracil.
The presence of thiouracil at such low level could be
linked as a result of the natural presence of crucifera
plants in feed.
β-testosterone - <0.1 µg/kg; αtestosterone 2.8 µg/kg - serum –
young bovine at farm
2 samples were taken from one farm. The farm of
origin was investigated immediately after receiving
positive results.
α-testosterone 0.8 µg/kg - serum –
young bovine at farm
Movement of animals from farm to other facilities or
movement to the slaughterhouse was temporarily
stopped. 2 additional (serum) samples were taken and
analysed with negative results.
During the follow-up inspection in the farm of origin
it became obvious that both samples were taken from
pregnant young bovines and there were no
indications of an illegal use of testosterone.
* Information to be included for each non-compliant result.
In case of several non-compliant results for the same substance in the same holding or related
holdings, data could be aggregated.
Data on concentration and matrix is very useful to be used as background information for the
monitoring of the prevalence of use of group A substances.
Group B substances
All the 2009 non-compliant results (except wild game) have been taken into account
74
regarding the 2010 plan and the numbers of samples have been increased accordingly.
The number of the wild game samples will be at the same level as 2009.
Follow-up actions
Bovines
Pigs
Poultry
Sheep and goat
Horses
Milk
Microbiological screening – positive The farm of origin was investigated immediately.
result – for further examination with Additional raw milk sample was taken and analysed
LC-MS/MS – PenicillinG – 4.5 with negative result.
µg/kg
Eggs
Salinomycin – 8.35 µg/kg
The farm of origin was investigated immediately
after receiving positive result. 1 additional egg
sample was taken and analysed with negative result.
The farm has its own feed–mill plant. Investigation
was performed on the feed-mill plant too. Additional
animal feed samples (2 samples) were taken and
analysed with positive results: salinomycin 193
µg/kg and salinomycin 18 µg/kg.
The contamination reason was feedingstuffs crosscontamination.
Rabbit
@
Aquaculture
Farmed game
@
Wild game
2 muscle samples in wild boar were
Heavy metals are present in the environment as a
positive for cadmium
result of a long-time absorption and may accumulate
1 muscle sample in roe was positive
in animal tissues.
for lead
Honey
75
ES
SPAIN
Group A substances
Equino:Incremento de la investigación de nuevas sustancias en el grupo A3 y A6
(nitrofuranos)
Follow-up actions
2. Cloranfenicol en músculo de aves.
Control
dirigido.
Análisis
iniciales:0,25 y 0,47 µg/kg.Análisis
contradictorios 0,23 y 1,57 µg/kg
Actuaciones C. Sanidad: Inhibición CCAA de
origen. Comunicación SCIRI (Sistema Coordinado
de Intercambio Rápido de Información). Seguimiento
analítico de 21 muestras correspondiente a 1 lote con
resultado negativo a petición de la CCAA de origen
dentro del Plan de Sospechosos.
Actuaciones en la Comunidad Autónoma de
Origen:
Investigación en las explotaciones ganaderas de
avicultura - producción de carne, verificación de
registros de la explotación, movimientos de animales,
consumos de pienso y prescripciones de pienso
medicamentoso.
Implantación de medidas cautelares, inmovilización
de los animales de las explotaciones (20.994 y
10.200), recogida, en total, para análisis de 3
muestras de pienso y 3 de agua de bebida, con
resultado negativo. Se procede al sacrificio bajo
control sanitario de un lote de 21 animales, de cada
explotación, resultando negativos a la detección de
Cloranfenicol, por lo que son conducidos a matadero
para su sacrificio.
Iniciación de expediente sancionador calificado como
muy grave en una cuantía de 30.000 €. En
tramitación. El resultado de los análisis
contradictorios confirman la no conformidad
1. Cloranfenicol en músculo de aves. Actuaciones C. Sanidad: Inhibición CCAA de
Control dirigido. Análisis inicial: 0,90 origen. Comunicación SCIRI. Seguimiento analítico
µg/kg Análisis contradictorios: 0,38 de 21 muestras correspondiente a 1 lote con resultado
µg/kg
negativo a petición de la CCAA de origen dentro del
Plan de Sospechosos.
Origen:
Los Servicios Veterinarios Oficiales, realizan visita
de inspección a dicha explotación con las
consiguientes investigaciones pertinentes, referentes
a libro de registro de tratamientos, recetas de
prescripción veterinaria de medicamentos, así como
76
los controles documentales sobre entradas y salidas
de animales, alimentos, piensos y materias primas
destinadas a la alimentación animal. Así mismo se
procede a la correspondiente toma de muestra de
pienso y envío al Laboratorio.
Concluida la inspección y tras la realización de los
análisis con resultado conforme, se informa al
ganadero que puede optar por anticipar el envío de un
lote representativo y selectivo al matadero, el cual
será analizado con intervención de canales y
despojos, habiendo una restricción total de
movimientos del resto del lote (en la explotación)
hasta la obtención de resultados. Si estos fueran
satisfactorios, se podrán sacrificar el resto del lote sin
intervención ni análisis, siendo la selección del lote
en la explotación para su sacrificio y muestreo,
realizado por las Autoridades competentes de la
Oficina Comarcal Agraria.
Así mismo, durante los doce primeros 12 meses, la
documentación que acompañe a los animales al
matadero hará mención expresa de que dicha
explotación se encuentra bajo vigilancia por haber
detectado cloranfenicol en alguno de los animales de
dicha explotación en el ámbito de actuaciones del
Plan Nacional de Investigación de Residuos, al objeto
de proceder a las medidas contempladas en el artículo
22 del RD 1749/1998.
Posteriormente se realiza nueva visita por los
Servicios Veterinarios Oficiales, procediendo a la
toma de muestras de 21 animales como lote
representativo para su envío al matadero, toma de
muestras y análisis, siendo el resultado del mismo
conforme.
Situación
del
expediente
administrativo:
Suspendido por estar conociendo el juzgado de
instrucción correspondiente.
1. Cloranfenicol en músculo de aves. Actuaciones Consejería de Sanidad: Comunicación
Control dirigido. Análisis inicial: 0,19 a Consejería de Agricultura, Pesca y Alimentación
µg/kg. Análisis contradictorio: 0,28 para la investigación de la explotación de origen.
µg/kg
Comunicación SCIRI. Seguimiento analítico de 21
muestras correspondiente a 1 lote con resultado
negativo a petición de la Consejería de Agricultura,
Pesca y Alimentación dentro del Plan de
Sospechosos.
Comunicación a la Unidad de Sanciones para la
incoación del correspondiente expediente.
Actuaciones Consejería de Agricultura:
Se realiza una investigación en granja, con censado y
toma de muestras, e inmovilización cautelar.
77
Los análisis de pienso, agua y animales han dado
resultado negativo, por lo que no se ha podido
determinar el origen del residuo.
1. Cloranfenicol en músculo de Actuaciones de la Agencia de Protección de la
pollo.Control
dirigido.Analisis Salud.:
inicial:
1,04
µg/kg.Análisis Expediente incoado y suspendido al enviarse a
contradictorio: 0,40 µg/kg.
fiscalía. Comunicación al Departamento de
Agricultura y a la Unidad de Consumo.
Comunicación a la AESAN a través del SCIRI.
Actuaciones del Departamento de Agricultura,
Alimentación y Acción Rural:
1 explotación intervenida. Toma de muestras: 3
aguas, 4 piensos y 4 orinas de los bovinos presentes
en la explotación. Todos los resultados negativos.
1. Ronidazol en músculo de
ovino.Control
dirigido.Analisis
inicial:
1,2
µg/kg.Análisis
contradictorio: 1,4 µg/kg.
Actuaciones de la Agencia de Protección de la
Salud:
Expediente incoado y suspendido al enviarse a
Explotación intervenida (1880 animales). Toma de
muestras: 5 aguas, y 7 piensos. Todos los resultados
negativos.
1. Ronidazol en músculo de ovino. Actuaciones de la Agencia de Protección de la
Control dirigido. Análisis inicial: 2,2 Salud.:
µg/kg.Análisis contradictorio: 1,4 Se ha enviado el expediente a la Consejería de
µg/kg.
Sanidad de la comunidad de origen de la explotación
y se ha comunicado también a la AESAN a través del
SCIRI.
Actuación en la explotación ganadera de la
Comunidad Autónoma de Origen:
Los Servicios Veterinarios Oficiales de la Delegación
de Agricultura y D.R. y de la Oficina Comarcal
Agraria, realizan visita de inspección a dicha
explotación con las consiguientes investigaciones
pertinentes, referentes a libro de registro de
tratamientos, recetas de prescripción veterinaria de
medicamentos, así como los controles documentales
sobre entradas y salidas de animales, alimentos,
piensos y materias primas destinadas a la
alimentación animal. Así mismo se procede a la
correspondiente toma de muestra de pienso (2
muestras) y envío al Laboratorio correspondiente.
Concluida la inspección y tras la realización de los
análisis del pienso con resultado conforme, se
informa al ganadero que, durante los seis primeros
meses a partir del 05/10/2009 (fecha de
78
comunicación de AESAN), puede optar por anticipar
el envío de un lote representativo y selectivo al
matadero, el cual será analizado con intervención de
canales y despojos, habiendo una restricción total de
movimientos del resto del lote (en la explotación)
hasta la obtención de resultados. Si estos fueran
satisfactorios, se podrán sacrificar el resto del lote sin
intervención ni análisis, siendo la selección del lote
en la explotación para su sacrificio y muestreo,
realizado por las Autoridades competentes de la
Oficina Comarcal Agraria.
En este caso el ganadero ha decidido acogerse a esta
opción.
Hasta el 25 de marzo se han formado 8 lotes de
corderos con destino a sacrificio, tomándose muestras
representativas de ellos para su análisis, siendo los
resultados conformes.
Así mismo, durante los doce primeros meses a partir
de dicha fecha, la documentación que acompañe a los
animales al matadero hará mención expresa de que
dicha explotación se encuentra bajo vigilancia por
haber detectado ronidazol en alguno de los animales
de dicha explotación en el ámbito de actuaciones del
de proceder a las medidas contempladas en el artículo 22 del
RD 1749/1998.
1. Cloranfenicol en leche de Inmovilización de 344 ovejas en la explotación y de
3000 quesos elaborados a partir de la leche de la
ovino.Control dirigido.2 µg/kg
explotación.
Apertura de expediente sancionador.
Recogida de muestras de agua y de queso que
resultaron negativas.
Como resultado de la investigación se concluyó que
el origen del cloranfenicol se encontraba en el
conservante empleado para recogida de muestras
decontrol lechero efectuada, por la Asociación de
Ovino Lechero, en el mismo día en que se recogió la
muestra para el PNIR. La contaminación tuvo lugar
por desbordamiento del contenido de los envases en
el flujo que conduce la leche al tanque.
Como consecuencia de ello, se ha modificado el
procedimiento de recogida de muestras de la citada
asociación y se levantaron las medidas cautelares
adoptadas en la explotación.
79
Group B substances
Miel: Incremento de la frecuencia de muestreo en los grupos B1 y B2f.
Leche: Inclusión de la investigación en esta matriz del grupo B2e.
Follow-up actions
Bovines
1.
Oxitetraciclina
pienso
no Análisis Contradictorio: Confirmada presencia.
medicado. Control dirigido: 1.293,00 Investigación en la fábrica de las posibles causas.
µg/kg
Implementación del sistema de control de calidad en
referencia a contaminaciones cruzadas en fábrica.
Archivo expediente.
6. Prednisolona/prednisona orina. Consejería de Medio Rural y Pesca
Control dirigido
1. Positivo en explotación
1,54 µg/L de PREDNISONA y 1,93 µg/L de
PREDNISOLONA en orina de bovino de cebo
macho de 11 meses de edad de raza asturiana de los
valles.
Actuaciones en explotación según normativa
aplicable (RD 1749/98).
Incoada propuesta de procedimiento sancionador
Se comunica a la Agencia de Sanidad Ambiental y
Consumo para su seguimiento en matadero.
>0,25 µg/L de PREDNISOLONA en orina de bovino
de cebo macho de 7 meses de edad mestizo.
Pendiente de actuaciones en explotación según
normativa aplicable (RD 1749/1998).
de cebo macho de 9 meses de edad de raza asturiana
de los valles.
>0,50 µg/L de PREDNISONA en orina de bovino de
cebo macho de 12 meses de edad de raza asturiana de
los valles.
Consumo para su seguimiento en matadero según
80
normativa aplicable (RD 1749/98).
5. positivo en explotación
de los valles.
de los valles.
aplicable (RD 1749/98). Las investigaciones revelan
que el resultado se debe a tratamiento autorizado
avalado por la correspondiente receta y anotado en el
registro de tratamientos.
No se abre expediente y se notifica al titular como
resultado favorable.
Actuaciones Agencia Sanidad Ambiental y
Consumo en los 6 casos En los casos de positividad
a prednisolona: traslado de la información a los
Servicios Veterinarios de los mataderos de la
Comunidad Autónoma. Se ha investigado 11
animales originarios de esas explotaciones. Todos los
resultados fueron satisfactorios.
1. Dihidroestreptomicina. Riñón. 1 Canal decomisada por screening positivo a
Control sospechoso.5068 ppb
antibacterianos, confirmada la presencia de
dihidroestreptomicina (5068 ppb) por encima de los
LMR. Renuncia a análisis contradictorio.
Bovino hembra, 13 años de edad.
Incoado procedimiento sancionador. Trasladado a
Fiscalía.
Se trasladó toda la información a la Consejería de
Medio Rural y Pesca.
Actuaciones Consejería de Medio Rural y Pesca:
Se comprueban los movimientos del animal en la
base de datos REMO y se realiza visita de inspección
a la explotación de origen del animal, donde se ponen
de manifiesto los siguientes hechos:
No consta ningún tratamiento anotado en el libro de
registro de explotación de ganado vacuno.
No hay ninguna receta correspondiente a los últimos
81
1. Doxiciclina en músculo.Control
dirigido
9. Doxiciclina
sospechoso
en
orina.Control
1. Oxitetraciclina en riñon.Control
dirigido.Bovino de lidia .5521 µg/kg
2. Dexametasona en hígado. Control
dirigido.15 y 19 µg/kg
1. Zearalenona en pienso. Control
sospechoso.21 µg/kg
meses.
No hay ningún medicamento en el establo
Medidas cautelares en la explotación.
Inmovilización y toma de muestras y demás medidas
del RD 1749/1998.(Véase **)
Comunicación a través de red de alerta.
Toma regular de muestras por sospecha en
explotación y matadero.
Propuesta de expediente sancionador.
Los 9 no conformes son consecuencia del citado mas
arriba (relación con **).
Inmovilización cautelar de 280 reses en explotación,
con restricción de movimientos y control por
muestreo en matadero previo a sacrificio.
Inclusión en red de alerta durante 7 meses.
Propuesta de expediente sancionador (diferente al no
conforme en matadero)
Comunicación a Comunidad Autónoma de Origen.
Actuación en la Comunidad Autónoma de Origen:
En la Comunidad Autónoma de origen se realiza una
investigación epidemiológica, con inmovilización
cautelar, y toma de muestra de piensos y agua con
resultados conformes, En el Libro de registro de
Tratamientos de la explotación no viene reflejado que
se haya tratado alguno de los bovinos que fueron a la
plaza de toros. No hay evidencias que indiquen que
se le administró dicho antibiótico en la explotación
de origen.
Las dos no conformidades son de la misma
explotación.
Investigación en la explotación ganadera de
Bovino de cebo, verificación de registros de la
explotación,
especialmente de tratamientos
veterinarios con antiinflamatorios, procedencia y
consumos de pienso y prescripciones de pienso
medicamentoso.
de 641 bovinos, se recogen 3 muestras de pienso y 1
de agua con resultados analíticos negativos a
dexametasona. Se procede al sacrificio bajo control
sanitario de un lote de 21 animales, resultando aptos
para el consumo.
grave en una cuantía de 3.500 €. Resuelto con fecha
21/01/2010
Investigación en la explotación ganadera de bovino
de producción de carne, verificación de registros de
la explotación, movimientos de animales, consumos
de pienso.
82
de los animales de la explotación (89 bovinos). Se
mantiene la inmovilización hasta el muestreo de los
animales en el momento de su sacrificio en matadero
2. Cadmio en riñón. Control
dirigido.1, 41 mg/kg y 3,3 mg/kg.
Salud.:
Comunicaciones al Departamento de Medio
Ambiente
de
la
Comunidad
Autónoma
correspondiente.
1. Dexametasona en hígado. Control Actuaciones de la Consejería de Sanidad:
dirigido. Bovino de lidia Mas de
Comunicado a través del SCIRI.
4,8µg/kg
Iniciado expediente sancionador.
Estado de tramitación: Acuerdo de iniciación y
Pliego de cargos.
Actuaciones de la Consejería de Agricultura y
Ganadería:
Visita a la explotación y revisión documental, del
botiquín y del contenedor de residuos de
medicamentos, comprobación de la trazabilidad del
animal afectado, así como diligenciado del libro de
registro.
Notificación de las actuaciones llevadas a cabo al
departamento de Salud.
1. Dexametasona en hígado .Control Actuaciones de la Consejería de Sanidad:
dirigido. Mas de 4,8µg/kg
Comunicado a través del SCIRI
Ha resultado positivo en una nueva partida de
animales a matadero.
Seguimiento de la explotación con muestreo en
matadero durante seis meses.
Estado de tramitación: acuerdo de inicio.
Ganadería:
medicamentos, comprobación de la trazabilidad del
animal afectado, así como diligenciado del libro de
registro.
Retirada de talonarios de autoguías y marcado de las
GOSA en caso de salida de animales de la
explotación hasta la obtención de los resultados de
las nuevas muestras de pienso recogidas de las que
todavía no se dispone de los resultados.
1. Triamcinolona acetonide en hígado de Comunicación a través del SCIRI. Inmovilización
y destrucción de la canal Traslado del expediente a
toro de lidia. Control dirigido 2,4 µg/kg
la Comunidad Autónoma de origen. Entrada en
listado de sospechosos para seguimiento.
Personado el control oficial en la explotación de
origen, donde se censa el efectivo de la explotación
83
que cuenta con 309 animales. No hay anomalía en la
identificación. Se comprueba el pienso que se da a
los animales, es correcto con identificación correcta.
Se coteja el libro de tratamientos veterinarios, el cual
solo tiene anotaciones desde el 8 de julio de 2.009. A
partir de ese momento se procede a consignar en las
G.O.S.P. emitidas desde la explotación, la referencia
del seguimiento a la investigación de la sustancia
referida anteriormente.
1. Dexametasona en hígado de toro Comunicación a través del SCIRI. Traslado del
de lidia. Control dirigido 49,7 µg/kg. expediente a la Comunidad Autónoma de origen.
Entrada en listado de sospechosos para
seguimiento.
Se procedió a la investigación epidemiológica,
inmovilización cautelar de la explotación. No
procedía un muestreo reforzado por haber
transcurrido cierto tiempo desde la toma de
muestras que dio resultado positivo hasta que llegó
la notificación. Comprobado libro de tratamientos
medicamentosos de la explotación, y según
manifestaciones del representante, no se ha
aplicado dicha sustancia a ningún toro. Que el
titular ya tenía conocimiento del positivo, pues
había recibido notificación de la Comunidad
Autónoma que detecto la no conformidad, en la
que se le notificaba y se le daba la posibilidad de
realizar el Análisis Contradictorio. El titular
solicita dicho análisis con el resultado no conforme
de 10µg/kg.Desde la C.A.que detectó la no
conformidad se está incoando el expediente. No
hay evidencias para atribuir responsabilidades al
titular de la explotación de origen.
.
1. Dexametasona en hígado de toro
Comunicación a través del SCIRI. Inmovilización
de lidia. Control dirigido 10 µg/kg
y destrucción de la canal Traslado del expediente a la
Comunidad Autónoma de origen. Entrada en listado
de sospechosos para seguimiento
Actuaciones en explotación: Los Servicios
Veterinarios Oficiales, realizan visita de inspección a
dicha
explotación
con
las
consiguientes
investigaciones pertinentes, referentes a libro de
registro de tratamientos, recetas de prescripción
veterinaria de medicamentos, así como los controles
documentales sobre entradas y salidas de animales,
alimentos, piensos y materias primas destinadas a la
alimentación animal. Se comprueba la anotación en
el libro de tratamientos de una administración de
Vetione (medicamento a base de dexametasona)
84
prescrito mediante receta veterinaria número
D/0053368-0, con fecha 22 de julio de 2009.
Se informa al ganadero que durante seis meses la
detectado dexametasona en alguno de los animales de
dicha explotación en el ámbito de actuaciones del
de proceder a las medidas contempladas en el artículo
22 del RD 1749/1998.
Actuaciones en mataderos: Se han sacrificado 33
animales procedentes de la explotación sospechosa
inmovilizándose las canales hasta la obtención de los
informes laboratoriales, que resultaron negativos.
Situación del expediente administrativo:
Expediente en tramitación.
Pigs
1. Prednisolona- Hígado. Control
Actuaciones del Departamento de Salud:
dirigido
Comunicación SCIRI
Comunicación y traslado de documentación a la
Agencia Española de Seguridad Alimentaria y
Nutrición (AESAN)
Seguimiento en matadero durante tres meses
Actuaciones de AESAN:
Comunicación a las autoridades competentes de
Portugal ya que la explotación es de dicho país.
1. Doxiciclina Riñón. Control
dirigido
Comunicación SCIRI
Comunicación al Departamento de Desarrollo Rural
y Medio Ambiente
Comunicación al Juzgado de Primera Instancia
Comunicación al interesado
Seguimiento en matadero durante tres meses.
Propuesta de apertura de expediente sancionador.
Actuaciones del Departamento de Desarrollo
Rural y Medio Ambiente
Visita de inspección a la explotación e
inmovilización cautelar de la misma
1. Doxiciclina en músculo.Control Actuaciones de la Agencia de Protección de la
dirigido. Mas de 150 µg/kg
Salud.:
Una explotación visitada. Comprobación de
documentación. No hay toma de muestras.
85
1. Enrofloxacina en músculo. Actuaciones de la Agencia de Protección de la
Control dirigido. Mas de 150 µg/kg
Salud.
Comunicación a la AESAN a través del SCIRI
1 explotación intervenida. Toma de muestras: 1 agua
y 1 pienso. Todos los resultados negativos.
1. Sulfametacina (sulfadimidina) en Actuaciones de la Agencia de Protección de la
músculo.Control dirigido. Inicial más Salud.:
de 150 µg/kg y Contradictorio mas Expediente incoado y suspendido al enviarse a
de150 µg/kg
1 explotación intervenida (3550 animales) Toma de
muestras: 1 agua y 1 pienso. Todos los resultados
negativos.
1. Sulfametacina (sulfadimidina) en Actuaciones de la Agencia de Protección de la
músculo. Control dirigido. Inicial Salud:
Mas de 150 µg/kg y Contradictorio Se ha enviado el expediente a la Consejería de
mas de150 µg/kg
SCIRI.
Actuaciones Consejería de Sanidad: comunicación
Consejería de Agricultura, Pesca y Alimentación para
la investigación en la explotación de origen.
Seguimiento
analítico
de
20
muestras
correspondiente a 1 lote con resultado negativo a
petición de la Consejería de Agricultura Pesca y
Alimentación dentro del Plan de Sospechosos.
Comunicación a la Unidad de Sanciones para la
incoación del correspondiente expediente.
Actuaciones Consejería de Agricultura:
Se realiza una investigación en granja. Con
anterioridad al envío al matadero se trataron los
animales con sulfametazina entre el 27/02/09 y el
03/03/09. El período de supresión es de 8 días, y el
primer envío a matadero se realizó el 22/04/09 por lo
que se respetó el período de supresión
1. Sulfadiacina en músculo. Control Actuaciones de la Consejería de Sanidad:
dirigido. 178 µg/kg
Notificación a la CA de origen de los animales.
Renuncia a la realización del contradictorio.
Estado de tramitación: Propuesta de Resolución, en
86
periodo de alegaciones, con sanción pecuniaria de
3.005,07 €
Salud.:
Comunicación al Departamento de Agricultura y a la
Unidad de Consumo.
1
Explotación
visitada.
Comprobación
de
Se comprobó el registro de tratamientos veterinarios
y se observó que se hizo un tratamiento con
sulfadiazina mediante premezcla medicamentosa
autorizada un tiempo antes de la salida de los
animales al matadero.se comprobaron las fechas de
administración del tratamiento y salida de los
animales a matadero y se comprobó que se respetó el
tiempo de espera.
1. Sulfadiacina en músculo. Control Actuaciones de la Consejería de Sanidad:
dirigido. Más de 200 µg/kg
Análisis contradictorio positivo.
3.005,07 €.
Ganadería:
medicamentos, comprobación de la trazabilidad de
los posibles animales afectados, así como
diligenciado del libro de registro.
las nuevas muestras de pienso y agua recogidas que
finalmente resultaron negativas.
2. Sulfametacina (sulfadimidina) Actuaciones de la Consejería de Sanidad:
en músculo.Control dirigido. 123 Comunicado a través del SCIRI.
µg/kg y 176 µg/kg
Renuncia a la realización del contradictorio.
3.005,07 €
Actuación en la explotación ganadera de la
Comunidad Autónoma de Origen:
87
1. Dioxinas y furanos en aditivo
tecnológico con destino a la
alimentación animal.Control
dirigido.3.61 ng TEQ/kg
4. Sulfametacina en pienso. Control
sospechoso.0,9 mg/kg,0,9 mg/kg,0,5
mg/kg y 4,2 mg/kg
2. Clortetraciclina en pienso.Control
dirigido. 8.7 +/- 2.0 mg/kg. Y 6.0 +/1.5 mg/kg
2 Doxiciclina en pienso.Control
dirigido. 17 +/- 4.0 mg/kg. y 18 +/-4
mg/kg
1. Doxiciclina más tilosina en
pienso.Control dirigido.6.6 +/- 1.6
mg/kg y 1.5 +/- 0.4 mg/kg
1. Doxiciclina más tilosina en
pienso.Control dirigido.9 +/- 2 mg/kg
y 24 mg/kg
4. Oxitetraciclina en pienso .Control
dirigido. 10 +/- 2.0 mg/kg., 14 +/-3
mg/kg, 9 +/- 2 mg/kg y 9.5 +/- 2.2
mg/kg
1. Oxitetraciclina en pienso. Control
dirigido.42 +/- 8 mg/kg
Investigación en granja de origen, todos animales
inmovilizados cautelarmente en la granja hasta los
primeros resultados, 0 animales sacrificados, 6
meses duración del seguimiento, todas muestras
resultados negativos, no procede iniciar expediente
ya que la Comunidad Autónoma que lo detectó no se
inhibe por cuestión de territorialidad.
Comunicación alerta RASFF nº E10/2009. En la
actualidad sigue prohibida la comercialización de
este aditivo hasta que identifiquen la fuente de
contaminación y aseguren su inocuidad.
920 Animales inmovilizados cautelarmente hasta los
primeros resultados.Se toman 4 muestras por haber 4
lotes de animales comiendo piensos diferentes.Tras
los resultados restricción total movimientos hasta
nuevos análisis, continua seguimiento otros 6 meses
con toma de muestras cada 3 meses. Segunda toma
de muestras dan resultados negativos, se levanta la
restricción una vez pasado periodo de espera del
primer pienso consumido que dio positivo. Tercera
toma de muestras dan resultados negativos. Se
inicia expediente sancionador por parte de
Agricultura consecuencia de los primeros análisis.
El Departamento de Agricultura, Alimentación y
Acción Rural no realiza ninguna actuación /
expediente sancionador cuando se obtienen
resultados inferiores o igual a 20 mg/kg +/- de
antibióticos en piensos.
1 Expediente sancionador iniciado en trámite.
1 Explotación intervenida (800 animales). Toma de
muestras: 4 aguas y 3 piensos. Todos los resultados
negativos.
antibióticos en piensos
88
muestras: 1 Agua y 1 pienso. Todos los resultados
negativos.
1. Oxitetraciclina en pienso. Control 1 Expediente sancionador con resolución de
dirigido.57 +/- 10 mg/kg
sobreseimiento del mismo
3. Tilosina en pienso. Control El Departamento de Agricultura, Alimentación y
dirigido. 4 +/- 0.7 mg/kg. , 2.6 +/-0.5 Acción Rural no realiza ninguna actuación /
mg/kg, y 0.9 +/- 0.3 mg/kg
1. Tilosina en
dirigido. 48 mg/kg
pienso.Control 1 Expediente sancionador iniciado en trámite.
muestras: 1 Agua y 1 pienso. Todos los resultados
negativos.
Poultry
1. Enrofloxacina músculo (pollo Renuncia a contradictorio
broiler). Control sospechoso. Inicial: Control de la explotación ganadera y restricción
164 µg/kg
salida de animales.
Investigación en la explotación de las posibles causas
(libros de explotación y de medicamentos,
alimentación, sistema de administración de
medicación en agua).
Comunicación SCIRI
Muestreo representativo en granja del lote con
engorde finalizado.
Autorización de salida a matadero del lote con
engorde acabado tras resultados de muestreo
representativo conforme.
Instrucción de expediente sancionador.
Causa más probable: falta de control en el sistema de
administración de medicamento en agua.
Medidas
cautelares en explotación.
1.
Enrofloxacina
más
Ciprofloxacina en músculo. Control Inmovilización y toma de muestras y demás medidas
dirigido.
del RD 1749/1998.
Comunicación a SCIRI.
Toma regular de muestras por sospecha en
explotación y matadero.
Propuesta de expediente sancionador.
1.
Enrofloxacina
más Actuaciones de la Agencia de Protección de la
Ciprofloxacina en músculo de pato. Salud.:
Control dirigido. Más de 150 µg/kg
Agricultura y a la Unidad de Consumo la Comunidad
Autónoma. Comunicación a la AESAN a través del
SCIRI
1 explotación intervenida (980 animales). Toma de
muestras: 1 agua y 2 piensos. 2 resultados positivos a
89
enrofloxacina en las muestras de pienso (1139µg/kg y
936µg/kg).(véase también****)
1 expediente sancionador iniciado en trámite.
2. Enrofloxacina en pienso. Control En los dos casos es consecuencia del citado mas
sospechoso. 1139µg/kg y 936µg/kg
arriba (véase ****).
Quedan pendientes las actuaciones a la explotación
con resultado positivo. Se han dado instrucciones a
los servicios veterinarios locales para realizar dichas
actuaciones.
2. Oxitetraciclina en pienso. Control En 2 casos investigaciones en granja.Se observa que
dirigido
el origen está en la fabrica de piensos, lo que genera
nuevas
actuaciones
por
sospecha
en
explotaciones.(véase *)
3. Oxitetraciclina en pienso. Control En los 3 casos es consecuencia del citado mas arriba
sospechoso
(relación con *).Se concluye que se debe a una
contaminación cruzada en la fabrica.
Propuesta de expediente sancionador a la fábrica.
1. Doxiciclina en músculo. Control Actuaciones en matadero:
dirigido.140,3 µg/kg
Comunicación al SCIRI.
Comunicación a la autoridad Competente de origen
y al Vocal del PNIR en la Comunidad Autónoma de
Origen.
Solicitud y auditoria del Plan de residuos del
matadero en cuestión.
Propuesta de sanción a la explotación ganadera.
Inclusión en relación de explotación sospechosa.
Se realiza la investigación epidemiológica, con
inmovilización cautelar, con toma de muestras con
resultado negativo y en el libro de tratamientos de la
explotación figura que la manada de aves fue tratada
en el agua de bebida con una combinación de
doxiciclina y enrofloxacina, y que se respetaron los
tiempos de espera (4 días).
Nos llega fax indicándonos que el Análisis Dirimente
ha resultado no conforme (No teníamos noticia de
que se hubiera realizado el Contradictorio)
En octubre, se recibe oficio de la Autoridad
competente que ha detectado la no conformidad, en el
que nos vuelven a notificar un segundo positivo a
doxiciclina (>150 µg/kg) en músculo de pollo de la
misma explotación y en el mismo matadero. El
Análisis Dirimente de este positivo da un resultado
de no superar el límite de Decisión (CC alfa).
Nuevamente, se realiza un estudio epidemiológico,
con toma de muestras negativa, y donde se pone de
manifiesto que este lote de aves ha sido tratado con la
misma combinación de antibióticos que la anterior.
Que la explotación de aves pertenece a una
90
1. Sulfametacina en músculo.
Control dirigido. Inicial 178 µg/kg
Contradictorio: 159 µg/kg
1. Doxiciclina en agua. Control
dirigido. 3mg/kg
dirigido. 33,6mg/kg
sospechoso. 12 +/- 3 mg/kg .
1. Oxitetraciclina en agua.Control
sospechoso. 10 +/- 2 mg/kg .
integradora que la suministra los pollitos de un día de
vida, el pienso que consume, el matadero donde se
sacrifican y el veterinario que prescribió ambos
tratamientos.
Se han respetado los tiempos de espera prescritos (4
días), no obstante, si la asociación de más de un
medicamento se puede entender como una
prescripción excepcional, entonces, en el artículo 81
del RD 109/95, de 27 de enero, sobre medicamentos
veterinarios, se establece un tiempo de espera de 28
días para carnes de aves de corral.
origen
Actuaciones Consejería de Sanidad:
Comunicación a Consejería de Agricultura, Pesca y
Alimentación para la investigación en la explotación
de origen. Seguimiento analítico de 21 muestras
correspondiente a 3 lotes con resultado negativo a
petición de la.Consejeria de Agricultura, Pesca y
Alimentación
dentro
del
plan
de
sospechosos.Comunicación a la Unidad de Sanciones
para la incoación del correspondiente expediente.
Actuaciones C. agricultura:
Se efectúa una investigación completa en la
explotación, con toma de muestras de pienso y
animales, con resultado negativo. Se investigan
también la fábrica suministradora del pienso y los
transportistas de pienso medicamentoso, con
resultados negativos, por lo que no se puede
determinar el origen del residuo.
1 expediente sancionador iniciado en trámite.
muestras: 7 aguas y 4 piensos. Todos los resultados
negativos
91
2. Doxiciclina en pienso. Control El Departamento de Agricultura, Alimentación y
dirigido. 7,7 +/- 1,8 mg/kg y 7,4 +/- Acción Rural no realiza ninguna actuación /
1,7 mg/kg
1. Doxiciclina en pienso. Control El Departamento de Agricultura, Alimentación y
sospechoso. 10 +/- 2 mg/kg
1. Oxitetraciclina en pienso.Control El Departamento de Agricultura, Alimentación y
sospechoso. 7.5 +/- 1.8 mg/kg.
1. Oxitetraciclina mas sulfadiazina El Departamento de Agricultura, Alimentación y
en pienso. Control sospechoso. 18 y Acción Rural no realiza ninguna actuación /
7.2 +/- 1.7 mg/kg.
1. Oxitetraciclina mas sulfadiazina El Departamento de Agricultura, Alimentación y
en pienso. Control sospechoso. 20+/- Acción Rural no realiza ninguna actuación /
4 mg/Kg y 6.2 +/- 1.5 mg/kg.
1. Enrofloxacina en músculo. Actuaciones de la Consejería de Sanidad:
Control dirigido.>200 µg/kg
Análisis contradictorio negativo.
Análisis dirimente positivo.
Expediente sancionador resuelto, cuantía de la
sanción 4000 €.
Ganadería:
2. Enrofloxacina en músculo de Actuaciones de la Agencia de Protección de la
pollo. Control dirigido. En los dos Salud.:
casos: Análisis inicial: >150 µg/kg y Comunicación de ambos expedientes a la comunidad
Análisis contradictorio: >150 µg/kg
Autónoma de origen de loa animales.Comunicación a
92
2. Enrofloxacina en músculo.
Control dirigido.>200 µg/kg y .>200
µg/kg
1.
Plomo
hígado.
dirigido:0,92 mg/kg
Control
1. Plomo y 1 Cadmio en hígado.
Control dirigido. Cadmio: 0,71
mg/kg. Plomo: 0,79 mg/kg
la AESAN a través del SCIRI.
Actuación en la Comunidad Autónoma de origen
Iniciación de expedientes y propuesta de resolución.
Comunicaciones al Servicio de Seguridad
Agroalimentaria.
Investigación en granjas
de origen, todos los
animales inmovilizados cautelarmente en la granja
hasta los primeros resultados, 0 animales
sacrificados, 6 meses duración del seguimiento,
muestras tomadas de pienso 4 y agua 5, todas
muestras resultados negativos.
Actuaciones de la Consejería de Sanidad:
Ha resultado positivo en un muestreo de otra partida
de animales.
Estado de tramitación: habiendo resultado infructuosa
las notificaciones se ha publicado el Acuerdo de
Iniciación y Pliego de cargos en Boletín Oficial de la
Comunidad Autónoma.
Ganadería:
Sheep and goat
Renuncia a contradictorio
Investigación en la explotación de las posibles
causas.
Archivo expediente
Comunicación a la Autoridad Competente de origen
y al Vocal del PNIR en la Comunidad Autónoma de
Origen.
Personado el control oficial en la explotación de
origen, se toman muestras de agua y de pienso que se
distribuye a los animales en ese momento, siendo los
resultados conformes. Se censa toda la explotación
que resulta ser de 1.910 cabezas de ovino y 810
cabezas de porcino.
93
3. Sulfadiazina en riñón. Control Actuaciones en matadero en los tres casos:
dirigido.2 con mas de 150 µg/kg y 1 Comunicación al SCIRI.
con 137 µg/kg
Comunicación a las autoridades Competentes de
origen y a los dos Vocal del PNIR de las
Comunidades Autónomas de Origen.
Propuesta de sanción a las explotaciones ganaderas.
Inclusión en relación de explotaciones sospechosas.
Actuación en la primera explotación :
Inspección de la explotación y realización de
investigación pertinente.Se comprobó una inadecuada
utilización de un medicamento autorizado.
Restricción total de movimientos por un periodo no
inferior al periodo de supresión del producto.
Restricción parcial de movimientos desde 3 de agosto
hasta diciembre, permitiendo
movimientos a
matadero con comunicación oficial a destino y
detallando en el documento de acompañamiento que
la explotación está sometida a controles por presencia
de residuos.
Actuación en la segunda explotación ubicada en
una de las CCAA de origen:
Los Servicios Veterinarios Oficiales, realizan visita
de inspección a dicha explotación con las
consiguientes investigaciones pertinentes, referentes
a libro de registro de tratamientos, recetas de
prescripción veterinaria de medicamentos, así como
los controles documentales sobre entradas y salidas
de animales, alimentos, piensos y materias primas
destinadas a la alimentación animal. De todo ello se
levanta el correspondiente Acta de Inspección,
poniendo de manifiesto que el la revisión del libro de
registro de tratamientos se comprueba que existen
dos anotaciones, una con fecha 20/01/2009 y otra con
fecha 13/02/2009 de un pienso medicamentoso que
contiene sulfadiazina. El administrador de la empresa
manifiesta que el pienso medicamentoso se retira con
una antelación mínima de 10 días de ser enviados los
corderos al matadero, pero que por error en el manejo
alguno de los animales ha podido tener acceso a este
pienso sin respetarse el periodo de supresión.
Concluida la investigación se informa al matadero de
las medidas tomadas por la mala utilización del
pienso restringiendo por un periodo de 10 días los
movimientos para sacrificio.Así mismo, durante los
seis primeros
meses, la documentación que
acompañe a los animales al matadero hará mención
expresa de que dicha explotación se encuentra bajo
vigilancia por haber detectado sulfadiazina en alguno
94
2. Sulfadiacina y 2 Clortetraciclina
en riñón. Control dirigido. Las 2
Sulfadiazina con mas de 200 µg/kg y
las 2 Clortetraciclina con mas de 733
µg/kg
2. Sulfadiacina músculo. Control
sospechoso
1. Sulfadiacina y Cortetraciclina en
riñón.Control
dirigido.La
Sulfadiazina con mas de 151 µg/kg y
de los animales de dicha explotación en el ámbito de
actuaciones del Plan Nacional de Investigación de
Residuos, al objeto de proceder a las medidas
contempladas en el artículo 22 del RD 1749/1998.
Actuación en la tercera explotación ubicada en
otra de las CCAA de origen:
Revisión del sistema de autocontrol de la fabricación
de piensos de la explotación.
Visita a la comercial veterinaria de la explotación.
departamento de Salud correspondiente.
Comunicación SCIRI
y Medio Ambiente
Seguimiento en matadero durante tres meses. (***)
Se detecta, en mayo y en junio, Sulfadiazina y
Clortetraciclina por encima del LMR en muestras de
riñón de ovino, ambas muestras procedentes del
mismo cebadero de ovino. Se realiza una encuesta
epidemiológica: con inmovilización cautelar de la
explotación, y toma de muestras de piensos y agua, con
resultado conforme. Se inspeccionó la fábrica de
piensos, donde se detectó incidencias en el control de
calidad de los piensos. El titular administra a los
corderos piensos medicamentosos, que contienen
premezclas medicamentosas con ambos antibióticos, y
que según manifiesta el ganadero, respeta los tiempos
de espera. La explotación se somete a un control
durante seis meses, conforme al artículo 16 del RD
1749/98.
Dichas no conformidades son consecuencia del
citado mas arriba (***). Mismas medidas
Actuaciones en matadero:
Comunicación al SCIRI.
Comunicación a la autoridad Competente de origen y
95
la Clortetraciclina con mas de 900 al Vocal del PNIR en la Comunidad Autónoma de
µg/kg
Origen.
Propuesta de sanción a la explotación ganadera.
Inclusión en relación de explotación sospechosa.
Se procedió a la investigación epidemiológica: se
inmovilizó cautelarmente la explotación se
efectuaron muestras de pienso y agua con resultado
conforme. Se inspeccionó el distribuidor de piensos y
al fabricante de piensos. A los animales se les
administró pienso medicamentoso que contenía como
premezclas medicamentosas ambos antibióticos. Se
establece un incumplimiento de los tiempos de espera
por parte del ganadero.
Actuaciones en explotación: Los Servicios
1. Sulfadiacina y Clortetraciclina
Veterinarios Oficiales, realizan visita de inspección a
en riñón. Control dirigido.La
explotación
con
las
consiguientes
sulfadiacina con mas de 300 µg/kg y dicha
investigaciones pertinentes, referentes a libro de
la Clortetraciclina con mas de 900
registro de tratamientos, recetas de prescripción
µg/kg
veterinaria de medicamentos, así como los controles
documentales sobre entradas y salidas de animales,
alimentos, piensos y materias primas destinadas a la
alimentación animal.
Así mismo, durante los seis primeros meses, la
detectado sulfadiazina y clortetraciclina en alguno de
los animales de dicha explotación en el ámbito de
actuaciones del Plan Nacional de Investigación de
Residuos, al objeto de proceder a las medidas
contempladas en el artículo 22 del RD 1749/1998.
Situación
del
expediente
administrativo:
Sancionada la explotación con 3100 €.
Seguimiento en mataderos: Se sacrifican durante el
periodo de vigilancia un total de 650 animales en
mataderos de nuestra Comunidad, realizándose
análisis a cada partida con resultado conforme.
1. Sulfadiacina en riñón. Control Actuación en la explotación ganadera de la
dirigido. Mas de 300 µg/kg
Comunidad Autónoma de origen
Se procede a la inmovilización de 110 y 87 caprinos
reproductores y 98 corderos. Se procede al sacrificio
bajo control sanitario de un lote de 20 animales,
resultando aptos para el consumo. 17/03/2009.
grave en una cuantía de 3.500 €. Resuelto
1. Sulfadiacina en músculo. Control Investigación en la explotación de ganado ovino,
dirigido.383 µg/kg
verificación de registros de la explotación,
96
1. Sulfadiacina en músculo. Control
dirigido. Más de 150 µg/kg
2 Oxitetraciclina en músculo de
caprino. Control dirigido. En los dos
casos >150 µg/kg
1. Sulfadiacina y Clortetraciclina
en músculo de ovino. Control
dirigido. La sulfadiazina con mas de
150 µg/kg en inicial y contradictorio
y la Clortetraciclina con 122 µg/kg
en inicial, 94 µg/kg en contradictorio
y 142,3 µg/kg en el dirimente
1. Sulfadiacina en músculo de ovino.
Control dirigido. Mas de 150 µg/kg
especialmente de tratamientos veterinarios con
Sulfamidas, procedencia y consumos de pienso y
prescripciones
de
pienso
medicamentoso.
de 438 ovinos y 27 caprinos reproductores y 100
corderos, recogiendo 1 muestras de agua y otra de
pienso medicado detectando la sulfadiacina, entre
otros inhibidores en el pienso medicamentoso. Se
procede al sacrificio bajo control sanitario de los 100
animales de cebo en varios lotes previo muestreo
analítico en el matadero resultando negativos a la
detección de Sulfadiacina.
grave en una cuantía de 3.500 €
Una vez comunicado el positivo, se inmoviliza la
granja, tomando muestras en la misma.
El interesado rechaza el análisis contradictorio
La Delegación Provincial de Salud inicia
procedimiento sancionador
Comunicación y traslado de documentación a la
Agencia Española de Seguridad Alimentaria y
Nutrición (AESAN)
Actuaciones de AESAN:
Comunicación a las autoridades competentes de
Países Bajos ya que la explotación es de dicho país.
Salud.:
Se ha enviado el expediente a la Consejería de
SCIRI.
Personado el Control Oficial en la explotación se
procede a la inmovilización de la misma por un
periodo mínimo de 28 días.
Se toman muestras de pienso y agua de bebida y se
envían a Laboratorios acreditados para la
determinación de sulfadiazina y clortetraciclina,
siendo en ambos casos los resultados conformes.
Se propone desde la Consejeria de Agricultura y
Pesca la exclusión de la citada explotación de la red
de alerta.
Salud.:
Agricultura y a la Unidad de Consumo de "Mossos
d'Esquadra". Comunicación a la AESAN a través del
SCIRI.
97
1. Clortetraciclina en músculo de
ovino. Control dirigido.309 µg/kg
1. Enrofloxacina en músculo de
ovino. Control dirigido. Mas de 200
µg/kg
1. Enrofloxacina en músculo de
ovino. Control dirigido. Mas de 200
muestras: 1 agua y 2 piensos. Todos los resultados
negativos.
Expediente sancionador resuelto, cuantía de sanción
3.005,06 €
Investigación en la explotación ganadera de cebo
de ovino, verificación de registros de la explotación,
especialmente de tratamientos veterinarios con
Clortetraciclina, procedencia y consumos de pienso y
prescripciones de pienso medicamentoso.
2000 corderos, se recogen 3 muestras de pienso (uno
medicado) y una de agua, con resultados analíticos
negativos a inhibidores a excepción del pienso
medicado. Se procede al sacrificio bajo control
sanitario de los animales previo muestreo analítico de
un lote de 21 animales en matadero, resultando
negativos a la detección de clortetraciclina. No se
inicia expediente sancionador ya que la Comunidad
Autónoma que lo detectó no se inhibe por cuestión de
territorialidad.
Estado de tramitación: en periodo de alegaciones al
Pliego de Cargos por infracción grave
Los corderos permanecieron 3 días en el matadero.
Se realizó la investigación epidemiológica:
inmovilización cautelar de la explotación, toma de
muestras de piensos y agua, con resultado conforme
en el Laboratorio correspondiente. Que el titular
administra a los corderos piensos medicamentosos
(correctamente recetados y dispensados) que
contienen otros antibióticos, pero ninguno con
enrofloxacina. Que tanto en este caso, como en otro
positivo a enrofloxacina, también detectado en el
mismo matadero, el entrador (y gestor del matadero)
fue el mismo, y manifiestan que dicho señor también
dispone de un cebadero de corderos próximo al
matadero.
98
µg/kg
Estado de tramitación: no ha sido localizado el
responsable en la dirección disponible. El expediente
se halla en publicación en Boletín oficial autonómico
de Pliego de Cargos por infracción grave.
Se realiza una investigación epidemiológica:
inmovilización cautelar de la explotación, toma de
muestras de piensos y agua, con resultado conforme
en el Laboratorio correspondiente. Que los animales
estuvieron 3 días en el matadero antes de su
sacrificio. El ganadero alimenta a los corderos con
piensos medicamentosos (correctamente recetados y
dispensados) que no contienen en sus premezclas
medicamentosas la enrofloxacina. Que tanto en este
caso, como en otro positivo a enrofloxacina , también
detectado en el mismo matadero, el entrador (y gestor
del matadero) fue el mismo, y manifiestan que dicho
señor también dispone de un cebadero de corderos
próximo al matadero.
Milk
Horses
Investigación en la explotación de las posibles
causas.
Archivo expediente
Investigación en la explotación de las posibles causas
Archivo expediente
6. Cadmio Hígado. Control dirigido
Actuaciones del Departamento de Salud
y Medio ambiente
Seguimiento en matadero durante 3 meses
1. Dihidroestreptomicina en riñón. Actuaciones del Departamento de Salud:
Control dirigido
Comunicación SCIRI
y Medio Ambiente
Seguimiento en matadero durante tres meses.
Actuaciones del Departamento de Desarrollo
Rural y Medio Ambiente:
Visita a la explotación comprobando que no se ha
respetado el periodo de supresión e inmovilización
cautelar de la misma.
1 Cadmio en hígado. Control Comunicación al servicio de Ganadería.
1. Cadmio hígado .Control dirigido:
2.0 mg/kg
1 Cadmio riñón. Control dirigido: >2
mg/kg
99
dirigido.1,99 mg/Kg.
Actuaciones del servicio de Ganadería:
Inspección del libro de registro de tratamientos y se
levantan actas de control de alimentación animal.
Al mismo tiempo se procede a la toma de muestras
de pienso, alfalfa y agua, cuyos análisis dieron
negativo a la presencia de metales pesados.
La explotación se incluye en el plan de controles de
la alimentación animal durante el año 2009.
3. Cadmio
en riñón. Control Actuaciones de la Agencia de Protección de la
dirigido.4,8 mg/kg, 22,6 mg/kg y Salud.:
1,221 mg/kg
Comunicaciones al Departamento de Medio
Ambiente correspondiente.
Eggs
Rabbit
1. Oxitetraciclina en pienso. Control Investigación en granja y propuesta de expediente
dirigido.
sancionador.
Contaminación cruzada en la explotación por mala
manipulación accidental en el almacenamiento.
Apertura de expediente.
1. Oxitetraciclina en músculo. Actuaciones de la Agencia de Protección de la
Control dirigido. >150 µg/kg
Salud.:
Agricultura y a la Unidad de Consumo de "Mossos
d'Esquadra". Comunicación a la AESAN a través del
SCIRI.
1
Explotación
visitada.
Comprobación
de
Aquaculture
2. Arsénico en músculo. Control Comunicación al Departamento de Medio Ambiente
dirigido.0, 390 µg/kg y 1,777. µg/kg
correspondiente
Farmed game
2. Cadmio en Hígado jabalí. Control
dirigido
3. Sulfatiazol .Control dirigido
(primer caso >25 µg/kg, segundo
caso >6,1 µg/kg y tercer caso 10,6
µg/kg)
Wild game
Comunicación al departamento de Desarrollo Rural y
Medio Ambiente.
Honey
Salud.:
fiscalía. Seguimiento de los productos elaborados de
los mismos lotes.Comunicación al Departamento de
100
3 Explotaciones visitadas (1895 enjambres). Toma de
3 muestras de miel. Pendientes de resultados.
101
FI
FINLAND
Group A substances
Modifications 2009 2010
• A1: Stilbenes are added to the plan of horses and fish GC-MS / GC-MS
• A2: Thyreostats are added to plan of horses and poultry LC-MS-MS /LC-MS-MS
• A4: Zeranol is added to the plan of horses Elisa /GC-MS
• A5: Beta-agonists are added to the plan of horses LC-MS-MS / LC-MS-MS
• A6: Nitroimidazoles are added to the plan of horses. GC-MS-MS /GC-MS-MS
• Chloramfenicol and nitrofuranes of all matrixes LC-MS-MS/LC-MS-MS
• Some changes are made due to changes in production numbers
• The missing information on CC-alfa and CC-beta are added to the plan
• LC-MS LC-MS-MS
Follow-up actions
One urine sample of pig was noncompliant for
17-beta-19-nortestosteron
(224 µg/kg)
Due to the non-compliant result official control
actions have been carried out. On the spot control
was made by the local municipal veterinarian. The
record (medicinal product) has been checked. Two
additional samples (urine/pigs) were taken for futher
testing and these samples were compliant. No
violation of medication was detected. According to
the investigations the sample was taken from a
cryptorchid animal (= information on the sampling
form).
Group B substances
Modifications 2009 2010
• B1: Beta-lactams are added to the plan of horses HPLC-fluo/HPLC-fluo
• Tetracyclines are added to the plan of pig HPLC-UV/HPLC-UV
• Kinolones are tested insteadt of streptomycins in milk HPLC-fluo/HPLC-fluo
• Sulfonamides in fish, farmed game and honey
new metods HPLC-UV / HPLCUV
• Tetracyclines and tylosin in honey nem methods LC-MS-MS / LS-MS-MS
• B2b: Toltrazurilsulfon is added to the plan of horses HPLC-UV / LC-MS-MS
• Coccidiostats are added to the plan of bovine and pigs feed samples LC-MS-MS /
LC-MS-MS. Eggs and farmed game LC-MS-MS. /LC-MS-MS
• B2c: Permethrin is added to the plan of horses GC-MS / GC-MS
102
•
•
•
•
•
•
•
•
•
•
•
•
B2d: Xylazine is added to the plan of horses HPLC-DAD/HPLC-DAD
B2e: Flunixin, phenylbutazone and oxphenylbutazone new method LC-MS-MS
/LC-MS-MS
B2f: Dexamethasone and prednisolone are added to the plan of horses Elisa/LCMS-MS.
B3a: The organochlorines are added to the plan of horses GC-ECD / GC-ECD
(incl. PCB-congeners). The group of organochlorines in eggs is enlarged GC-MSMS/ GC-MS-MS. Chlordimeform in honey new method GC-MS / GC-MS
B3b: Organophosphors are added to the plan of horses GS-MS/GC-MS
The group of organophosphors in eggs is enlarged GC-MS-MS /GC-MS-MS
B 3d: Ochratoxin is added to the plan of horses HPLC-fluo/HPLC-fluo (method
changed also for other species)
Some changes are made due to the changes in production numbers
The goat milk samples are added to the plan for the groups B1 and B3d
The number of coccidiostat analyses in eggs is increased due to non-comliant findings.
The number of farmed game samples will be at the same level as 2009 (even there
were non-compliant reindeer liver and kidney)
The number of wild game samples will be at the same level as 2009 (even there were
non compliant elks liver and kidney)
Follow-up actions
Bovines
No
-Pigs
Suspect:
Two suspect samples of one pig were
non-compliant for oxytetracycline
(muscle 1.08 mg/kg and kidney 13.2
mg/kg)
Two meat control samples of one pig were send for
the confirmation due to the positive microbiological
test results in the slaughterhouse. Official
investigations in the farm of origin, checks of
medicinal product records, no additional samples
have been taken, the carcass has been declared unfit
for human consumption. The possible reason for the
source of the residue was some misunderstanding
between the owner and the assisting personnel in
farm.
Poultry
no
Sheep and goat
no
Horses
no
Milk
One egg sample was non-compliant
Eggs
Investigations on the farm of origin, verification of
103
for salinomycin ( 3,8 µg/kg)
records (medicinal products and feed). No additional
samples were taken because there were neither
animals nor eggs left on the farm at the time of
control. No violation of medication was detected. The
source of residue was not found.
One egg sample was non-compliant
for naracin (3.8 µg/kg)
Investigations on the farm of origin, verification of
records (medicinal products and feed). Additional
samples were taken. The sample of eggs was
compliant. The sample of feed contained narasin 48
µg/kg (< MRL for feed). No violation of medication
was detected. The possibility of contaminated feed
could not be excluded.
Rabbit
no
Aquaculture
no
Farmed game
5/9 liver samples and 7/9 kidney
samples of reindeer were noncompliant for cadmium.
11/ 19 liver samples and 14 / 19
kidney samples of elk were noncompliant for cadmium. 1/7 liver
samples and 4/6 kidney samples of
wild deer were non-compliant for
cadmium
Wild game
According to Finnish legislation livers and kidneys of
over one year old elks are not accepted for human
consumption.
Honey
no
104
FR
FRANCE
Group A substances
En France, toute mise en évidence de substances interdites par une DDSV (direction
départementale des services vétérinaires) doit être transmise à la Brigade Nationale
d’Enquêtes Vétérinaires et Phytosanitaires (BNEVP) qui mène les enquêtes et informe
les autorités juridiques. Dans le but de démanteler des trafics de substances interdites, les
enquêtes sont longues et les rapports ne parviennent à la DGAL (Direction Générale de
l’Alimentation) qu’une fois l’affaire jugée (secret de l’instruction).
Tous les élevages et établissements ayant eu des résultats non conformes au cours des
plans de contrôle 2009 seront ciblés prioritairement pour les plans 2010.
Follow-up actions
Substance--Matrix-animal or animal Actions: (investigations in the farm of origin,
product-Concentration*
Example: MPA-kidney fat-pig-3 ppb intensified sampling in related farms, products
La Brigade Nationale d’Enquêtes Vétérinaires et
6 Thiouracil– bovin – ferme – 3
Phytosanitaires (BNEVP) a été informée de ces
dont la quantification a été
précisément rapportée : 6,1 µg/L ; résultats non conformes. La présence de ces
molécules, en faibles concentrations, pourraient
8,8 µg/kg ; 6,8 µg/kg ; autres
être dues à la consommation par les animaux de
résultats compris entre 5 et 10
plantes Crucifères.
µg/kg
5 Thiouracil – bovin – abattoir – La Brigade Nationale d’Enquêtes Vétérinaires et
2 dont la quantification a été
précisément rapportée : 8,8 µg/L résultats non conformes. La présence de ces
; 7,0 µg/L ; autres résultats
compris entre 5 et 10 µg/kg
1 Thiouracil – urine – porcin –
abattoir – 6,0 µg/kg
résultats non conformes. La présence de ces
1 Thiouracil – urine – ovin –
abattoir – 19,4 µg/L
La BNEVP a été informée de ces résultats non
2 Nandrolone – urine bovin –
105
abattoir - 3,6 µg/kg ; 2,2 µg/kg
12 β-nandrolone – urine – porcin
– entre 1 et 10 µg/kg
conformes. Des enquêtes sont en cours.
conformes. Des enquêtes sont en cours, ainsi que
des études basées sur la compilation des résultats
des années précédentes.
1 Zéranol + Taléranol – urine Phytosanitaires (BNEVP) a été informée de ces
bovin – ferme - 2,5 µg/kg + 3
µg/kg
molécules pourraient être dues à la consommation
par les animaux de fourrages contaminés par des
mycotoxines.
16 Zéranol + Taléranol – bovin – La Brigade Nationale d’Enquêtes Vétérinaires et
abattoir – résultats quantitatifs
compris entre 1 µg/kg et 3 µg/kg
molécules pourraient être dues à la consommation
par les animaux de fourrages contaminés par des
mycotoxines.
La BNEVP a été informée de ce résultat. Une
1 Chloramphénicol – muscle enquête est en cours. La très faible contamination
bovin – abattoir – 0,07 µg/kg
relevée peut laisser penser à des hypothèses autres
que la fraude.
3 chloramphénicol – muscle –
porcin – 0,04 µg/kg ; 0,14 µg/kg ; conformes. Des enquêtes sont en cours. Les très
faibles contaminations relevées peuvent laisser
0,1 µg/kg
penser à des hypothèses autres que la fraude.
3 Hydroxymétronidazole – muscle La BNEVP a été informée de ces résultats non
conformes. Des enquêtes sont en cours. Les très
– porcin – 1,5 µg/kg ; 0,3 µg/kg ;
faibles contaminations relevées peuvent laisser
0,4 µg/kg
penser à des hypothèses autres que la fraude.
La BNEVP a été informée de ce résultat. Les
1 17-β-estradiol – foie – poule de
connaissances relatives aux niveaux
réforme – 7,65 µg/kg
physiologiques de cette substance dans les foies de
volailles sont partielles. Il est donc difficile
d’établir un « seuil de non-conformité ». De plus,
les concentrations sont trop faibles pour réaliser
une confirmation basée sur la spectrométrie de
masse de rapport isotopique de manière à
différencier une administration d’une production
endogène.
1 boldénone méthyl – foie – truite La BNEVP a été informée de ces résultats non
conformes. Des enquêtes sont en cours.
arc-en-ciel – > 1 µg/kg
Group B substances
La quasi totalité des élevages ou entreprises ayant fait l’objet d’un résultat non conforme
fera l’objet d’un nouveau contrôle par les agents des services déconcentrés pour l’année
2010.
106
1 antibiotique – muscle - bovin
1 Pénicilline G – muscle – bovin –
2635 µg/kg
1 Chlortétracycline – muscle –
bovin – 842 µg/kg
14 Oxytétracycline – muscle
bovin – 252 µg/kg ; 352 µg/kg ;
528 µg/kg ; 169,5 µg/kg ; 671
µg/kg ; 600 µg/kg ; 551 µg/kg ;
337 µg/kg ; 777 µg/kg ; 400
µg/kg ; 287 µg/kg ; 21910 µg/kg ;
113 µg/kg ; 122 µg/kg
2 Tétracycline – muscle – bovin –
147,5 µg/kg ; 100 µg/kg
1 Tétracycline + Tylosine –
muscle – muscle bovin – 195
µg/kg + 33 µg/kg
1 Doramectin – foie – bovin – 10
µg/kg
Follow-up actions
Bovines
Déclaration de résultat non-conforme par le
laboratoire erronée : échantillon non-analysable
Un rappel à la réglementation a été adressé à
l’éleveur.
l’éleveur.
Cas à 337 µg/kg : ordonnance vraisemblablement
incomplète ayant conduit l’éleveur a surdosé le
médicament ce qui serait à l’origine de la NC
malgré le respect du temps d’attente. Un courrier
de rappel a été envoyé au vétérinaire traitant.
Cas à 169,5 µg/kg : suite à une injection de
tétracyclines le temps d’attente de 15 j n’a pas été
respecté. Une inspection en pharmacie vétérinaire
a été menée dans l’élevage et un rappel à la
réglementation signifié à l’éleveur
Cas à 400 µg/kg : l’animal, un taureau de 5 ans, a
été abattu et à fait l’objet d’une saisie totale pour
endocardite fibrineuse, arthrite unique et myosite
localisée (590 kg). L’inspection en pharmacie
vétérinaire menée à la suite de ce résultat a montré
de nombreuses anomalies notamment dans la tenue
des registres et l’enregistrement des ordonnances.
Le taureau en question apparaît avoir été traité
sans ordonnance avec un restant de flacon destiné
à un autre animal. Un dossier a été transmis au
procureur de la République pour tromperie.
L’élevage sera contrôlé au titre de la
conditionnalité en 2011. Un rappel réglementaire a
également été adressé au cabinet vétérinaire
responsable du suivi de cet élevage et il sera
également inspecté en 2011.
Dans la plupart des autres cas, il a été mis en
évidence un non respect du temps d’attente. Un
rappel à la réglementation a été adressé à l’eleveur.
Cas à 147,5 µg/kg : une inspection en pharmacie
vétérinaire a été menée dans l’élevage impacté.
L’éleveur a fait l’objet d’un rappel réglementaire
concernant l’enregistrement de l’ensemble des
traitements.
Cas à 100 µg/kg : Un rappel à la réglementation a
été adressé à l’eleveur.
l’eleveur.
l’eleveur.
107
1 moxidectin – foie – bovin – 230
µg/kg
1 Diclofenac – muscle – bovin –
9,3 µg/kg
2 Prednisolone – foie – bovin – 4,5
µg/kg ; 2,45 µg/kg
1 Prednisolone – poil – bovin >8,25 µg/kg
1 Cadmium – muscle – bovin –
120 µg/kg
2 oxytrétracycline – muscle –
porcin - 1295 µg/kg ; 200 µg/kg
2 prednisone + prédnisolone –
poil – porcin - > 4 µg/kg et
>8µg/kg ; > 8,25 µg/kg et >7,9
µg/kg
1 Cadmium – muscle – porcin –
103 µg/kg
1 oxytétracycline – muscle –
poulet réforme
l’eleveur.
l’eleveur.
l’eleveur.
l’eleveur.
L’élevage sera prélevé à nouveau lors des plans
2010.
Pigs
Cas à 200 µg/kg : l’inspection de l’élevage en
pharmacie vétérinaire a montré qu’un traitement
avait été administré mais que le temps d’attente
avait été a priori respecté. Toutefois, l’élevage ne
tenait pas de registre de soins. Un rappel à la
réglementation lui a été adressé.
Une inspection en pharmacie vétérinaire a été
menée dans l’élevage d’où le porc était issu. Il a
été constaté de nombreuses anomalies relatives à
la réglementation de la pharmacie vétérinaire en
élevage. Toutefois, cela n’a pas permis d’identifier
l’utilisation de cette molécule sur le lot d’animaux
auquel appartenait l’animal incriminé.
2010.
Poultry
Cause détectée : non respect du temps d'attente
avec envoi d'animaux sous traitement antibiotiques
(problème organisationnel de filière avec gestion
de l'alimentation et de l'enlèvement par le
propriétaire du lot). Le lot de reproducteurs chair a
été réformé de manière anticipée par le
propriétaire alors qu'il était encore sous traitement
antibiotique. L'éleveur n'a pas réagi.
Autres anomalies relevées :
Eleveur : suite à inspection en pharmacie
vétérinaire : insuffisance d'enregistrement des
traitements, registre non ordonné, quelques
documents manquants et non respect des règles de
prescriptions (durée de traitement) : rapport et
courrier de rappel à la réglementation
Vétérinaires : insuffisance sur les prescriptions
détectées et sur les règles de délivrance par rapport
aux prescriptions : rapport et courrier en lien avec
une visite déjà faite au cabinet (mise en demeure
sur le cabinet)
Usine d'aliment : rappel réglementaire sur les
délivrance avec programmation de contrôle en
108
4 maduramycine – foie – poulet
de chair – 1,5 µg/kg ; 2,6 µg/kg ; 2
µg/kg ; 3,3 µg/kg
2 maduramycine – foie – dinde –
6,1 µg/kg ; 48,7 µg/kg
21 nicarbazine – foie – poulet de
chair – 16 échantillons entre 4,9
µg/kg et 99,7 µg/kg ; 176,2 µg/kg ;
110,9 µg/kg ; 106,8 µg/kg ;
106,4 µg/kg ; 1355,9 µg/kg
1 oxytétracycline – muscle –
caprin – 139 µg/kg
2 sulfadiméthoxine – muscle –
ovin 208 µg/kg ; 241 µg/kg
1 sulfadiméthoxine + sulfadiazine
muscle – ovin – 109 µg/kg + 12
µg/kg
1 Diazinon – muscle – ovin – 69,7
µg/kg
1 Cadmium – muscle – cheval –
400 µg/kg
2010 sur les Bonnes pratiques de Fabrication et de
distribution de l'aliment
Les enquêtes menées sur les élevages pour
lesquels des non-conformités en anticoccidiens ont
été relevés ont fait l’objet d’inspections en
pharmacie vétérinaire.
Pour une majorité d’entre eux, il n’a pas été relevé
d’anomalie majeure. Une contamination croisée
d’aliments blancs par des aliments médicamenteux
est possible (au stade du transport, de l’élevage ou
de la fabrique). Il semblerait que des débris
d’aliment supplémentés puissent se retrouver dans
les assiettes, et se mélanger avec les aliments
blancs. C’est hypothèse semble assez cohérente et,
dans certains départements, les éleveurs travaillent
une amélioration de leurs pratiques pour supprimer
ces contaminations croisées.
Les élevages en cause seront prélevés
prioritairement lors du plan 2010.
Sheep and goat
Suite à ce résultat et au vu de l'historique de
l'élevage (problème de
pleuro-pneumonies) et en l'absence d'une
traçabilité fiable de
l'abattoir, la DDSV :
1/ a considéré l'ensemble des chevreaux issus de
cet élevage et abattus
le même jour comme un seul lot,
2/ a fait retirer les restes de viandes congelées
issues de ces
animaux encore disponibles au niveau de l'abattoir
(autour de 170 kg).
Une enquête a été menée en élevage.
Un rappel à la réglementation a été adressé aux
éleveurs.
Suite à ce résultat, une enquête a été menée par la
DDSV concernée. Des animaux, normalement
destinés à être prochainement abattus, auraient
accidentellement été mélangés avec des animaux
traités avec un aliment médicamenteux et auraient
donc pu manger cet aliment. Un rappel à la
réglementation a été signifié à l’éleveur.
l’éleveur.
Horses
Une enquête a été menée autour de l'élevage pour
identifier d'éventuelles causes de la nonconformité et celui-ci sera prélevé à nouveau lors
des plans 2010.
109
1 Fenbendazole – lait d’ovin – 74
µg/kg
1 Chlorpyrifos éthyl – lait de
caprin – 11,9 µg/kg
1 plomb – lait de bovin – 163
µg/kg
1 sulfadiméthoxine – oeuf de
poule – 27,150 mg/kg
3 dinitrocarbanilide – œufs de
poule – 1,35 µg/kg ; 2,8 µg/kg ; 8
µg/kg
Milk
l’éleveur.
La LMR étant de 10 µg/kg et le résultat donné par
le laboratoire non corrigé en tenant compte de
l’incertitude de mesure, il n’a pas été donné suite à
cette non-conformité.
2010.
Eggs
Ce taux très élevé serait dû au prélevement d’œufs
lors d’un traitement. En effet, l’enquête a montré
qu’un traitement de 5 jours a été effectué suite à
des résultats d’autopsies demandées par l’éleveur.
Le registre d’élevage a montré l’enregistrement de
ce traitement mais il semble que ces mentions
n’aient pas été de suite inscrites car lors du
prélèvement fait par le technicien, seule
l’information de la responsable indiquant que les
œufs n’étaient pas mis à la consommation, lui a été
donnée. De ce fait, les analyses ont été demandées
quand même.
Le temps d’attente de 12 jours a été respecté selon
les indications ; cependant le décompte a été fait à
partir du premier jour de traitement et non pas à la
fin.
Cependant les œufs (175 000) auraient été détruits,
selon les dires de l’éleveur, sur les champs et n’ont
pas été envoyés à l’équarrissage. Le nombre
d’œufs indiqués sur le registre est imprécis. Un
décompte a été refait ensuite en fonction des
relevers de ponte.
L’historique des bons de livraisons a été remis lors
de la visite sur place. Une enquête a été faite
auprès de la casserie et les détails des livraisons
envoyés ; aucune livraison n’a été réalisée vers la
casserie lors de la période incriminée.
Un rapport de visite et une lettre
d’accompagnement ont été envoyés à la suite et
concernaient aussi d’autres non conformités dont
une livraison d’aliments médicamenteux sans
ordonnance par un fabricant d’aliments.
Pas d’action car entrée en vigueur au 1er juillet
2009 du « RÈGLEMENT (CE) No 124/2009 DE
LA COMMISSION du 10 février 2009 établissant
des valeurs maximales pour la présence dans les
denrées alimentaires de coccidiostatiques ou
d'histomonostatiques résultant du transfert
inévitable de ces substances vers des aliments pour
110
2 nicarbazine – œufs de poule – 2
µg/kg ; 16 µg/kg
1 lasalocide – œuf de caille – 213
µg/kg
5 Sulfadiméthoxine – muscle –
lapin – 122 µg/kg ; 142 µg/kg ;
901 µg/kg ; 1542 µg/kg ; 2120
µg/kg
animaux non cibles » et valeur très inférieure à la
limite de 100 µg/kg prévue par ce réglement
Pas d’action car entrée en vigueur au 1er juillet
2009 du RÈGLEMENT (CE) No 124/2009 DE LA
COMMISSION du 10 février 2009 établissant des
valeurs maximales pour la présence dans les
denrées alimentaires de coccidiostatiques ou
d'histomonostatiques résultant du transfert
inévitable de ces substances vers des aliments pour
animaux non cibles et valeur très inférieure à la
limite de 100 µg/kg prévue par ce réglement
l’éleveur.
Rabbit
Cas à 901 µg/kg : Une enquête a été menée dans
l’élevage concerné. Il n’a pas été relevé
d’anomalie majeure dans cet élevage. L’usine
d’aliments ayant livré l’élevage a fait l’objet d’une
inspection qui n’a pas révélé d’anomalie. Une
analyse sur l’aliment blanc livré n’a pas mis en
évidence de contamination croisée.
Une contamination croisée non homogène
d’aliments blancs reste néanmoins possible.
Cas à 2120 µg/kg : Une enquête en pharmacie
vétérinaire a été menée dans l’élevage. D'après les
déclarations de l'éleveur, ce prélèvement fortement
positif serait de nature accidentelle. Il reconnaît
une possibilité d'erreur dans la distribution
d'aliment médicamenteux destiné aux lapines, en
lien avec le transfert précipité de lapins
d'engraissement 2 jours avant leur départ pour
l'abattoir. Cette hypothèse est compatible avec la
dose élevée de sulfadimétoxine trouvée dans le
muscle (2 120 µg/kg).
L'anomalie « non respect du délai d'attente à une
seule reprise » a été retenue dans le compte-rendu
de contrôle sur place paquet
hygiène/Conditionnalité 2009, ce qui est
susceptible d'entraîner une pénalité de 1% de ses
primes PAC 2009.
L'erreur étant de nature accidentelle, il n'a pas été
dressé de procès-verbal.
Cas à 122 µg/kg : l’information sur la chaîne
alimentaire ne montre aucun élément de suspicion
(mortalité normale, pas de pathologie ni de
traitement mentionnés). L'aliment supplémenté a
été arrêté dans les délais conformes. Aucune
anomalie majeur n’a été mise en évidence lors de
l’inspection de l’élevage pour la pharmacie
vétérinaire. Une contamination croisée d’aliments
111
blancs reste possible.
La traçabilité de l'abattoir et de la découpe est faite
à la journée. Le listage des produits restants
congelés montre qu'il reste 20,18 kg de découpe de
lapin et 57,00 kg de gigolette de lapin.
Ces produits ont été consignés et détruits
(enlèvement C2).
1 Sulfadiméthoxine +
benzosulfonamide 97 µg/kg + 65
µg/kg
1 Cadmium – foie – lapin – 560
µg/kg
3 Cadmium – foie – grand gibier
– 700 µg/kg , 1252 µg/kg, 1,22
µg/kg
1 HCH-α – muscle – grand gibier
– 304 µg/kg
4 Plomb – miel – 140 µg/kg ; 170
µg/kg ; 330 µg/kg ; 890 µg/kg
1 oxytétracycline – miel – 15,6
µg/kg
Ces élevages seront prélevés prioritairement lors
du plan 2010.
Une enquête a été menée en élevage et, hormis un
manque de rigueur de l’éleveur dans la conduite de
son élevage (activité arrêtée le 01/05/2009), il n’a
pas été établi de lien entre la non-conformité et la
conduite de l’élevage.
Par contre, le risque de contamination croisée au
niveau de l’usine d’aliment n’est pas totalement
maîtrisé. Toutefois, cette usine a cesser
l’incorporation de sulfamides dans les aliments
d’engraissement pour lapins au 1er juillet, ce qui
devrait améliorer ses résultats aux tests de
contamination croisée.
2010.
Wild game
Pas d’action sur les gibiers de chasse
Pas d’action sur les gibiers de chasse
Honey
Les apiculteurs concernés seront prélevés en
priorité dans le cadre du plan de contrôle 2010.
Les apiculteurs concernés seront prélevés en
priorité dans le cadre du plan de contrôle 2010.
112
GR
GREECE
GREECE
Member State
Modifications of the NRCP 2010 were performed mostly, due to the following
reasons:
1) An extended redistribution of the samples, between the NRCP laboratories took
place, in order to facilitate their work, by fully exploiting their existing
capabilities in personnel and expendables.
2) The new NRCP for 2010 requires the minimum no of samples to be
collected(plus 10%) as a reserve. (The fact that, a large number of extra
samples were requested for the 2009 NRCP, instead of the minimum required
according to the national production, created a serious nuisance to local
producers, which was expressed by complaints to the sample collectors;
furthermore the examination of a large number of extra samples except been
very costly, created a serious accumulation problems in the laboratories and
many deficiencies in expendables).
Mycotoxine/ochratoxine – Kidney
(4 samples)
Soulfadimidine– Meat/Kidneys
(3 samples)
Follow-up actions
Pigs
Investigation of feed. The results of the
investigation were negative. No administrative
measures were taken
- Quarantine
-
Heavy Metals-Meat
(1 sample)
Nitrofurans - Meat
(1 sample)
Heavy metals (Kd) – Liver
(4 samples)
Aflatoxine – Bovine
(3 sample)
Heavy metals –
(3 samples) 1 bovine, 2 sheep
Additional sampling with negative results
Poultry
investigations in the farm of origin, additional
sampling with negative results;
Investigation on the farm, new sampling with
negative results.
Sheep and goat
-investigations in the farm of origin
-investigation of feed.
- The results of the investigation were negative.
No administrative measures were taken.
Milk
- investigations in the farm of origin,
- additional sampling;
- destruction of feed
- Quarantine animals held in the farm,
- intensified milk sampling
- investigations in the farm of origin,
- additional sampling;
- Feed examination, no results
Aquaculture
113
Malachite Green-Flesh-Fish-n.a
(9 samples)
Heavy Metals (Pb)
(1 sample)
Chlorotetracycline-Honey(1 sample)
Sulfathiazole-Honey(1 sample)
-
investigations in the farm of origin,
-
intensified checks
-
additional sampling
-
administrative measures(fine),
-
denial of EC aid.
-
Prohibition of fishing in the suspect area.
Honey
- The infected butch was confiscated and
destroyed; an investigation in the farm of
origin took place; Quarantine was
established.
-
The results of the investigation were
negative. No administrative measures were
taken
-
investigations in the farm of origin; no
indications of the suspect substance were
found.
-
Suspect sampling was performed.
114
HU
HUNGARY
Group A substances
According to the FVO recommendations and CRL comments we have modified the annual
2010 plan
Follow-up actions
There was no non-compliant results
Group B substances
Follow-up actions
Bovines
Bovine –muscle and liver-inhibitors: - additional sampling
- administrative measures,
Amoxicillin, 2 pc
- modifications of the NRCP of 2010
Bovine kidney: Cadmium Cd, 2pc
Pigs
- additional sampling
Pig plasma: progesterone, 1pc
Pig muscle: metronidazole, 1pc
Pig kidney Gentamycin 1 pc
Poultry
Turkey liver: enrofloxacin, 1pc
Sheep and goat
sheep kidney: Cadmium Cd, 1pcs
Horses
Milk
Eggs
Rabbit
115
Aquaculture
Farmed game
wild board muscle: Lead Pb, 2pcs
Honey: Sulphadimethoxin 1 pc
Wild game
Honey
116
IE
IRELAND
Group A substances
Analysis for Ethynlestradiol in live bovines and Nitromidizoles in milk and honey have been
added to the 2010 plan
Follow-up actions
15 non-compliant results
Bovines
11
target samples confirmed non-compliant for
• Thyrostats –Thiouracil
Thiouracil at the following levels:
• Urine
• 11 Non-Compliant results
(1) 38.2µg/kg (2) 4.5µg/kg (3) 13.4µg/kg
(4) 19.8µg/kg (5) 16.8µg/kg (6) 1.6µg/kg
(7) 25.2µg/kg (8) 87.4µg/kg (9) 8.1µg/kg
(10) 27.1µg/kg (11) 33ug/kg
A follow up investigation was initiated at farm level
in all cases and no evidence of illegal use was
identified. In line with scientific evidence, the
Competent Authority has concluded that the residues
resulted from dietary factors.
•
•
•
Nitrofurans- Nitrofurazone as
SEM
Plasma
4 Non-Compliant results
4 target samples confirmed non-compliant for
Nitrofurazone as SEM at the following levels:
(1) 0.14µg/kg, (2) 0.32µg/kg, (3) 0.09µg/kg,
(4) 0.110µg/kg
Follow up investigations were initiated at the farms
of origin in all cases and no evidence of illegal use
was identified. In line with scientific evidence, the
resulted from extraneous factors.
9 Non- Compliant results
Pigs
117
•
•
•
Thyrostats- Thiouracil
Urine
9 Non-compliant results
(1) 1.8µg/kg (2) 3.0µg/kg (3) 12.0µg/kg
(4) 2.5µg/kg (5) 3.0µg/kg (6) 0.9µg/kg
(7) 6.5µg/kg (8) 3.3µg/kg (9) 2.6µg/kg
•
•
•
Thyrostats-Thiouracil
Urine
Ovine
(1) 7.3µg/kg (2) 31.9µg/kg (3) 1.3µg/kg
(4) 20.0µg/kg (5) 12.6µg/kg (6) 5.4µg/kg
(7) 0.9µg/kg
•
•
•
Nitrofurans-Nitrofurazone as
SEM
Liver
Nitrofurazone as SEM at the following levels:
(1) 0.172µg/kg, (2) 0.122µg/kg, (3) 0.182µg/kg,
(4) 0.2582µg/kg
resulted from extraneous factors.
Aquaculture
118
4 non-compliant farm finfish
samples for Leuco Malachite green
This substance is not authorised as an animal
remedy, and does not have an established MRL. The
reporting limit for the purposes of the Irish NRMP is
1µg/kg. As part of 2009 monitoring, 3 routine target
samples of freshwater trout from one farm were
found to have Leuco malachite Green (LMG)
present; levels were between 0.6 – 0.99µg/kg. These
levels were below the reporting limit of 1µg/kg for
LMG and were therefore reported as compliant. An
investigation was initiated including an on –farm
investigation. A legal notice under national
legislation, was issued to restrict the movement of
fish off the farm. Follow-up samples were taken
from fish and sediment throughout the farm. Of 14
suspect samples taken 4 confirmed positive for LMG
at levels of 1.2, 1.8, 2.5 & 20.8 µg/kg while 3 of the
samples had levels below the reporting limit of
LMG. All stock from the pond that had the level of
20.8 µg/kg of LMG was culled. Recent sampling has
shown no further non-compliances and movement
restrictions were removed. A programme of
enhanced monitoring is ongoing at that farm.
Group B substances
• NSAID analysis in porcine tissue has been added to the plan.
• Sampling of anthelmintics in the bovine milk sector has increased due to the incidence of noncompliant results in 2009.
Follow-up actions
Bovines
Suspect samples
• Antimicrobials
9 suspect samples confirmed non-compliant for antimicrobial
• Muscle
• 9 non-compliant results* substances as follows:
• 5 x Oxytetracycline
(1 @ 900µg/kg, 2 @ >500µg/kg,
2 @ >200µg/kg)
• 1 x Enrofloxacin @ 150µg/kg
• 1 x Tilmicosin @ >250µg/kg
• 2 x Amoxicyllin @ >100µg/kg & 62.8µg/kg
All suspect carcases declared unfit for human consumption and
destroyed. Full on farm investigations including examination of
medicines on farm and animal remedies record were carried out in
each case. As appropriate, advice is given to the farmer and
follow-up visits take place.
• Antimicrobials
• Muscle
Pigs
Suspect Samples
2 suspect samples confirmed non-compliant for antimicrobial
119
•
3 non-compliant result*
substances as follows:
• 1 x Oxytetracycline at a level >500µg/kg
• 1 x Marbofloxacin at a level of 660µg/kg
Target Samples
1 target sample confirmed non-compliant for
Trimethroprim @ >100µg/kg & Sulfadiazine @
>200µg/kg.
All suspect carcases are declared unfit for human consumption,
destroyed and excluded from the food chain. Full on farm
investigations including examination of medicines on farm and
animal remedies record were carried out in each case. As
appropriate, advice is given to the farmer and follow-up visits take
place.
•
•
•
OC’s & PCB’s
Fat
• Anticoccidials
• Liver
• 9 non-compliant results
•
•
•
NSAID’s
Plasma
1 non-compliant result
• Anthelmintics
• Liver
• 6 non-compliant
results*
3 suspect samples associated with the dioxin incident in this
sector in late 2008, confirmed positive for PCB’s and Dioxins in
early 2009. All carcases were destroyed and excluded from the
food chain.
Poultry
9 Target Broiler samples confirmed non-compliant for Nicarbazin
above the ad-hoc national level of 228µg/kg. The levels found
ranged from 240µg/kg to >500µg/kg. Follow up investigations at
farm of origin were carried out in respect of the 2 samples with
levels exceeding 500µg/kg.
1 Target sample confirmed non-compliant for Diclofenac at a level
of 20ng/ml
The follow up investigation identified contamination of the sample
from use of human medicines by the sampling officer as the
source of this result.
Ovine
6 target samples confirmed non-compliant for Anthelmintics as
follows:
•
•
•
3 x Rafoxanide at (1) 367.47µg/kg
(2) 316.6µg/kg
(3) 246.6µg/kg
1 x Fenbendazole Sulphone: >2619µg/kg
2 x Closantel (1)6918.6µg/kg (2) 2916µg/kg
Full on farm investigations including examination of medicines
on farm and animal remedies record were carried out in each case.
As appropriate, advice is given to the farmer and follow-up visits
120
• Anthelmintics
• Bovine Milk
• 12 non-compliant
results*
•
•
•
Antimicrobials
Bovine Milk
2 non-compliant result*
take place.
Milk
12 target samples taken from milk tanks at farm level confirmed
non-compliant as follows:
• 7 x Nitroxinil at the following levels:
(1) 2.17µg/kg, (2) 7.228µg/kg, (3) 2.2µg/kg,
(4) 1.43µg/kg, (5) 7.8µg/kg, (6) .795µg/kg,
(7) 7.84µg/kg.
•
4 x Closantel at the following levels:
(1) 1.99µg/kg, (2) 3.49µg/kg, (3) 1.836µg/kg
(4) 1.01µg/kg.
•
1 x Rafoxanide at 9.83µg/kg
Follow up farm investigations were carried out in all cases.
Further scientific data revealed that existing VMP labelling was
not adequate to avoid presence of residues; immediate action was
taken to amend product labels and advise FBOs. Risk assessment
concluded that at the very low levels found, it was not necessary to
withdraw milk from the market. Restrictions on movement of
milk/treated animals; additional sampling and on-going
monitoring were implemented as appropriate following the
findings of the follow up investigations.
2 target sample taken from milk tanks at farm level confirmed
non-compliant as follows:
•
•
1 Non-Compliant
• 1 non compliant
• Chemical Elements
• Muscle
1 x Sulfadimidine at 147µg/kg
1 x Amoxycillin at >20µg/kg
Full on farm investigations including examination of medicines
on farm and animal remedies record were carried out in each case.
As appropriate, advice is given to the farmer and follow-up visits
take place.
Wild Game
1 target sample confirmed positive for lead at 3140ug/kg
*Non-compliant results as appropriate, have been reported to the relevant Services of the CA
for the purposes of implementation of Commission Regulation (EC) No 796/2004
DETAILS OF NON-COMPLIANT RESULTS – TARGETED SAMPLING
GROUP
RESIDU
SUBSTANCE
ANIMAL
CATEGOR
121
FARM/
SLAUGHTERHOUSE/OTHE
NONCOMPLIAN
E
Y/
SPECIES
RS
T
A2
THYROSTATS
BOVINE
FARM
4
A2
THYROSTATS
BOVINE
SLAUGHTER
7
A2
THYROSTATS
PORCINE
SLAUGHTER
9
A2
THYROSTATS
OVINE
SLAUGHTER
7
A6
NITROFURANS
BOVINE
FARM
4
A6
NITROFURANS
OVINE
SLAUGHTER
4
B1
ANTIBIOTICS
MILK
FARM
2
B1
ANTIBIOTICS
PORCINE
SLAUGHTER
1
B2a
ANTHELMINTI
CS
NSAID’s
FARM
12
POULTRY
SLAUGHTER
1
B2e
B2a
B2b
B3c
MILK
ANTHELMINTI
CS
NICARBAZIN
OVINE
SLAUGHTER
6
POULTRY
SLAUGHTER
9
CHEMICAL
ELEMENTS
WILD
DEER
SLAUGHTER
1
SUM
67
122
DETAILS OF NON-COMPLIANT RESULTS – SUSPECT SAMPLING
Ireland 2009
GROUP
RESIDU
E
SUBSTANCE
B1
ANTIBIOTIC
S
ANTIBIOTIC
S
OC’s
including PCB
Dyes-Leuco
Malachite
green
B1
B3a
B3e
ANIMAL
FARM/
CATEGORY SLAUGHTERHOUSE/OTHER
/
S
SPECIES
BOVINE
SLAUGHTER
NONCOMPLIAN
T
9
PORCINE
SLAUGHTER
2
PORCINE
SLAUGHTER
3
Farmed
finfish
Farm
4
SUM
123
18
IT
ITALY
Group A substances
Considering the non compliance found on 2008 and on the first semester of 2009, the
number of sampling for the following substances was increased: steroids, progesterone,
resorcylic acid lactones including zeranol, metabolites of nitrofurans, chloramphenicol.
A new substance has been added to be monitored: nitroimidazoles in eggs and milk,
zilpaterol in urine.
Follow-up actions
2 Boldenone – urine – young
Suspect and Other samples. 5 carcasses put
bovine:
under seizure at slaughterhouse. Investigations in
- 0.69 ppb;
the farm: record checks, n=27 additional samples
- 0.79 pp.
have been taken (urine), intensified check in the
farm, n= 579 animals put under temporary seizure
in farm, administrative measures and criminal
penalties. Denial EC aid
1 Betametasone – liver – young
Other sample. In the slaughterhouse 12 carcasses
bovines:
have put under seizure and then 55,5 kg of
- 3.16 ppb.
products have been declare unfit for human
consumption, in the farm of origin have been
intensified the checks (record), 2 additional
samples have been taken. The source was
established in the illegal treatment. Administrative
measures.
71 Prednisolone – urine – cows:
Other samples. (1) Investigations in the farm:
1. 1.72 ppb;
record checks, no additional samples, intensified
2. 0.88 ppb;
checks, ask for confirmatory analyses by operator;
3. 1.95 ppb;
(2) Investigations in the farm: record checks, no
4. 0.59 ppb;
additional samples, intensified checks, n=1 carcass
5. 2.36 ppb;
has been put under seizure at the slaughterhouse;
6. 3.57 ppb;
7. 3.77 ppb;
additional samples, intensified checks. Ask for
8. 4.86 ppb;
confirmatory analyses by operator; (4) n=1 carcass
9. 3.22 ppb;
has been put under seizure at the slaughterhouse
10. 0.87 ppb;
and declared unfit for human consumption; (5) No
11. 1.81 ppb;
information; (6) Investigations in the farm: record
12. 1.92 ppb;
checks, no additional samples, intensified checks
13. 2.77 ppb;
on n=1 farm; (7) No information; (8)
14. 2.69 ppb;
Investigations in the farm: record checks, no
15. 4.93 ppb;
additional samples and no intensified checks on
16. 5.80 ppb;
farm, n=1 carcass has been put under seizure at the
17. 2.4 ppb;
slaughterhouse, administrative measures and
18. 3.6 ppb;
criminal penalties; (9) Investigations in the farm:
19. 37.8 ppb;
20. 1.31 ppb;
checks, administrative measures and criminal
21. 0.65 ppb;
penalties; (10) Investigations in the farm: record
124
22.
23.
24.
25.
26.
27.
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
41.
42.
43.
44.
45.
46.
47.
48.
49.
50.
51.
52.
53.
54.
55.
56.
57.
58.
59.
60.
61.
62.
63.
64.
65.
66.
67.
68.
69.
70.
71.
2.43 ppb;
11.4 ppb also liver matrix;
5.04 ppb;
0.95 ppb;
7.09 ppb;
1.81 ppb;
2.17 ppb;
0.8 ppb;
4.77 ppb;
3.46 ppb;
1.16 ppb;
0.77 ppb;
5.07 ppb;
2.07 ppb;
0.68 ppb;
1.32 ppb;
0.66 ppb
2.3 ppb;
1.41 ppb;
2.38 ppb;
3.28 ppb;
2.43 ppb;
1.84 ppb;
2.32 ppb;
5.43 ppb;
1.46 ppb;
7.1 ppb;
1.13 ppb;
1.32 ppb;
1.27 ppb;
0.66 ppb;
1.89 ppb;
3.09 ppb;
1.28 ppb;
2.44 ppb;
0.77 ppb;
1.83 ppb;
2.49 ppb;
8.85 ppb;
0.97 ppb;
1.34 ppb;
6.97 ppb;
6.04 ppb;
1.71 ppb;
0.82 ppb;
3.51 ppb;
1.92 ppb;
2.11 ppb;
1.57 ppb;
2.74 ppb.
checks, no additional samples, intensified checks,
administrative measures and report to the judicial
authority; (11) No information about follow up
actions, n=1 carcass has been put under seizure at
the slaughterhouse; (12) No information about
follow up actions, n=1 carcass has been put under
seizure at the slaughterhouse and declared unfit
for human consumption; (13) Investigations in the
farm: record checks, no additional samples,
intensified checks, criminal penalties; n=1 carcass
has been declared unfit for human consumption;
(14) See point 13 above; (15) No information
about follow up actions, n=1 carcass has been put
under seizure at the slaughterhouse and declared
unfit for human consumption; (16) Investigations
in the farm: record checks, no additional samples,
intensified checks, administrative measures and
criminal penalties, n=1 carcass has been put under
seizure at the slaughterhouse and declared unfit
for human consumption; (17) See point 16 above;
(18) See point 16 above; (19) See point 16 above;
about follow up actions; (22) Investigations in the
criminal penalties, report to the judicial authority
for non compliant about food chain information;
(23) See point 16 above; (24) Investigations in the
criminal penalties, n=1 carcass has been declared
unfit for human consumption; (25) See point 16
above; (26) See point 24 above; (27)
Investigations in the farm: record checks, n=4
has been declared unfit for human consumption;
has been put under seizure at the slaughterhouse,
administrative measures and report to the judicial
authority; (29) See point 24 above; (30) See point
10 above; (31 Investigations in the farm: record
n=1 carcass has been put under seizure at the
slaughterhouse, administrative measures and
criminal penalties; (32) ) Investigations in the
farm: record checks, n=17 additional samples,
intensified checks, n=1 animal has been put under
seizure at the farm, administrative measures; (33)
125
has been put under seizure at the slaughterhouse
and declared unfit for human consumption,
administrative measures, ask for confirmatory
analyses by operator; (34) See point 16 above;
farm: record checks, n=21 additional samples,
intensified checks, administrative measures; (38)
See point 28 above; (39) See point 16 above; (40)
No information about follow up actions; (41) See
point 16 above; (42) Investigations in the farm:
checks, administrative measures and criminal
penalties; (43) See point 33 above; (44)
additional samples, intensified checks on n=1
farm, administrative measures and criminal
penalties, n=1 carcass has been put under seizure
at the slaughterhouse and n=1 carcass has been
declared unfit for human consumption; (45) See
point 42 above; (46) (47) See point 44 above; (47)
n=1 carcass has been declared unfit for human
consumption, Investigations in the farm: record
checks, no additional samples, administrative
measures and criminal penalties, investigations are
still in progress; (49) (50) (51) See point 42 above;
For (49) has been asked for confirmatory analyses
by operator; (52) See point 47 above; (53) (54)
See point 44 above; (55)(56)(57)(58)(59) n=1
carcass has been put under seizure at the
slaughterhouse and n=1 carcass has been declared
unfit for human consumption, no information
intensified checks, administrative measures; (61)
n=1 carcass has been declared unfit for human
consumption, administrative measures and
criminal penalties; (62) No information about
follow up actions; (63) the hind quarters has bee
put under seizure and declared unfit for human
consumption, investigations in the farm: record
administrative measures and criminal penalties;
(64) (65) See point 16 above; (66) Investigations
in the farm: record checks, no additional samples;
(67) See point 16 above; (68) Investigation in
farm: record checks but no additional samples, 1
carcass has been put under seizure in farm,
administrative measures; (69) See point 68 above;
126
3 Dexamethasone – liver – cows:
1. 5.03 ppb;
2. 66 ppb;
3. 3.80 ppb.
2 Dexamethasone – urine and liver
– cows:
1. 3.07 ppb - 3.31 ppb;
2. 5.89 ppb – 9.3 ppb;
1 Prednisolone - 1 Prednisone -1
Betametasone – urine – young
bovines:
1. 21.2– 5.35 - 12.5 ppb.
9 Dexamethasone – liver – cows:
1. 2.69 ppb;
2. 1.51 ppb;
3. 1.01 ppb;
4. 1.09 ppb;
5. 10.9 ppb;
6. 32.5 ppb;
7. 6.7 ppb;
8. 15.10 ppb;
9. 13.83 ppb.
9 Dexamethasone – urine – young
bovines:
1. 1.08 ppb;
2. 0.62 ppb;
3. 20.1 ppb;
4. 1.40 ppb;
5. 0.91 ppb;
6. 1.18 ppb;
7. 0.99 ppb;
8. 1.75 ppb;
9. 1.24 ppb.
(70) No information about follow up actions; (71)
Investigation in the farm: record checks, no
additional samples, criminal penalties.
Investigations are still in progress.
Target and Other samples. Investigations in the
intensified checks, n=1 carcass put under
temporary seizure, administrative measures and
criminal penalties. For point 2, besides the
investigation in the farm and of record, n=21
additional samples have been taken, 638 animals
have been punt under temporary seizure at farm
and n=1 carcass at slaughterhouse. The source was
established in the treatment not recorded but the
investigation is still in progress.
Other samples. See above. For sample (2) also
report to the judicial authority for non compliant
about food chain information.
Other samples. Investigation in the farm: record
checks, no additional samples, criminal penalties.
farm: record checks and 15 additional samples,
intensified checks on 7 farms, 1 carcasses at the
slaughterhouse and 16 animals on the farm put
under temporary seizure, alert notification (for
point (1) and (6), administrative measures and
criminal penalties; For point (3) report to the
judicial authority; For point 5, besides 103 animals
on the farm put under temporary seizure and n=17
additional samples. For point (7) the operator has
asked for confirmatory analyses. For point (9) the
source was established in illegal treatment.
Target and Other samples. n=463 animals have
been put under seizure at the farm and n=2
destroyed, investigations in the farm and
intensified checks on n=2 farms, record checks,
n=33 additional samples have been taken (16 in
the same farm and 16 in linked farm,
administrative measures. For points (4)(5)(6) also
criminal penalties and denial EC aid. For points
(5) (6) the source was the illegal treatment by
mouth.
127
10 Dexamethasone – liver – young
bovines:
1. 20.1 ppb;
2. 14.8 ppb;
3. N/A;
4. 3.07 ppb;
5. 2.64 ppb;
6. 2.91 ppb;
7. 404 ppb;
8. 3.39 ppb;
9. 6.74 ppb;
10. 3.70 ppb.
1 Prednisolone – muscle - veal
calves:
- 2.9 ppb
Target, Other and Suspect samples.
Investigations in the farms of origin: record
checks, n=5 carcass has been put under seizure at
slaughterhouse, administrative measures. For point
(3) 1 carcass has put under temporary seizure and
839,95 kg products have been declared unfit for
human consumption. For point 6 investigations are
still in progress. For point (7) n=8 additional
samples have been taken, 1 carcass has put under
seizure and declared unfit for human consumption,
administrative measures, criminal penalties and
denial EC aid. For points (8) (9) investigations are
intensified in 1 farm, 1797 animals have put under
seizure waiting for the results of the 21 additional
samples taken, the source could be illegal
treatment. For point (10) n=6 additional samples
have been taken.
Target sample. Investigations both in the
slaughterhouse or in the farm of origin, no
additional samples have been taken, verification of
records and no treatment was been recorded.
Intensified checks for 6 months, administrative
measures.
1 Prednisolone – urine – young
bovines:
- 1.05 ppb
Suspect sample. No information
2 Prednisolone – urine - veal
calves:
- 8.94 ppb;
- 17.8 ppb.
farm: record checks, 8 additional samples,
intensified checks in 3 farms, administrative
measures, criminal penalties and denial EC aid.
1 Prednisone – urine – young
bovines:
- 0.82 ppb.
1 Prednisolone and 2 Prednisone –
urine - young bovines:
- 2.37-0.85-3.39 ppb.
Other sample. No information
Suspect samples. Investigations in the farm:
record checks, 17 additional samples, intensified
checks in the farm, administrative measures
criminal penalties and denial EC aid. 66 animals
put under temporary seizure waiting for the
additional samples’ results. Investigations are still
in progress.
128
1 Prednisolone and 1 Prednisone –
urine - young bovines:
- 6.21-4.64 ppb.
Target samples. Investigations in the farm: record
checks, 21 additional samples (1 non compliant
for prednisone and 1 non compliant for
prednisolone), intensified checks in one farm,
administrative measures criminal penalties and
denial EC aid. 103 animals put under temporary
seizure waiting for the additional samples’ results.
1 Testosteron-17-beta-serum-veal
calv:
- 2.0 ppb
Other sample. Investigation in the farm: records
checks, 21 additional samples, intensified checks
in farm and 1 animal put under temporary seizure.
1 Boldenone-Alpha – 1 Boldenone
– 1 Boldione – urine – young
bovines:
- 0.69-0.88-2.44 ppb
Target samples. Investigations in the farm: record
checks, intensified checks, 21 additional samples,
administrative measures, criminal penalties and
denial EC aid. 1 animal has put under seizure in
the farm and then put down. The operator has
asked for confirmatory analyses.
1 Chloramphenicol – poultry –
muscle:
- 1,5 ppb.
Target sample. Investigations in the farm are still
in progress, examination of the records, 2
additional samples of muscle have been taken.
Intensified controls in the farm. The source of
residue wasn’t established.
1 Chloramphenicol – cows –
muscle:
Target sample. Investigations in the farm are still
in progress, examination of the records, additional
samples have been taken, 16 animals have been
put under seizure at farm.
-
2,3 ppb.
1 Chloramphenicol – pig – muscle:
-
1,4 ppb.
1 Clenbuterol – liver – veal calves:
-
N/A
1 Taleranol – urine – cows:
-
0.58 ppb.
Target sample. Investigations in the farm:
examination of the records, 3 additional samples
have been taken (n=2 feed and n=1 drinking
water), 370 animals have been put under seizure at
farm waiting for results.
Other sample. 1 carcass has put under temporary
seizure at slaughterhouse and 178.06 kg of
products declared unfit for human consumption.
No additional information about follow up actions.
Target sample. Investigations are still in progress
in the farm of origin: examination of the records,
n=15 additional samples, intensified controls in 1
farm, 1 carcass and 64 animals have been put
under seizure at farm.
129
1 Alpha Zeralanol and 1 Beta
Zeralanol – urine – cows:
-
1.10-2.14 ppb
1 Semicarbazide – muscle –
poultry:
-
Target samples. Investigations are still in
progress: record checks, 17 additional samples, 67
animals put under seizure in the farm, measures
administrative and criminal penalties.
Target sample. No information.
N/A
Group B substances
Considering the non compliance found on 2008 and on the first semester of 2009, the
number of sampling for the following substances was increased: antibacterial substances,
including sulfonamides and chinolones, coccidiostats, anthelmintics, organochlorine
substances including PCB, chemical elements and aflatoxines.
A new substance has been added to be monitored: ionophore coccidiostats in bovine and
milk, levamisole in milk.
Follow-up actions
Bovines
2 Penicillin G – muscle – young
Suspect samples. N=1 carcass has been put under
bovines and cow
temporary seizure at the slaughterhouse and 1
carcass has been declared unfit for human
consumption, investigations in the farm of origin:
verification of records, intensified checks in the
farm, no additional sample has been taken,
administrative measures and criminal penalties.
1 Beta HCH – feed
Other sample. The source of residue has been
established (environmental contamination).
2 Sulfadimethoxine – muscle –
Target samples. Investigations in the farm:
young bovine
intensified checks in the farm, no additional
samples have been taken, administrative measures.
1 Amoxycillin - muscle
Target sample. Investigations in the farm: record
checks, n=23 additional sampling (21 urine, I milk
and 1 feed), intensified checks in farm, n=1
carcass and n=60 animals have been declared unfit
for human consumption.
1 Ampicillin - muscle
Other sample. 1 carcass the declared unfit for
human consumption has put under temporary
seizure at slaughterhouse. Investigation in the
farm: records checks, no additional sample,
intensified checks in farm. The source was
established in different treatment compared to
recorded treatment. The operator asks for
confirmatory analyses.
130
1 Sulfamonomethoxine – muscle cows
2 Sulfadimidine – muscle – veal
calves and 1 Sulfadimidine in
muscle of cows
4 Oxytetracycline – muscle
1 Dioxins - muscle
1 Tetracycline, 1 Oxitetracycline
and 1 Chlortetracycline - muscle
1 Danafloxacin - muscle
3 Chlortetracycline - muscle
8 Sulfadimethoxine – muscle:
1. 180 ppb;
2. 6.12 ppb;
3. 337 ppb;
4. 360 ppb;
5. 115
6. 132
7. 360;
8. lkl
Target sample. N=1 carcass has put under seizure
at slaughterhouse, investigations in the farm but no
additional samples have been taken, intensified
checks at farm, administrative measures and
criminal penalties.
Target samples. 2 carcass has been put under
temporary seizure at the slaughterhouse,
investigations in the farm: record checks, no
additional samples, the source was the treatment
recorded but the withdrawal period wasn’t
observed, administrative measures.
Other and Suspect samples. N=8 carcasses have
put under seizure at slaughterhouse and 15
products have been declared unfit for human
consumption, no additional information about
follow up actions. Intensified checks in one farm.
Target Sample. Investigations in the farm and
additional sample (1), intensified checks in 1 farm.
Target samples. Investigations in the farm of
origin, no additional sampling, intensified checks,
1 carcass put under temporary seizure at
criminal penalties. The source of residues was
established in the illegal treatment.
Suspect sample. N=1 carcass has put under
seizure at slaughterhouse and declared unfit for
human consumption, no additional sample has
been taken, investigation on the farm,
administrative measures.
Pigs
Target and Other samples. Investigation on the
farm of origin, examination of the records, 2
carcass has been put under temporary seizure at
the slaughterhouse and 2 carcass has been declared
unfit for human consumption, administrative
measures and criminal penalties. For one case the
source of residues is the treatment not recorded
and not observations of the withdrawal period.
Target samples. Intensified checks in the farm of
origin and administrative measures, no additional
samples, n=2 carcass has been put under
temporary seizure at the slaughterhouse and n=2
declared unfit for human consumption. For sample
(2) the source of residues could be the treatment
not recorded and for sample 3 also criminal
penalties.
131
1 Colistin – drinking water
1 Sulfadiazine –muscle
1 Sulfadimidine - muscle
1 Doxicycline - muscle
8 Lead - muscle
1 Dioxins – muscle
1 Tylosin – drinking water
1 Ciprofloxacin – 1 Enrofloxacin –
1 Sulfadimidine - muscle
1 Sulfadimethoxine – drinking
water
2 Nicarbazin – muscle
1 Nicarbazin and 1 Monensin muscle
1 Oxytetracycline - muscle
Other sample. Investigations in the farm, n0
additional sampling. The source of residues was
established in the administration of medicated
water, administrative measures, intensified checks
in =1 farm.
Other sample. Investigations in the farm of
origin: records checks, no additional sampling.
The source of residues was established in the
administration of medicated feed, 109 animals put
under seizure in the farm. Intensified checks in 2
farms.
Other sample. Investigations in the f: record
checks, 1 sample of feed has been taken,
intensified checks in one farm. The source was the
treatment recorded for other category of pigs.
Administrative measures.
Other sample. Investigations in the farm of
origin: verification of records, intensified checks
in one farm, additional samples (1). The source
was non recorded treatment. Administrative
measures.
Target and Suspect samples. Investigations in
the farm of origin: verification of records,
intensified checks in one farm, n=13 (8 feed, 1
milk, 6 water) additional samples have been taken
and 3 non compliant, 17 animals put under
temporary seizure. The source could be the
medicated feed.
Poultry
Target samples. Increased controls in the farms of
origin. The source of residue wasn’t established.
Other sample. Investigations in the farm.
Other sample. Investigation in the farm for the
records of treatment.
Other sample. Intensified checks on n=1 farm, no
additional sample, the source has been established
in the withdrawal period not observed,
Target samples. N=7 carcasses put under seizure
at slaughterhouse, 4.5 kg of products declared
Other sample. Investigation in the farm with
intensified checks. The source was established in
illegal treatment.
Target sample. Investigation in the farm and 21
additional sample have been taken.
132
1 Doxycycline – muscle
Other sample. Administrative measures. No
additional information about follow up actions.
1 Doxycycline and 1
Oxitetracycline – muscle
1 Doxycycline – drinking water
1 Aflatoxin M1 – feed
1 Lead – muscle
4 Beta HCH - fat
2 Dioxins - liver
1 Cadmium - muscle
1 Oxytetracycline - bovine
1 Dioxins - bovine
2 Dioxins - buffalo
22 Aflatoxin M1 – bovine
Other sample. Investigations in the farm and
intensified checks, record check, n=1 additional
sample have been taken, the source of residues
was established in treatment not recorded,
Sheep and goat
Target sample. No follow-up actions.
Target sample. Investigations are still in progress.
Other samples. 1 carcass has been put under
temporary seizure at slaughterhouse, record checks
at farm, 1 additional sample, intensified checks in
29 farms, 519 animals have bee put under
temporary seizure at farm and 1900 kg of milk
declared unfit for human consumption.
Other sample. At slaughterhouse the liver has
declared unfit for human consumption. At farm the
investigations have been intensified (records), no
additional samples have been taken. The illegal
pasture was the source of contamination. Ban
pasture bylaw.
Horses
Milk
Suspect sample. No information.
Target sample. Investigations in the farm of
origin: additional sample has been taken (1 milk).
Increased controls in the farms, 2311 litres of milk
have put under temporary seizure and declared
unfit for human consumption and destroyed, 105
animals at farm have been put under seizure,
farm of origin: additional sample has been taken (1
feed). Increased controls in the farm, 117 animals
have put under temporary seizure.
Target - Suspect - Other samples. Investigations
in the farm of origin: examination of the records,
additional sampling (n=24 of milk with 1 non
compliant and 8 of feed), 11100 kilograms of milk
have been declared unfit for human consumption,
13900 kilograms of milk destroyed and 303
moulds of cheese have been declared unfit for
133
1 Aflatoxin M1 – sheep&goats
7 Beta HCH – bovine
5 Beta HCH - buffalo
8 Beta HCH – sheep&goats
6 Dioxins
1 Sulfadimethoxine - muscle
human consumption and destroyed. For samples
(4)(5)(6) the source of residue was established like
contaminated feed. For sample (7) (10) criminal
penalties. For (10) the source was contaminated
feed. For sample (20) administrative measures.
Other sample. Investigations in the farm and 2
additional samples of feed have been taken. The
source of contamination was established in
contaminated feed. Administrative measures.
Intensified checks in one farm.
Target sample. Investigations in the farm:
additional sampling (5 of milk and 4 of feed). In
the bovine’s farm n=207 animals have been put
under temporary seizure. Intensified checks in 43
farms, 92 ql of milk have been declared unfit for
human consumption. The source of residue has
been established (environmental contamination).
Other sample. Investigations in the farm:
additional sampling (3 of milk and 1 of feed). In
the bovine’s farm n=19 animals have been put
under temporary seizure. Intensified checks in 29
farms. 200 l of milk declared unfit for human
consumption. Investigations are still in progress.
farm of origin: intensified checks in 29 farms,
additional sampling (1 of milk and 1 of feed), 135
animals have been put under seizure at farm, 405.5
ql of milk declared unfit for human consumption.
Eggs
Other and Suspect samples. Investigations in the
farm: examination of the records and intensified
checks in the 6 farm, n=5 additional sampling, 74
animals have put under seizure at farm. For some
non compliant the investigations are still in
progress. Administrative measures. The source
could be the contaminated environment.
Rabbit
1 Target sample. Investigations in the farm:
records check and intensified checks in 1 farm,
n=1 additional sample has been taken.
Aquaculture
No non-compliant
134
Farmed game
No Non Compliant
Wild game
No Non Compliant
2 Tetracycline
2 Chlortetracycline
2 Sulfathiazole
Honey
Other and Suspect samples. Investigations to the
original producer: verification of records,
intensified checks in the farm, n=9 additional
samples have been taken with 1 non compliant, 2,4
ql of honey have been declared unfit the human
criminal penalties. The source is the use of not
adequately checked beeswax.
Other and Suspect samples. Investigations in the
farm: record checks and no additional samples,
administrative measures applied, 520,5 kg of
honey have been declared unfit for human
consumption waiting for being destroyed,
Target and Other samples. Investigations to the
original producer: examination of the records, 3
additional samples have been taken [1 beehive in
other place), intensified checks, 10 beehives with
honeycomb, 12 beehives with family, 2 empty
beehives and 450 kg of honey have been put under
temporary seizure. Administrative measures.
Investigations showed evidence of old treatment
without records.
135
LT
LITHUANIA
Group A substances
plan
Number of samples of bovine animals and pigs is decreased whereas there is decrease in
the number of slaughtered bovine animals and pigs in Lithuania. Number of honey and
aquaculture samples is increased whereas there is increase in production in Lithuania.
Number of farmed game and wild game samples is increased up to 100 samples
following FVO recommendations.
Laboratories involved in analyses of residues of veterinary medicinal products are
accredited and use validated methods according to Commission Decision 2002/657/EC.
All compulsory substance groups to be monitored according to the Annex II of the
Council Directive 96/23/EC are included in the monitoring plan. Groups B2b, B2d, B3d
are added for ovine animals, groups B2b and B2e are added for rabbits, groups B2a, B2b,
B2c, B2d, B3a, B3b and B3c are added for horses and groups A1, A2, A3, A4, B2c, B2e
and B3a are added for farmed game.
The requirement to include in the monitoring plan at least 3 substances from the
substance groups A6, B1, B2a and B2e to be tested in 70 % of milk samples is fulfilled.
Milk samples are sampled only at dairy farm level.
Testing of nitrofurans is foreseen only in NFVRAI. It has validated testing method for all
four stable metabolites of nitrofurans. Testing of chloramfenicol is foreseen only in
NFVRAI by confirmatory method.
A3 group substance medroxyprogesterone was introduced into the monitoring plan for
bovine animals and pigs.
Testing of beta-agonists (A5 group) is foreseen by LC-MS/MS technique., tests using
ELISA are no longer performed.
1 chloramphenicol – swine muscle
Follow-up actions
Swine
Investigation was carried out, farm was identified.
Products were consumed before investigation. The
cause of contamination with chloramphenicol was
not identified. It was found non-compliances
related to withdrawal period for antimicrobials.
Administrative sanctions have been applied.
136
Group B substances
plan
UPLC- MS/MS technique is introduced for the testing of B1 group antimicrobials in
milk. It is foreseen to test lincomycin, canamycin and spectinomycin (frequently used
substances in Lithuania) in milk samples.
Testing of avermectins (abamectin, doramectin, ivermectin, emamectin, moxidectin)
(B2a group substances) is introduced into monitoring plan for bovine animals, pigs,
sheep, horses, poultry, farmed game, eggs, milk and aquaculture.
Testing of carbadox and olaquindox (B2f group substances) is introduced into
monitoring plan for pigs (feed samples).
Testing of mercury (B3c group substance) is introduced into monitoring plan for pigs.
Lead and cadmium are tested by Z-ETA-AAS technique.
2 antibacterials – muscle
(in one sample confirmatory
method revealed presence of
chlortetracycline within the limits
of MRL, in another sample
dihydrostreptomycin above MRL
was confirmed)
1 enrofloxacin and ciprofloxacin –
muscle
1 cadmium - kidney
1 enrofloxacin and ciprofloxacin –
muscle
1 antibacterials – muscle
Follow-up actions
Bovines
Investigation was carried out, farms and animals
were identified. In both cases infringements
regarding withdrawal period were detected and
administrative sanctions have been applied. In one
case products were consumed before investigation,
in other case part of products were consumed
before investigation and part of products were
withdrawn from the market and destroyed.
Investigation was carried out, farm and animal
were identified. Products were consumed before
investigation. The cause of contamination was not
identified. Administrative sanctions have been
applied.
Farm was identified and investigation on the farm
was carried out. Products were consumed before
the investigation.
Swine
were identified. Suspected animal products were
sampled and tested. Samples were negative for
antimicrobials. Products were consumed before
investigation. It was found non compliances
related to withdrawal period. The farm was
included in the group of high risk establishments.
Control of movement of animals was intensified.
137
1 Spectinomycin and lincomycin –
muscle
1 salicylat – muscle
1 lasalocid – eggs
4 inhibitors – bovine milk by
DELVO-SP method (cloxacillin
was confirmed in one sample, and
penicillin G was confirmed in
another sample)
2 dioxins and dioxin-like PCB – 1
cod liver, 1 headlong (Baltic
herring)
were identified. Suspected animal products were
sampled and tested. Samples were negative for
antimicrobials. Products from the animal were
consumed before the investigation. The cause of
contamination was not identified.
Investigation is ongoing. Samples have been taken
for testing. Products have been withdrawn from
the market and destroyed. RASFF notification was
sent.
Horses
were identified. Products were sold before
investigation. By-products were used for feeding
of fur animals. The cause of contamination was
not identified.
Eggs
Investigation was carried out. Suspected products
(eggs, drinking water, feed) were sampled and
tested. They were negative for coccidiostats. It was
suspected cross-contamination of feed during
transportation. Contaminated eggs were collected
and destroyed. Administrative sanctions have been
applied.
Milk
Investigations were carried out.. In one case it was
found infringement related to withdrawal time. In
two cases it was suspected that milk could be
contaminated using medicated hand ointment.
Aquaculture
Investigations were carried out. Products were
consumed before the investigation.
138
LU
LUXEMBURG
Group A substances
Follow-up actions
Substance--Matrix-animal or animal Actions:
Thiouracil-urine-bovine-14ppb
Investigations in the farm of origin, sampling on
farm of 7 more animals and sampling of feed. All
samples were negative.
Group B substances
Follow-up actions
Bovines
Pigs
Poultry
Sheep and goat
Horses
Milk
Eggs
Rabbit
Aquaculture
Farmed game
139
1 sample Pb-liver-roe-3.9mg/kg
1 sample Cd-liver-roe0.922mg/kg
1 sample Permethrine-fatwildboar-0.07mg/kg
Wild game
Intensifying sampling for the same substances in
the same region. All samples were negative and
there id no indication that a region is more
contaminated than an other.
Honey
140
LV
LATVIA
Group A substances
plan
Modification of plan is described in laboratory file.
Follow-up actions
Chloramphenicol - 0,46 µg/kg – pig 1 farm (10045 pigs held in the farm) was
meat
investigated. Stopping of meat realization till
situation will clarified. Origin of CAP was not
identified. Additional sampling – 1 feed sample.
Chloramphenicol - 0,20 µg/kg – pig 1 farm (11125 pigs held in the farm) was
meat
investigated. Stopping of meat realization till
situation will clarified. Origin of CAP was not
identified. Additional sampling – 1 meat sample.
Group B substances
plan
Modification of plan is described in laboratory file.
Follow-up actions
Bovines
Cadmium – 1,78 ± 0,18 mg/kg – 1
It was clarified that sample was taken from old
cow kidney
cow (8 years of age) and farm since last
slaughtering is not breed bovines.
Cadmium – 1,68 ± 0,17 mg/kg – 1
1 farm (11 cows held in the farm) was investigated
cow kidney
and was clarified that sample was taken from old
cow (11 years of age).
Cadmium – 2,86 ± 0,29 mg/kg – 1
1 farm (28 cows held in the farm) was
cow kidney
investigated.
Pigs
Poultry
Sheep and goat
Horses
Milk
Eggs
Rabbit
141
Aquaculture
Farmed game
Cadmium – 6 liver samples (0,520
mg/kg to 5,41 mg/kg); 20 kidney
samples (1,15 mg/kg to 6,35
mg/kg); 5 muscle samples (0,069
mg/kg to 0,493 mg/kg).
Lead – 4 liver samples (0,515
mg/kg to 0,778 mg/kg); 6 kidney
samples (0,566 mg/kg to 3,12
mg/kg); 8 muscle samples (0,11
mg/kg to 0,92 mg/kg)
SEM - 4,2 µg/kg - honey
SEM - 4,2 µg/kg - honey
Wild game
Public warning – press release.
Honey
Origin of honey was country of EU. The product
was withdrawn from the market, RASFF
notification was created.
Origin of honey was country of EU. The product
was withdrawn from the market, RASFF
notification was created.
142
MT
MALTA
Group A substances
Nor testosterone:
Urine: 45 ug/L α Nor testosterone,
14 ug/L β Nor testosterone
Equine (Target)
Follow-up actions
Investigation is still underway since the result was
received recently. The middleman has been informed
to provide owner details.
Group B substances
Follow-up actions
Bovines
Pigs
Poultry Liver and Eggs (Target and Suspects)
1 Salinomycin; Liver; 11 ug/kg (Target)
Withdrawal period of zoo technical feed
1 Salinomycin: Liver; 10 ug/kg (Target)
(containing salinomycin is not being
1 Salinomycin: Liver; 11 ug/kg (Suspect)
respected. Warning letter sent to farmers.
1 Salinomycin: Liver; 10 ug/kg (Suspect)
Follow up by means of targeting sampling
1 Salinomycin: Eggs; 11 ug/kg (Target)
from farmers is being undertaken.
One farmer had non compliant results
previously. In fact 2 suspect samples were
non compliant from the four targeted
samples taken in 2009.
1 PCDD-PCDF + dioxin-like PCBs (Target)
MEPA (Malta Environment Planning
Muscle => 5.76 pg-TE/g fat
Authority) is informed for further action.
Liver below level of action => 0.07 pg-TE/g fat
The farm is going to be investigated and
targeted samples will be sent immediately
for prompt action.
Sheep and goat
Horses
Milk
Eggs
143
Rabbit
-----------Aquaculture (Imports)
1 Mercury; Frozen fish (Vietnam);
Competent authority of the exporting country has
1.59mg/kg (Imports)
been informed and also BIP will target products from
the same country/ producer.
Farmed game
Wild game
Honey
144
NL
THE NETHERLANDS
Group A substances
11 non-compliant result for
conjugated 17-alfa-boldenone bovine
(calves).
2 non-compliant results for
testosterone in bovine (calves)
1 non-compliant result for alfanortestosterone in equine.
2 non-compliant result for alfanortestosterone in sheep.
4 non-compliant results for alfanortestosterone in bovine
9 non-compliant result for betanortestosterone in pig.
4 non-compliant results for betaestradiol in bovine (calves)
dexamethasone in cattle ( 2 calves, 4
older bovine)
Follow-up actions
All cases were on-farm investigated. Additional
sampling was performed and again 17-alfa-boldenone
was detected. A probable cause was not observed.
Administrative records were complete and up-todate. No penalties applied
Investigation conducted. One animal proved to be
male instead of female. Additional sampling for noncompliant female animal was carried out but those
samples proved compliant. No penalties applied.
Investigation closed.
The animal was imported for slaughter.Identification
of the animal proved impossible due to improper use
of the European horse passport. Investigation closed
No investigation conducted. Alfa-nortestosterone is
endogenous in sheep.
Investigation conducted. Additional sampling carried
out but no further non-compliant samples were
found. Records were properly kept. Investigation
closed
In three cases the gender of the animal was male.
Beta-nortestosterone is endogenous in male pigs. The
administration records were inspected and additional
sampling was carried out which did not reveal further
indications of the use of beta-nortestosterone.
Investigation pending
Investigation conducted in three cases, in two cases
the legal application of dexamethasone was observed.
The withdrawal period was respected.
In one other case investigation could not be
completed due to an incomplete track record.
No penalties applied.
1 non-compliant result for betaAdditional sampling carried out but no additional
testosterone in tilapia
non-compliant results were found. No indications of
VMP use, records properly kept. Investigation closed
1 non-compliant result for isoxuprine Investigation conducted. The use of Duphaspasmin
in cattle (calf)
was observed. Maternal transfer is a possible
explanation. Investigation closed. No penalties
applied.
2 non-compliant result for CAP in pig One animal originated from Belgium. Belgian
Authorities were informed
145
Investigation was conducted for the other animal.
Additional sampling was carried out, no additional
non-compliant samples were found and no prove for
abuse of CAP could be obtained. Penalty applied and
investigation was closed.
Investigation conducted. No evidence of abuse of
nitrofurazon was found
1 non-compliant result for semicarbazide in pig
Group B substances
1 non-compliant result for cadmium
Follow-up actions
Bovine animals
Investigation was carried out, animal originated from
Belgium. Belgian authorities were informed
dihydrostreptomycine
ivermectine
1 non-compliant result for neomycine
Animal originated from Belgium. Belgian authorities
were informed
In one case records were improperly kept. Official
warning issued. The other investigation is pending.
Records concerning VMP use were absent. Penalty
applied
Porcine animals
1 non-compliant result for cadmium.
Investigation conducted. Additional samples (feed)
were taken. No cause found, investigation closed.
One investigations conducted. Records of VMP use
dihydrostreptomycine
were properly kept By accident a treated animal was
send for slaughter. Warning issued.
One animal originated from Belgium, BE authorities
doxycycline
were informed
One fine was applied for not respecting the
withdrawal period, one official warning issued. One
farmer was instructed concerning use of VMP and
cleaning after treatment (compliance assistance)
1 non-compliant result for fenvaleraat Investigation conducted. No probable cause found.
6 non-compliant results for levamisol Use of levamisol was confirmed. Withdrawal period
was not respected (3 cases). Penalties applied
Investigations were conducted. 1 fine was issued for
oxytetracycline
not respecting the withdrawal period. Two warnings
were issued when records were not complete. In one
case no cause ahs been found and no abnormalities
were observed
Two investigations were conducted. In one case
sulfonamides (2 sulfadiazine, 3
records were properly kept. No sulfonamide
sulfamethoxazole)
containing drugs were administered. No probably
cause found. In the other case records were not
properly kept, penalty applied.
Records were properly kept, withdrawal period
tulathromycine
respected. Investigation closed.
Poultry
146
nicarbazin.
Four cases were investigated. One flock originated
from Germany. German Authorities were informed.
No probable causes found. Use of nicarbazin was
confirmed in all cases. Administration records were
kept. Indications found that withdrawal periods were
not fully respected. Two warnings were issued.
Sheep and goat
Pharmaceutical formulation for cattle applied to
ivermectine
sheep. Official warning issued.
Insufficient data for tracking and tracing of the
dihydrostreptomycine and neomycine animal. No investigation conducted
Off-label use of Ampiject 15% was observed.
gentamicine
Horses
None
Milk
No investigation conducted
aminoglycosides
Eggs
1 non-compliant result for monensin
No investigation conducted
Rabbit
None
.
Aquaculture
None
Farmed game
None
Wild game
3 non-compliant results for lead in
Free range animals. No investigation conducted
rabbit
roe deer
deer
hare
wild boar
wild pigeon
wild duck
Honey
None
147
PL
POLAND
Group A substances
plan
substances
Increased number of samples of bovines and chickens and decreased number of
samples of pigs and turkeys for many substances from group A.
New compound/matrix included to the plan:
A6 Nitroimidazoles and hydroxymetabolites of nitroimidazoles in milk and
honey.
Updating of action levels (MRLs, MLs, national levels) and validation data (CCα and
CCβ).
A2 – Thiouracil (target)
Bovines – urine – 31.4 ppb
A3 – 7 Nandrolone (target)
6 Pigs – urine
1. - 78 ppb
2. - 11.5 ppb
3. - 15.5 ppb
4. - 28.9 ppb
5. - 36.7 ppb
6. - 23.5 ppb
Follow-up actions
Investigation in the slaughterhouse and in the
farm of origin; verification of records;additional
sampling (urine, water); all results compliant;
origin of thiouracil was not identified; medical
treatment registraton kept correct; farm
subjected to intensified checks; 1 administrative
measure.
1. Investigation on the farm of
origin;verification of records; additional
samplings (4 urine) - animals were held in the
farm until sampling results (all compliant) ;
infringements in medical treatment registration
and animal registration (administrative
procedure); 3 administrative measures; farm
subjected to intensified checks.
2.,3. Animals from one origin; investigation in
the farm of origin; verification of records;
animal medical treatment registration kept
correct, additional sampling (2 urine, 1 water),
animals were held until sampling results
(compliant); 2 administrative measures; farm
subjected to intensified checks; additonal
farmaceutical control – reason of presence of
nandrolone was not established.
4. Investigation on the farm of origin;
verification of records; additional sampling (2
urine, 1 water); animals were held until
sampling results - all compliant; 2 administrative
measures.
5. Investigation on the farm of origin; additional
sampling (urine, feed) – compliant results;
148
reason of NC – problem w with sampling
procedure – urine was taken from male –
training for official veterinarian took place.
6. Investigation in the slaughterhouse and on the
farm of origin (additional sampling - urine); the
reason of presence of nandrolone was not
identified.
Investigaton in the slaughterhouse and on the
farm of origin; verification of records; additional
sampling (water, urine) - animals were held until
sampling results (both compliant); 1
administrative measure.
Investigation in the slaughterhouse; the reason
A3 – Testosterone (target)
of presence of testosterone was established as
Bovines – serum – 0.73 ppb
follows – mistake during sampling - gender of
the animal was mark wrongly - female instead of
male; 0.73 ppb for male is compliant result;
official veterinarian who took the samples was
trained according to CVO monitoring
instruction.
Investigation on the farm of origin; additional
A6 – SEM (target)
sampling (urine, milk, feed, water) - compliant
results (animals were held until sampling
results), verification of record; origin of SEM
was not identified; farm subjected to intensified
checks; 1 administrative measure; additional
control concerning drug wholesaler and
veterinarian responsible for treating the herd.
Country of origin India; notification to RASFF;
A6 – AOZ (import)
enforced checks of consignements from this
Shrimps – muscle – 4.7 ppb
producer were established.
Group B substances
plan
Increased number of samples of bovines, chickens and milk and decreased number of
samples of pigs and turkeys for many substances from group B.
New compounds included to the plan:
B1 Florfenikol in aquaculture
Methods changes:
B1 Antibacterials – LC-MS/MS (confirmatory),
149
B1 Antibacterials – Charm BL/TET, Twinsensor BT (screening) in milk
Updating of action levels (MRLs, MLs, national levels), validation data (CCα and
CCβ) and methods (AAS specified).
B1 – 6 Antibacterials (4 target +
2 suspect) – muscle + kidney
B1 – Oxytetracycline – muscle
B2f – Dexamethazone – liver
(target)
B3a – Lindane – fat (target)
B1 – 14 Antibacterials –
(3 target + 11 suspect) muscle +
kidney
B1 – 3 Doxycycline – (target)
B1 – 2 Penicillin – (target)
B1 – Oxytetracycline – (target)
B1 – Tetracycline – (suspect)
B3a – Lindane – fat (target)
B3a – DDT – fat (target)
B3d – 4 Ochratoxin A (target) –
kidney
Follow-up actions
Bovines
Investigations on the farms of origin and in the
establishments; verification of records; additional
sampling (compliant results); in most cases farms
subjected to intensified checks; in cases where
reason for presence of antibacterials was
established, it was withdrawal period, that wasn’t
kept – 2 cases (infringement) were bring before
the prosecution authority,5 administrative
measures.
Investigation in the farm of origin and in the
establishment; carcasses unfit for human
consumption (after post-mortem check); the
animal was treated before slaughter (withdrawal
period wasn’t kept; however it wasn’t
dexamethazone) - reason for presence of
dexamethazone wasn’t established; farm subjected
to intensified checks; infringements in FBO
responsible for purchase of animals (purchasing
center) - case was bring before the prosecution
authority.
Investigation in the establishment and on the farm
of origin; verification of records; additional feed
sampling – all compliant; farm suspected.
Pigs
Investigations on the farms of origin and in the
establishments; verification of records; 11 suspect
carcasses and offal declared unfit for human
consumption; in one case 135 kg of meat
utilized/rendered; additional sampling;
verification of records; farms subjected to
intensified checks; 10 administrative measures; in
3 cases the reason for presence of antibcterial was
indentified - withdrawal period wasn’t kept
(sanctions – fine).
2 investigations on the farms of origin and in the
establishments; additional sampling (feed, fat) –
all compliant results; farms subjected to
intensified checks; 2 administrative measures;
source of contamination wasn’t identified.
4 investigations on the farm of origin and in the
sampling (feed) – compliant results; farms
150
subjected to intensified checks; 4 administrative
measures; reason of contamination wasn’t
identified.
B1 – 4 Antibacterials (target) –
muscle + liver
B1 – Doxycycline (target) –
muscle
B2b – 15 Anticoccidials
(10 target + 5 suspect)
7 – Lazalocyd – liver (target)
2 – Nicarbazin – liver (target) +
feed (suspect)
5 – Salinomycin – 3 liver (2
target + 1 suspect) + 2 feed
(suspect)
1 – Maduramicin – feed
(suspect)
B3c – 8 Cadmium (target) –
muscle
B1 – 5 Antibacterials (target) –
milk
B3c – Lead (target)
B2b – 9 Anticoccidials (3 target
+ 6 suspect)
1 – Diclazuril – eggs (target)
1 – Lasalocid – eggs (suspect)
Poultry
establishments; verification of records - additional
sampling – compliant results; one case – 1016 kg
of meat and products utilized/ rendered; one case
sanction - fine; farms subjected to intensified
checks; origin of antibacterials wasn’t identified.
Investigation in the farm of origin and in the
establishment; verification of records; withdrawal
period wasn’t kept (lack of information in FCI;
case was bring before the prosecution authority);
farm subjected to intensified checks.
sampling (feed – NC results); in one case 165 kg
of frozen wings were held until results of
additional analysis - compliant results; farms
subjected to intensified checks; in case, where the
reason was found, it was cross-contamination at
the stage of feeding mill or on the farm.
Sheep and goat
Horses
Investigations on the farm of origin; verification
of records at the stage of FBO responsible for
purchase of animals (purchasing center); in one
case infringements in identification was
established - case were bring before the
prosecution office.
Milk
Investigations on the farms of origin; verification
of records, additional sampling; milk was held
until results of additional analysis, 1030 l of milk
and 1073 kg of cheese were utilized/rendered;
farms subjected to intensified checks; 5
administrative measures; origin of presence of
antibacterials wasn’t established.
Investigations on the farm of origin; verification
of records; additional sampling (all compliant);
the cause wasn’t identified.
Eggs
3 investigations on the farm of origin; verification
of records, additional sampling (NC results in
feed); 229 772 eggs and 955 kg of eggs were
utilized/rendered; farms subjected to intensified
151
2 – Nicarbazin – eggs (target +
suspect)
3 – Semduramicin – eggs + 2
feed (suspect)
1 – Salinomycin – eggs (target)
1 – Salinomycin – feed (suspect)
B3a – DDT (target) – muscle
(fish)
B3e – 8 Malachite green
(7 target + 1 suspect) – muscle
(fish)
B3c – 17 Arsenic (import) –
muscle (fish)
checks; additional control in feeding mills; 3
Rabbit
Aquaculture
Investigation on the farm of origin; additional
sampling (compliant results).
7 investigations in the farm of origin (2 cases
concerning carp, 5-trout,); verification of record;
additional sampling (fish held in the farm until
results – 7000 kg of trout); farms subjected to
intensified checks.
Farmed game
Wild game
9 investigations; verification of records; carcasses
B3c – Cadmium (target) – liver
or/and offal declared unfit for human consumption
B3c – 8 Lead (target) – muscle
B3c – Mercury (target) – muscle (about 74 kg of meat according to available data);
5 administrative measures.
B1 – 19 Sulfonamides
(12 target + 7 suspect) – honey
Honey
Investigations on the farms, verification of
records; additional sampling (7 NC results);
product was held until the results of additional
analyses; 800 kg of honey were utilized/ rendered;
farms subjected to intensified checks.
152
PT
PORTUGAL
Group A substances
1 - We had only one NC for Group A and it was from IMPORT. IN TARGET and in
SUSPECT we did not have any non-compliant results in 2009.
2 - In 2010 we kept samples reinforcement for A5 Beta-agonists and increased
reinforcement for A6 – Table 2 of Regulation (UE) n. º37/2010.
3 - Introduction of sampling for A2 in poultry.
4 - Introduction of sampling for A5 in milk and for A6 (nitroimidazoles) in milk and
honey as it was recommended by CRL Berlin
Follow-up actions
AOZ – Furazolidone
RASFF Information: Information Notification:
Prawns (IMPORT)
2009.1739 on 15 December 2009
1 non-compliant result in frozen
shell on Black Tiger Semi IQF
Prawns: 38.2 µg/kg
Group B substances
1 – B1 – Antibacterial substances – We reinforced the number of samples, due to the
non-compliant results that are appearing in a regular basis in Portugal and in Europe
2–B2a - Anthelmintics - Introduction of sampling in eggs as recommended by CRL
Berlin
3 – B2b - Anticoccidials - Reinforcement for 2010, due to the number of non-compliant
results in 2008 and 2009. Despite there is a National Control Plan for animal feed, we
introduced sampling in feed as it was recommended by CRL Berlin.
4 – B2e –NSAID’s - Introduction of the matrix muscle for this group of substances
5 – B2f - Quinoxalines – Despite we collect samples for quinoxalines every year, as we
had one non-compliant result for olaquindox we reinforced de number of samples.
6– B3a – Organochlorine compounds - We introduced samples for dioxins in other
species than poultry
Follow-up actions
Pigs
153
Sulfadimetoxin
1 non-compliant result in muscle –
0.163 mg/kg
Levamizol
2 non-compliant results in liver:
4612.0 µg/kg; 271.8 µg/kg
Investigations in the farms origin. Inquiry of
possible reasons for the presence of the substance.
Administrative measures: yes
Investigations in the farm origin. Inquiry of
Maduramicin
1 non-compliant result in liver: 15.8 Investigations in the farm origin. Inquiry of
µg/kg
Poultry
Nicarbazin – Broilers 14 noncompliant in liver: 172.0 µg/k
133.0 µg/kg; 182.0 µg/kg; 134
µg/kg; 363.0 µg/kg; 157.0 µg/kg;
411.0 µg/kg; 238.0 µg/kg; 303.0
µg/kg; 219 µg/kg; 203.5 µg/kg;
163.9 µg/kg; 1803.0 µg/kg; 160.7
µg/kg.
Investigation in the farm of origin. Inquiry of
possible reasons for the presence of the substance
Administrative measures in case of use in the five
days before slaughter
We would like to inform the
Commission, that we will include in
our 2009 Results Report, 7 non
compliant results from de NRCP
2008, due to the results had arrived
after the submission of the 2008
Questionnaire.
These results were as follows:
Broilers 7 noncompliant results in
liver: 152.0 µg/kg; 151.0 µg/kg;
141 µg/kg; 463 µg/kg; 261.0 µg/kg;
606.0 µg/kg; 724.0 µg/kg;
Maduramicin
Broiler 1 non-compliant in liver :
288,2 µg/kg
Commission, that we will include in
compliant results from de NRCP
2008, due to the results had arrived
Questionnaire.
154
These results were as follows:
Broilers - 2 non compliant results
in liver : 10.0 µg/kg; 12.0 µg/kg
Olaquindox – Broiler 1 noncompliant in liver: 0,065 mg/kg
Additional sampling of liver, feed and water. All
animals held in the farm origin, until results were
available
Lasalocid – Broiler 4 noncompliant in liver : 1031.0 µg/kg;
291.0 µg/kg; 938.4 µg/kg; 437.6
µg/kg
Cadmium and Lead:
2 non-compliant results for both
heavy metals in liver :
3.1 mg/kg (Cd); 0.6 mg/kg(Pb);
2.3 mg/kg (Cd); 0,6 mg/kg (Pb)
Cadmium
2 non – compliant results in liver:
0.7 mg/kg; 0,6 mg/kg
Maduramicin
2 non compliant results in liver:
12,6 µg/kg; 23.0 µg/kg;
Horses
Horses with more than two years old have their
livers rejected for human consumption.
Rabbit
Commission, that we will include in Administrative measures: yes
compliant result from de NRCP
2008, due to the result had arrived
Questionnaire.
This result was as follows:
1 non-compliant results in liver:
15.0 µg/kg;
Salinomicin – 1 non compliant
result in liver: 15.3 µg/kg
Doxiciclin
Farmed game
155
Quail - 1 non-compliant in muscle:
0.270 mg/kg
Lead
Veal - 1 non- compliant result in
liver: 1,5 mg/kg
Evaluate - 3 non-compliant results
in liver: 0,7mg/kg; 1,2 mg/kg; 1,2
mg/kg
Administrative measures: Yes
Wild game
156
RO
ROMANIA
Group A substances
A.1. No changes. The group was added to horses, the matrix is muscle, screening and
confirmatory method is GC-MS/MS.
A.2. No changes. The group was added to horses, the matrix is urine, screening and
confirmatory method is GC-MS/MS.
A.3. No changes. Nortestosteron and trenbolone were added to fish species, screening and
confirmatory method are GC-MS/MS (nortestosteron) and LC-MS/MS (trenbolone).
A.4. No changes
A. 5. No changes
A.6. Ipronidazol was excluded.
Follow-up actions
Group B substances
B.1. New substances were added : Difloxacine, Flumequin and Marbofloxacine. For milk were
added also Lincomycin, Pirlimycin, Cefalonium and Cefazoline. For honey on the
sulfonamides group was added Sulfadiazine.
B.2.a No changes
B.2. b. No changes
B.2. c. New substance was included: Flumetrin, Resmetrin. The all group substances was
included for rabbit and for horses. The matrix is muscle, screening and confirmatory method is
GC-ECD.
B.2.d. No changes
B.2.e. Were included vedaprofen, flunixin, meloxicam. As matrix, muscle has been excluded,
157
exceptions are poultry and farmed game. The screening and confirmation method is LCMS/MS.
B.2. f. New substances were added: prednisolon, methylprednisolone and betametasone; the
matrix selected is urine (for live and slaughtered animals) and milk. The screening and
confirmation method is GC-MS/MS.
B.3.a. No changes. The group substances was added to horses and removed from wild game.
B.3. b. New substances were added: Coumaphos, Phoxim. Screening method is GC-NPD and
confirmatory method is GC-MS/MS. For honey was added Coumaphos. The group substances
was added to horses.
B.3. c. No changes.
B.3. d. No changes.
B.3.e No changes
Follow-up actions
Bovines
Pigs
Poultry
Sheep and goat
Horses
Milk
Eggs
Rabbit
Aquaculture
Farmed game
Wild game
Honey
158
SI
SLOVENIA
Group A substances
plan in 2010
substances
A5 substance group has been extended to include:
•
Brombuterol CAS 41937-02-4
•
Cimbuterol CAS 54239-39-3
•
Mapenterol CAS 95656-68-1
NONE.
Follow-up actions
Group B substances
plan in 2010
substances
B2d substance group has been extended to include:
•
Acepromazine CAS 61-00-7
•
Propionylpromazine CAS 3568-24-9
•
Xylazine CAS 7361-61-7
Follow-up actions
1x
Honey
-obtain al the data required for the identification of
SULFAMONOMETHOXINE
animal product and of the holding of origin
Matrix:Honey
-honey was assessed as unfit for human
Results: 49 µg/kg
consumption and destroyed in accordance with
applicable regulations
Milk
1x
-obtain al the data required for the identification of
TETRACYCLINES
animal product and of the holding of origin
Matrix:Milk
-honey was assessed as unfit for human
159
Animal: Bovine (Cows)
consumption and destroyed in accordance with
Results: 174 µg/kg
applicable regulations
Eggs
12x
-Inquiry on the farm including official sampling
MADURAMICIN
-prohibition of placing eggs on the market till the
Matrix:Eggs
bussines operator with his own checks proves that
Animal: Hen
eggs is in compliance with legislation
Results: 1.8 µg/kg – 9.6 µg/kg
-conducted official inspection and control
including official sampling on all major egg farms
and packing centers
-taking official samples of animal feed on farms
and conducted official inspection and control in
the feed mills
-Inform European Commission, Health and
Consumer Protection Directorate-General, Unit
E3: Chemicals, Contaminants and Pesticides about
the problem with level of maduramicin in feed and
eggs (possible non-harmonisation in the legislation
between the authorised maximum level of carryover of the coccidiostat, maduramicin, in animal
feed, and the MRL of maduramicin in eggs).
Horses
2x
Check on slaughterhouse storage premises and
CADMIUM
when the other kidney was found, it was
Matrix: kidney
categorized as category 1 according to Regulation
Animal : Horse
2002/1774 ES;
Results: >6 mg/kg, >6 mg/kg
- Data of heavy metals are collected separately
and they will be incluted in the new aplication
which will provide us an overview of situation
(contamination with heavy metals) in our country.
Bovines
4x
Check on slaughterhouse storage premises and
CADMIUM
when the other kidney was found, it was
160
Matrix: kidney
categorized as category 1 according to Regulation
Animal : cow
2002/1774 ES;
Results:1,6 mg/kg; 3,32 mg/kg,
- Data of heavy metals are collected separately
1,67 mg/kg, 2,5 mg/kg
and they will be incluted in the new aplication
which will provide us an overview of situation
(contamination with heavy metals) in our country.
RESULTS OF RESIDUE MONITORING PROGRAMME AT BIPs
2x
MERCURY
Matrix: muscle
Animal : fish
Results: 0,55 mg/kg, 2,54 mg/kg
Follow-up actions
Fresh fish
- RASFF notification
- next 10 batches from the same source are
impounded and checked on presence of Mercury;
161
SK
SLOVAK REPUBLIC
Group A substances
Follow-up actions
Substance--Matrix-animal or animal Actions: (investigations in the farm of origin,
Example: MPA-kidney fat-pig-3 ppb intensified sampling in related farms, products
Group B substances
Follow-up actions
Bovines
1 Dimetridazole – Bovines – liveList actions: Under the National Residue Control
blood serum
Plan (NRCP) the blood sample from young
breeding cattle was taken on the farm, in which the
exceeded MRL of dimetridazole was detected. The
sample was tested by the accredited confirmation
method which confirmed a positive result for
dimetridazole. After reporting a positive result, the
respective District Veterinary and Food
Administration (DVFA) performed the additional
official control – investigation on the farm of
dimetridazole finding. It aimed at recording of
using the veterinary medicinal products and their
administration. The control did not reveal any
breaking of valid rules. The DVFA ordered by
measures the ban on movement of the suspicious
animal from the farm pending the results of
examination of suspect sample. Within the
investigation also samples of feed and drinking
water (own well) from the farm of housing and
origin of the animal were taken. By the additional
official control of measures their fulfilment was
162
1 Dimetridazole – live pig – blood
serum
1 Chloramphenicole – raw sheep
milk
found out. The suspect sample was negative.
Pigs
List actions: Under the NRCP the blood sample
was taken from the fattening pig on the farm and
the exceeded MRL of dimetridazole was detected.
The sample was examined by the accredited
confirmation method which confirmed the positive
finding of dimetridazole. Within the investigation
the suspect blood samples were taken also from
further pig from the same pen. In suspect blood
samples no presence of dimetridazole was
detected. The respective DVFA aimed upon the
investigation of positive dimetridazole finding at
the recording of veterinary medicinal products
used on the farm, their administration and by the
investigation no braking of valid rules was found
out. The DVFA ordered by measures the ban on
movement of pigs from which the samples were
taken, pending the results of examination. The
feed and drinking water samples were taken (own
well) from the farm. The results of examinations
did not confirm the presence of dimetridazole in
the blood of pigs, feed or water. By the additional
official control the fulfilment of ordered measures
was found out.
Poultry
Sheep and goat
Horses
Milk
List actions: Under the NRCP 1 commingled
sample of raw sheep milk was taken on the sheep
farm from the total amount of 60 l of milk. In the
sample the exceeded MRL of chloramphenicole
was found out by the accredited confirmation
method. After reporting a positive result for
chloramphenicole, the respective DVFA
performed the notification to the Rapid Alert
System for Food and Feed (RASFF) and
performed the investigation on the farm aimed at
the use of veterinary medicinal products, milking
hygiene of raw sheep milk and hygiene of
production of lumpy sheep cheese on the farm.
From the raw sheep milk the lumpy sheep cheese
was produced that was sold at the time of
investigation in small quantities to farm employees
and consumed. By the additional official control
163
1 DDT – hen’s eggs graded
1 Malachite-Green-Leuco – troutfarmed fish
no breaking of valid rules was found out. The
DVFA ordered measures to ban the placing on the
market of sheep milk and products thereof and
movement of sheep from the farm pending the
results of examination of suspect raw sheep milk
sample (commingled).
The results of examinations did not confirm the
presence of chloramphenicole in raw sheep milk.
By the additional official control the fulfilment of
measures ordered by the DVFA was found out.
Eggs
List actions: Under the NRCP the sample of hen’s
eggs was taken from the alternative hen’s farming
–laying hens with egg production and the
exceeded MRL of DDT was detected, confirmed
by the accredited confirmation method. After
reporting a positive finding of DDT, the DVFA
performed an investigation on the farm aimed at
detection of DDT source in the holding. By the
control it was found out that one range for laying
hens was located in the vicinity of the storehouse
of chemicals. The DVFA ordered measures for the
ban of the use of hen’s eggs from the holding for
human consumption, ordered to perform sanitation
of all ranges in the holding and to cancel the range
in the vicinity of the storehouse of chemicals and
not to use it upon alternative hen’s farming. The
suspect samples were not taken because the
holding of laying hens was immediately cancelled
from the decision of the owner and the animals
destroyed.
Rabbit
Aquaculture
List actions: Under the NRCP 1 fish sample from
farmed breeding - trout was taken in the breeder of
salmonids. By the accredited confirmation method
the exceeded MRL of Malachite-Green-Leuco was
found out. The DVFA performed the investigation
in a fish breeder. The DFVA immediately ordered
measures in respect of the ban on the movement,
transport and placing on the market of live fish
from the affected breeding facility and to submit to
the DVFA the results of laboratory examinations
from the performed control taking of fish samples
for the presence of Malachite-Green and
Malachite-Green-Leuko from all fish ponds and
tanks where are the fish intended for the market.
The whole holding was subsequently disposed due
164
1 Lead – Wild boar - muscle
2 Tylosin – bee honey
to infection by VHS virus.
Farmed game
Wild game
List actions: Under the NRCP the sample of wild
game muscle – wild boar was taken. The exceeded
MRL of lead in wild boar was reported to the
competent DVFA that ordered the measures by
which it prohibited the consumption of hunted
game prior to performance of repeated
examination of suspect sample for lead presence
and taking of sample for the lead presence from
the subsequently hunted game in the hunting
ground. The meat and viscera from this game will
be released for the human consumption after
obtaining a negative result only. It was proved by
the investigation that the sample did not originate
from the place of the shot surroundings. The
repeated muscle sample was taken from further
wild boar in the hunting ground in which the
exceeded MRL of lead was not found out.
Honey
List actions: Under the NRCP the exceeded MRL
of tylosine was detected in 2 samples of bee
honey. The sample was taken from 50-liter cans.
The DVFA performed the investigation and
ordered by measures the safe disposal of the honey
suspended at the time of the control and
submission of a document on its disposal, to report
to the DVFA the subsequent production of the
honey for the reason of the taking the official
sample. The DVFA by measures also prohibited
the honey producer to put into circulation the bee
honey and bee products intended for human
consumption pending the result of the examination
of the additional official sample. The honey was
disposed and confirmation on its disposal was
delivered to the DVFA.
165
SW
SWEDEN
Group A substances
Substance-Concentration-Matrixanimal or animal product*
Follow-up actions
Group B substances
plan
Follow-up actions
Bovines
Pigs
liver
2 Doramectin (two animals from
the same farm)
@ verification of records, investigation on the
farm, administrative measures).
Poultry
Sheep and goat
Horses
Milk
Eggs
Rabbit
Aquaculture
Farmed game
166
Wild game
Honey
167
UK
UNITED KINGDOM
Group A substances
Follow-up actions
Alpha-boldenone cattle urine 1, 2,
Residues were unconjugated alpha boldenone. All
2, 2, 2, 3, 3, 3, 3, 3.8, 4, 5, 5, 8,
samples were collected on farm and some were
11ppb,
discoloured; indicative of faecal contamination.
One on farm investigation was carried out and no
Alpha-boldenone sheep urine 1, 1,
evidence of abuse was found.
2, 2, 2, 2, 2.6, 3, 3, 6, 9, 10
Residues were unconjugated alpha boldenone. All
samples were collected at the abattoirs but were
discoloured indicative of Faecal contamination.
No evidence of abuse was found. However in the
Alpha-Nortestosterone in Cattle
case of one sample the farm of origin could not be
Urine 0.40,0.74, 6.2, 7, 7, 11, 33
traced.
One sample was taken at the abattoir and the
remaining samples were collected on farm... 4
Alpha-Nortestosterone in Sheep
samples were from female cattle that were in calf
Urine 0.3, 1, 1, 1, 1, 1, 1, 1, 1, 1, 1, at the time the samples were taken. On farm
1, 1.9, 2, 2, 2, 2, 2, 2, 2, 2, 2, 2, 2,
investigations were carried out for 3 samples and
2,2, 2.4, 2.5
no evidence of abuse was found.. Follow up
Zeranol in Cattle Urine, 0.40, 0.60, samples were compliant.
0.6, 0.9, 0.90, 1, 1, 1, 2, 2, 2, 3, 5, 6, No follow up investigations were undertaken into
12
the cause of these residues as past investigations
suggest that alpha-nortestosterone occurs naturally
in sheep at low concentrations.
Samples were collected at both Farms and
Taleranol in cattle(YB) urine, 1.7
Abattoirs. On farm investigations were carried out
for 3 samples and no evidence of abuse was found.
Research has shown that residues of zeranol can
Zeranol in Sheep Urine, 2
occur where an animal ingests contaminated feed.
Letters sent to the farmers of the remaining
Thiouracil inCattle Urine, 6, 6.5,
samples advising how to avoid residues in the
18
future.
On farm investigation established this was due to
Clenbuterol in Cattle urine, 0.2
the animal ingesting contaminated feed. No
further action was taken and farm was notified.
Progesterone in Cattle urine, 10
The sample was collected at the abattoir and an on
farm investigation was carried out. The residue
was found to be as a result of feed contamination
on the farm .
On farm investigations were carried out from
where the samples were originally collected and
168
follow up samples were all compliant.
The sample was collected on farm and a follow up
investigation was carried out. Follow up samples
were all compliant.
A follow-up investigation was requested when
this sample was reported. To date no samples have
been received. According to movement records,
this animal was transferred from another farm the
day before it was presented for slaughter.
Group B substances
Follow-up actions
Bovines
6 Cadmium in cattle kidney
Farm investigations for all samples. The source of
residue was not established in 4 samples. in one
sample it was accumulation due to diet. One
2 Dihydrostreptomycin/
sample due to environmental pollution. Follow up
Sulphadiazine in calves kidneys.
samples taken were all compliant.
Farm investigations: One calf was slaughtered
2 Benzimidazoles/Levamisole in
within the withdrawal period and the farmer has
cattle liver
received written advice.
Farm investigations: Medicine records and storage
checked. One animal had been slaughtered before
the end of the withdrawal period. The farmer has
1 Tilmicosin in cattle kidney
been advised on the requirements for record
keeping. The details of the second animal had
been incorrectly recorded at the abattoir..
2 Chlortetracycline in calves kidney Measures have been taken to prevent such
occurances.
A farm investigation found that this animal was
sent to slaughter whilst within the withdrawal
2 Phenylbutazone in cattle serum
period. Both the farmer and veterinary surgeon
have received written advice.
Farm investigations: One animal had been sent to
slaughter within the withdrawal period, the farmer
has received written advice. In the second case,
the investigating officer could not find any
evidence of the use of Chlortetracycline on the
farm.
Detected at time of slaughter confirmed in the case
of one where follow-up was initiated. An on-farm
investigation has been carried out in the case of the
169
1 Dexamethasone in cattle liver
first sample. This is a dairy herd. Medicine records
are in place in accordance with legislation. The
heard owner was unaware of the use of this
substance. It was noted that there are also horses
on the farm. There was no sign of phenylbutazone
on the farm. There was turnover of staff during
this period and a new foreman is now in place. The
owner & the foreman are now aware of the
situation. The DVO has sent a letter to the herd
owner and the heard has been flagged for sampling
of cows at slaughter.
The second sample, from a one year old male
bovine was tested for phenylbutazone at slaughter.
The farm was visited on 15.06.09; it is
predominantly a dairy farm that rears some bull
beef (the sampled animal was home bred). No
treatment was recorded for the sampled animal;
computerised records were checked for a few other
animals and found to be appropriate. The
medicines store contained several sachets of
Danilon Equidos (suxibuzone, a phenylbutazone
prodrug, licensed for use in horses not intended for
human consumption). The farmer said that these
were supplied by the PVP for use in cows that had
done the ‘splits’. It had not been given to the
sampled animal, and he had no record of its use in
others as this was too long ago to be computer
recorded. A total of 6 cows were blood sampled
(including one that was lame), only one sample
was suitable for analysis which was compliant.
Resampling was requested. The DVO has written
to the herdkeeper and the PVP about their
responsibilities.
Tested in the liver of one OTM. The farm was
visited on 22.06.2009. This herd is a short term
finisher/haulier with animals purchased only a few
days before presenting for slaughter. Medicine
records were checked and were found to be well
maintained. There was no entry for this animal.
This animal had been sold through a market the
day before slaughter (this may have contributed to
a breakdown in foodchain information). The
carcase was condemned at post mortem inspection
for abscess/pyaemia, and fascioliasis was also
reported and therefore did not enter the food chain.
170
1 Sulfadiazine
2 Chlortetracycline in pigs
1 Oxytetracycline in pigs kidney
3 Chlortetracycline in poultry
muscle.
Pigs
Farm investigation undertaken. Medicine records
and storage checked. The most likely cause of this
residue was considered to be unintentional crosscontamination of the feed.
Farm investigations: In one case it was established
that the animal was slaughtered within the
withdrawal period. In the second case the cause of
the residue could not be established. It is possible
that incorrect details were recorded at the abattoir.
Farm investigation established that the residue was
due to cross contamination of feed on farm.
Poultry
On farm investigations were carried out. Medicine
records and storage checked. The investigations
considered that the most likely cause was crosscontamination of the feed either at the feed-mill or
during transport.
Ionophores/Nicarbazines in poultry,
1 Salinomycin 3, Lasalocid, 1
Investigations carried out at 15 farms/mills .In
Monensin and 42 Nicarbazines,
these cases samples of retained feed from the mill
and/or farm were tested but none confirmed
positive.
In cases where the farm and mill were investigated
the most likely cause of the residue was considered
to be cross-contamination of feed due to the use of
a single bin-system on the farms. In one other
case the most likely cause was considered to be
due to the birds foraging in the litter and picking
up medicated feed.
Farms have received written advice in all of the
above cases.
Letters sent to farms where lower level residues of
Nicarbazin have been detected advising on how to
avoid residues
3 Cadmium in sheep kidney
2 Lead in sheep kidney
1 Chlorpyrofos in sheep kidney fat.
Sheep and goat
Farm investigations: There were no obvious
sources of cadmium on the farms and it was not
possible to establish the cause of these residues
Far investigations: The cause of the residue in one
was due to environmental pollution. The likely
cause of the second was whilst grazing the animal
had licked an item with lead based paint washed
up on the shore.
On farm investigation undertaken. There is no
171
1 Doramectin in sheep liver.
1 Oxfendazole in sheep liver
1 Amoxycillin in cows milk
1 nicarbazin in free range egg
1 P, P-DDE in free range egg
3 Emamectin in Salmon muscle.
1 Lasalocid in partridge muscle.
evidence to suggest abuse or accidental
contamination. The residue is most likely to have
come through exposure of animal to a recently
sprayed field.
On farm investigation undertaken. The sheep was
slaughtered within the withdrawal period. It was
probably treated at a pervious farm and bought for
slaughter. No records exist of previous locations.
On farm investigation undertaken. Animal was
mistakenly dosed with de-wormer at a
neighbouring farm without owner’s knowledge. It
was sent to slaughter by the owner within the
withdrawal period.
Milk
On farm investigation undertaken. The animals
had been treated with Duphamox, but the
medicines records had not been updated. The milk
sample was still within the withdrawal period.
The farmer has received written advice to avoid a
re-occurrence.
Eggs
On farm investigation undertaken. It suggested
that the most likely cause was cross-contamination
of the feed, though it was unclear exactly where
this had occurred. The mill has tightened up its
procedures to try and further minimise the chances
of cross-contamination. 6 follow up target samples
were taken, all proved compliant.
On farm investigation undertaken. It is a small
free range farm where birds were foraging in an
old orchard, where the residual contamination of
DDT could have been picked up. All the birds and
eggs have been disposed of.
Aquaculture
Three samples above the MRLs were sent for
follow up investigations. One sample results
showed there were no irregularities it was taken
just after the end of withdrawal period. In the case
of the other two samples. it appears that a
miscalculation of biomass to be treated had
occurred, resulting in a higher dosage of medicine
being administered, which contributed to the MRL
being exceeded. The Farm has been notified.
Farmed game
Farm and mill investigation undertaken. The
investigation established the most likely cause of
contamination was at the bagging stage of the
process within the Mill. The mill has received
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2 lead in wild deer muscle
1 Naphthalene/1-4 dichlorobenzene
in honey
written advice and a revised bagging procedure is
now in place.
Wild game
There were no follow-up investigations as the
residues were most likely to have been the result
of the deer being shot.
Honey
Farm investigation undertaken. The investigation
established that likely cause of residue was crosscontamination. The bee-keeper had treated his
supors with naphthalene/1-4 dichlorobenzene in
winter to prevent wax moth. The sample was taken
from a brood comb about a month before any
honey was withdrawn for bottling. The Local
Authority took samples from the bottled honey.
They informed the beekeeper that the honey
should be withdrawn from sale.
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EUROPEAN COMMISSION Brussels, 07.04.2011

Transcripción

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